Preparation, properties and structures of 1-methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium crystals with various counter anions
1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO) crystalline material. However, studies on property variation caused by anion exchange are still an interesting subject to find out new compounds not on...
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| Published in | Journal of crystal growth Vol. 310; no. 4; pp. 836 - 842 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.02.2008
Elsevier |
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| Abstract | 1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium
p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO) crystalline material. However, studies on property variation caused by anion exchange are still an interesting subject to find out new compounds not only with large NLO properties but also with easy crystal-growing ability. In this report, some 1-methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium derivatives with
p- or
m-substituted benzenesulfonate or 2-naphthalenesulfonate were prepared and their thermal properties, solubility in methanol and SHG activity were investigated. Their crystal growth was performed by the slow cooling method, and quality crystals for X-ray crystallographic analysis were obtained for three compounds. Among them, crystal structures of
p-ethylbenzenesulfonate and
p-styrenesulfonate derivatives were found to be almost the same as those of DAST. |
|---|---|
| AbstractList | 1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO) crystalline material. However, studies on property variation caused by anion exchange are still an interesting subject to find out new compounds not only with large NLO properties but also with easy crystal-growing ability. In this report, some 1-methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium derivatives with p- or m-substituted benzenesulfonate or 2-naphthalenesulfonate were prepared and their thermal properties, solubility in methanol and SHG activity were investigated. Their crystal growth was performed by the slow cooling method, and quality crystals for X-ray crystallographic analysis were obtained for three compounds. Among them, crystal structures of p-ethylbenzenesulfonate and p-styrenesulfonate derivatives were found to be almost the same as those of DAST. 1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO) crystalline material. However, studies on property variation caused by anion exchange are still an interesting subject to find out new compounds not only with large NLO properties but also with easy crystal-growing ability. In this report, some 1-methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium derivatives with p- or m-substituted benzenesulfonate or 2-naphthalenesulfonate were prepared and their thermal properties, solubility in methanol and SHG activity were investigated. Their crystal growth was performed by the slow cooling method, and quality crystals for X-ray crystallographic analysis were obtained for three compounds. Among them, crystal structures of p-ethylbenzenesulfonate and p-styrenesulfonate derivatives were found to be almost the same as those of DAST. |
| Author | Okada, Shuji Glavcheva, Zornitza Ogawa, Junko Nakanishi, Hachiro |
| Author_xml | – sequence: 1 givenname: Junko surname: Ogawa fullname: Ogawa, Junko organization: Department of Polymer Science and Engineering, Graduate School of Science and Engineering, Yamagata University, 4-3-16 Jonan, Yonezawa, Yamagata 992-8510, Japan – sequence: 2 givenname: Shuji surname: Okada fullname: Okada, Shuji email: okadas@yz.yamagata-u.ac.jp organization: Department of Polymer Science and Engineering, Graduate School of Science and Engineering, Yamagata University, 4-3-16 Jonan, Yonezawa, Yamagata 992-8510, Japan – sequence: 3 givenname: Zornitza surname: Glavcheva fullname: Glavcheva, Zornitza organization: Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan – sequence: 4 givenname: Hachiro surname: Nakanishi fullname: Nakanishi, Hachiro organization: Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan |
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| Keywords | 61.66.Hq B1. Aromatic compounds A1. Crystal structure 42.65.Ky 42.70.Mp A2. Growth from solutions B2. Nonlinear optical materials B1. Organic compounds 81.10.Dn A1. Solubility Crystal growth Second harmonic generation Solubility Crystal perfection Aromatics Thermal properties Diffraction pattern analysis Slow cooling Optical materials Ion exchange Nonlinear optics Organic compounds Methanol Crystal structure |
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| Snippet | 1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium
p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO)... 1-Methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium p-toluenesulfonate (DAST) is known to be an excellent second-order nonlinear optical (NLO)... |
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| SubjectTerms | A1. Crystal structure A1. Solubility A2. Growth from solutions B1. Aromatic compounds B1. Organic compounds B2. Nonlinear optical materials Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Exact sciences and technology Fundamental areas of phenomenology (including applications) Growth from solutions Materials science Methods of crystal growth; physics of crystal growth Nonlinear optical crystals Optical materials Optics Organic compounds Physics Structure of solids and liquids; crystallography Structure of specific crystalline solids Thermal expansion; thermomechanical effects and density Thermal properties of condensed matter Thermal properties of crystalline solids |
| Title | Preparation, properties and structures of 1-methyl-4-{2-[4-(dimethylamino)phenyl]ethenyl}pyridinium crystals with various counter anions |
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