Head group specificity of novel functionalized surfactants: synthesis, self-assembly and calcium tolerance

•Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed. The present work describes the synthesis,...

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Published inTetrahedron letters Vol. 55; no. 43; pp. 5925 - 5931
Main Authors Sarkar, Deboleena, Shukla, Ravi Kant, Gadgil, Vijay, Pramanik, Amitava
Format Journal Article
LanguageEnglish
Published OXFORD Elsevier Ltd 22.10.2014
Elsevier
Subjects
Aggregation number
Attachment
Ca2+ tolerance
Calcium
Chains
Chemistry
Chemistry, Organic
CMC
NMR
Physical Sciences
Science & Technology
Self assembly
Surface tension
Surfactant
Surfactants
Synthesis (chemistry)
Tolerances
Water hardness
CMC
Aggregation number
NMR
Surface tension
Ca2+ tolerance
Surfactant
PYRIDINIUM CATIONIC LIPIDS
GENE TRANSFECTION EFFICACIES
ALKYLOXYETHYLENE SULFATE
AROMATIC BACKBONE
ANIONIC SURFACTANT
BIOSURFACTANTS
DELIVERY
OILY SOIL REMOVAL
DNA COMPLEXES
CHLORIDE
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Abstract •Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed. The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol–keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air–water interface has been projected to cause this difference which is very interesting.
AbstractList The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol-keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca super(2+) ion than the other. The individual packing behaviour of the surfactants at the air-water interface has been projected to cause this difference which is very interesting.
•Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with respect to each other.•One type is found to be more calcium tolerant than the other, reasons disclosed. The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol–keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air–water interface has been projected to cause this difference which is very interesting.
The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These surfactants have been particularly tailor made to resist hardness due to calcium ions in water. It is unique of its kind because here the surfactants have an analogous hydrophobic chain but differ structurally in the composition of the head groups in terms of the position of attachment of the chain. The effect of this small variability in the head group on the surfactant property, adsorption, self assembly and calcium tolerance behaviour has been studied in detail. This kind of phenol-keto surfactants has not been reported before. It was also found that one of the surfactants was more tolerant towards Ca2+ ion than the other. The individual packing behaviour of the surfactants at the air-water interface has been projected to cause this difference which is very interesting. (C) 2014 Elsevier Ltd. All rights reserved.
Author Gadgil, Vijay
Sarkar, Deboleena
Shukla, Ravi Kant
Pramanik, Amitava
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Issue 43
Keywords CMC
Aggregation number
NMR
Surface tension
Ca2+ tolerance
Surfactant
PYRIDINIUM CATIONIC LIPIDS
GENE TRANSFECTION EFFICACIES
ALKYLOXYETHYLENE SULFATE
AROMATIC BACKBONE
ANIONIC SURFACTANT
BIOSURFACTANTS
DELIVERY
OILY SOIL REMOVAL
DNA COMPLEXES
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Snippet •Novel surfactants with analogous head groups have been synthesized and characterized.•Surfactant properties and self assembly behaviour were studied with...
The present work describes the synthesis, characterization and application of functionalized surfactants derived through simple organic reaction steps. These...
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SubjectTerms Aggregation number
Attachment
Ca2+ tolerance
Calcium
Chains
Chemistry
Chemistry, Organic
CMC
NMR
Physical Sciences
Science & Technology
Self assembly
Surface tension
Surfactant
Surfactants
Synthesis (chemistry)
Tolerances
Water hardness
Title Head group specificity of novel functionalized surfactants: synthesis, self-assembly and calcium tolerance
URI https://dx.doi.org/10.1016/j.tetlet.2014.08.111
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