Head group specificity of novel functionalized surfactants: synthesis, self-assembly and calcium tolerance
•Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed. The present work describes the synthesis,...
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Published in | Tetrahedron letters Vol. 55; no. 43; pp. 5925 - 5931 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
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Elsevier Ltd
22.10.2014
Elsevier |
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Abstract | •Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed.
The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol–keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air–water interface has been projected to cause this difference which is very interesting. |
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AbstractList | The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol-keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca super(2+) ion than the other. The individual packing behaviour of the surfactants at the air-water interface has been projected to cause this difference which is very interesting. •Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed. The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol–keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air–water interface has been projected to cause this difference which is very interesting. The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol-keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air-water interface has been projected to cause this difference which is very interesting. (C) 2014 Elsevier Ltd. All rights reserved. |
Author | Gadgil, Vijay Sarkar, Deboleena Shukla, Ravi Kant Pramanik, Amitava |
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CitedBy_id | crossref_primary_10_1016_j_colsurfa_2016_03_066 crossref_primary_10_1021_acs_analchem_9b03008 |
Cites_doi | 10.1021/la701151m 10.1021/jp901228v 10.1016/j.tetlet.2006.09.072 10.1021/ja803491y 10.1016/j.bbamem.2007.12.010 10.1021/ja055907h 10.1021/bc700181k 10.1021/bp050239p 10.1007/s10529-012-0956-x 10.1016/j.envpol.2004.06.009 10.1016/j.abb.2004.12.010 10.1021/la1021356 10.1016/s0021-9797(03)00027-4 10.1021/jm0499763 10.1021/bm700930y 10.1016/j.jcis.2009.06.032 10.1038/nbt0192-60 10.1006/jcis.1998.5750 10.1073/pnas.94.4.1160 10.1016/S0021-9258(19)50490-2 10.1007/BF02663829 10.1007/BF02671763 10.1021/la00085a015 10.1021/j100501a011 10.1039/a605577j 10.1016/0021-9797(87)90192-5 10.1517/14712598.5.1.33 10.1524/ract.1997.78.special-issue.39 10.1063/1.1746738 10.1007/BF02540479 10.1016/0021-9797(86)90390-5 10.1007/s002530051648 10.1016/0009-3084(95)02494-4 10.1016/S0040-4039(02)00758-X 10.1016/S0021-9797(03)00027-4 10.1016/S1004-9541(08)60115-9 10.1016/0021-9797(80)90117-4 |
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Keywords | CMC Aggregation number NMR Surface tension Ca2+ tolerance Surfactant PYRIDINIUM CATIONIC LIPIDS GENE TRANSFECTION EFFICACIES ALKYLOXYETHYLENE SULFATE AROMATIC BACKBONE ANIONIC SURFACTANT BIOSURFACTANTS DELIVERY OILY SOIL REMOVAL DNA COMPLEXES CHLORIDE |
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Snippet | •Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with... The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These... |
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SubjectTerms | Aggregation number Attachment Ca2+ tolerance Calcium Chains Chemistry Chemistry, Organic CMC NMR Physical Sciences Science & Technology Self assembly Surface tension Surfactant Surfactants Synthesis (chemistry) Tolerances Water hardness |
Title | Head group specificity of novel functionalized surfactants: synthesis, self-assembly and calcium tolerance |
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