Two‐dimensional Cu Plates with Steady Fluid Fields for High‐rate Nitrate Electroreduction to Ammonia and Efficient Zn‐Nitrate Batteries

Nitrate electroreduction reaction (eNO3−RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3−RR could be significantly boosted...

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Published inAngewandte Chemie International Edition Vol. 63; no. 18; pp. e202401924 - n/a
Main Authors Zhou, Limin, Chen, Xueqiu, Zhu, Shaojun, You, Kun, Wang, Zheng‐Jun, Fan, Ru, Li, Jun, Yuan, Yifei, Wang, Xin, Wang, Jichang, Chen, Yihuang, Jin, Huile, Wang, Shun, Lv, Jing‐Jing
Format Journal Article
LanguageEnglish
Published Germany Wiley Subscription Services, Inc 24.04.2024
EditionInternational ed. in English
Subjects
Ammonia
Carrier gases
Catalysts
Cu plates
Electrocatalysts
Electrolysis
Electrowinning
Fluid field
Infrared spectroscopy
Nitrate electroreduction reaction
Nitrates
Plates
Zn-nitrate battery
Cu plates
Fluid field
Nitrate electroreduction reaction
Zn-nitrate battery
Online AccessGet full text
ISSN1433-7851
1521-3773
1521-3773
DOI10.1002/anie.202401924

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Abstract Nitrate electroreduction reaction (eNO3−RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3−RR could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO3−RR setup provided superior NH3 Faradaic efficiency (FE) of 99 %, exceptional long‐term electrolysis for 120 h at 200 mA cm−2, and a record‐high yield rate of 3.14 mmol cm−2 h−1. Furthermore, the proposed strategy was successfully extended to the Zn‐nitrate battery system, providing a power density of 12.09 mW cm−2 and NH3 FE of 85.4 %, outperforming the state‐of‐the‐art eNO3−RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high‐efficiency NH3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis. The performance of nitrate electroreduction reaction (eNO3−RR) could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas in a microfluid flow cell to construct a steady fluid field. The developed eNO3−RR setup provided superior NH3 Faradaic efficiency, exceptional long‐term electrolysis, and could be extended to assemble efficient Zn‐nitrate batteries.
AbstractList Nitrate electroreduction reaction (eNO3−RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3−RR could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO3−RR setup provided superior NH3 Faradaic efficiency (FE) of 99 %, exceptional long‐term electrolysis for 120 h at 200 mA cm−2, and a record‐high yield rate of 3.14 mmol cm−2 h−1. Furthermore, the proposed strategy was successfully extended to the Zn‐nitrate battery system, providing a power density of 12.09 mW cm−2 and NH3 FE of 85.4 %, outperforming the state‐of‐the‐art eNO3−RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high‐efficiency NH3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis.
Nitrate electroreduction reaction (eNO3−RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3−RR could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO3−RR setup provided superior NH3 Faradaic efficiency (FE) of 99 %, exceptional long‐term electrolysis for 120 h at 200 mA cm−2, and a record‐high yield rate of 3.14 mmol cm−2 h−1. Furthermore, the proposed strategy was successfully extended to the Zn‐nitrate battery system, providing a power density of 12.09 mW cm−2 and NH3 FE of 85.4 %, outperforming the state‐of‐the‐art eNO3−RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high‐efficiency NH3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis. The performance of nitrate electroreduction reaction (eNO3−RR) could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas in a microfluid flow cell to construct a steady fluid field. The developed eNO3−RR setup provided superior NH3 Faradaic efficiency, exceptional long‐term electrolysis, and could be extended to assemble efficient Zn‐nitrate batteries.
Nitrate electroreduction reaction (eNO 3 − RR) to ammonia (NH 3 ) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO 3 − RR could be significantly boosted by introducing two‐dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO 3 − RR setup provided superior NH 3 Faradaic efficiency (FE) of 99 %, exceptional long‐term electrolysis for 120 h at 200 mA cm −2 , and a record‐high yield rate of 3.14 mmol cm −2  h −1 . Furthermore, the proposed strategy was successfully extended to the Zn‐nitrate battery system, providing a power density of 12.09 mW cm −2 and NH 3 FE of 85.4 %, outperforming the state‐of‐the‐art eNO 3 − RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high‐efficiency NH 3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis.
Nitrate electroreduction reaction (eNO3 -RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3 -RR could be significantly boosted by introducing two-dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO3 -RR setup provided superior NH3 Faradaic efficiency (FE) of 99 %, exceptional long-term electrolysis for 120 h at 200 mA cm-2, and a record-high yield rate of 3.14 mmol cm-2 h-1. Furthermore, the proposed strategy was successfully extended to the Zn-nitrate battery system, providing a power density of 12.09 mW cm-2 and NH3 FE of 85.4 %, outperforming the state-of-the-art eNO3 -RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high-efficiency NH3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis.Nitrate electroreduction reaction (eNO3 -RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO3 -RR could be significantly boosted by introducing two-dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO3 -RR setup provided superior NH3 Faradaic efficiency (FE) of 99 %, exceptional long-term electrolysis for 120 h at 200 mA cm-2, and a record-high yield rate of 3.14 mmol cm-2 h-1. Furthermore, the proposed strategy was successfully extended to the Zn-nitrate battery system, providing a power density of 12.09 mW cm-2 and NH3 FE of 85.4 %, outperforming the state-of-the-art eNO3 -RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high-efficiency NH3 production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis.
Nitrate electroreduction reaction (eNO RR) to ammonia (NH ) provides a promising strategy for nitrogen utilization, while achieving high selectivity and durability at an industrial scale has remained challenging. Herein, we demonstrated that the performance of eNO RR could be significantly boosted by introducing two-dimensional Cu plates as electrocatalysts and eliminating the general carrier gas to construct a steady fluid field. The developed eNO RR setup provided superior NH Faradaic efficiency (FE) of 99 %, exceptional long-term electrolysis for 120 h at 200 mA cm , and a record-high yield rate of 3.14 mmol cm  h . Furthermore, the proposed strategy was successfully extended to the Zn-nitrate battery system, providing a power density of 12.09 mW cm and NH FE of 85.4 %, outperforming the state-of-the-art eNO RR catalysts. Coupled with the COMSOL multiphysics simulations and in situ infrared spectroscopy, the main contributor for the high-efficiency NH production could be the steady fluid field to timely rejuvenate the electrocatalyst surface during the electrocatalysis.
Author Wang, Shun
Wang, Xin
Zhou, Limin
You, Kun
Li, Jun
Wang, Jichang
Chen, Yihuang
Fan, Ru
Chen, Xueqiu
Jin, Huile
Zhu, Shaojun
Yuan, Yifei
Wang, Zheng‐Jun
Lv, Jing‐Jing
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  organization: Wenzhou University
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  organization: Wenzhou University
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  organization: Zhejiang Engineering Research Center for Electrochemical Energy Materials and Devices
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  email: jjlyu@wzu.edu.cn
  organization: Wenzhou University
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Keywords Cu plates
Fluid field
Nitrate electroreduction reaction
Zn-nitrate battery
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Snippet Nitrate electroreduction reaction (eNO3−RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and...
Nitrate electroreduction reaction (eNO 3 − RR) to ammonia (NH 3 ) provides a promising strategy for nitrogen utilization, while achieving high selectivity and...
Nitrate electroreduction reaction (eNO RR) to ammonia (NH ) provides a promising strategy for nitrogen utilization, while achieving high selectivity and...
Nitrate electroreduction reaction (eNO3 -RR) to ammonia (NH3) provides a promising strategy for nitrogen utilization, while achieving high selectivity and...
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StartPage e202401924
SubjectTerms Ammonia
Carrier gases
Catalysts
Cu plates
Electrocatalysts
Electrolysis
Electrowinning
Fluid field
Infrared spectroscopy
Nitrate electroreduction reaction
Nitrates
Plates
Zn-nitrate battery
Title Two‐dimensional Cu Plates with Steady Fluid Fields for High‐rate Nitrate Electroreduction to Ammonia and Efficient Zn‐Nitrate Batteries
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fanie.202401924
https://www.ncbi.nlm.nih.gov/pubmed/38366134
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https://www.proquest.com/docview/2928244466
Volume 63
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