Interaction between single walled carbon nanotube and 1D crystal in CuX@SWCNT (X=Cl, Br, I) nanostructures
CuX@SWCNT (X=Cl, Br, I) nanostructures were prepared by capillary filling of 1.4–1.6nm single-walled carbon nanotubes (SWCNT) with copper halides. The structure of CuX@SWCNT (X=Cl, Br, I) represents a distorted two-layer hcp of halogen atoms arranged along the SWCNT. The EXAFS and the high angle ang...
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| Published in | Carbon (New York) Vol. 50; no. 11; pp. 4021 - 4039 |
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| Main Authors | , , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.09.2012
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| Online Access | Get full text |
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| Abstract | CuX@SWCNT (X=Cl, Br, I) nanostructures were prepared by capillary filling of 1.4–1.6nm single-walled carbon nanotubes (SWCNT) with copper halides. The structure of CuX@SWCNT (X=Cl, Br, I) represents a distorted two-layer hcp of halogen atoms arranged along the SWCNT. The EXAFS and the high angle angular dark field (HAADF) HRTEM data indicate that Cu is partially coordinated by C. According to the optical absorption, valence band photoemission spectroscopy and work function measurements, a Fermi level (FL) downshift as compared with the initial value for the nanotubes and a corresponding charge transfer from the nanotubes to the 1D crystals is observed for CuX@SWCNT nanostructures. The FL shift increases in the sequence CuI<CuBr<CuCl due to an increase of the electron affinity for the halogen atoms. The XPS data confirm the acceptor effect of copper halides and indicate that metallic and semiconducting nanotubes behave differently. Raman spectroscopy performed under electrochemical charging allowed estimation of the value of charge transfer between the nanotube walls and the intercalated 1D crystal. The X-ray absorption and emission spectra for carbon and copper thresholds revealed a new energy level composed of the carbon 2рz and copper 3d-orbitals. This indicates the Cu–C bonding, which in line with the structural HAADF HRTEM and EXAFS data. |
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| AbstractList | CuX@SWCNT (X=Cl, Br, I) nanostructures were prepared by capillary filling of 1.4–1.6nm single-walled carbon nanotubes (SWCNT) with copper halides. The structure of CuX@SWCNT (X=Cl, Br, I) represents a distorted two-layer hcp of halogen atoms arranged along the SWCNT. The EXAFS and the high angle angular dark field (HAADF) HRTEM data indicate that Cu is partially coordinated by C. According to the optical absorption, valence band photoemission spectroscopy and work function measurements, a Fermi level (FL) downshift as compared with the initial value for the nanotubes and a corresponding charge transfer from the nanotubes to the 1D crystals is observed for CuX@SWCNT nanostructures. The FL shift increases in the sequence CuI<CuBr<CuCl due to an increase of the electron affinity for the halogen atoms. The XPS data confirm the acceptor effect of copper halides and indicate that metallic and semiconducting nanotubes behave differently. Raman spectroscopy performed under electrochemical charging allowed estimation of the value of charge transfer between the nanotube walls and the intercalated 1D crystal. The X-ray absorption and emission spectra for carbon and copper thresholds revealed a new energy level composed of the carbon 2рz and copper 3d-orbitals. This indicates the Cu–C bonding, which in line with the structural HAADF HRTEM and EXAFS data. |
| Author | Zubavichus, Y.V. Kleimenov, E. Kiselev, N.A. Generalov, A.V. Eliseev, A.A. Chernysheva, M.V. Vinogradov, A.S. Kharlamova, M.V. Yashina, L.V. Verbitskiy, N.I. Lukashin, A.V. Kumskov, A.S. Freitag, B. Brzhezinskaya, M.M. Nachtegaal, M. |
| Author_xml | – sequence: 1 givenname: A.A. surname: Eliseev fullname: Eliseev, A.A. organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 2 givenname: L.V. surname: Yashina fullname: Yashina, L.V. organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 3 givenname: N.I. surname: Verbitskiy fullname: Verbitskiy, N.I. email: dr.haider.est@gmail.com organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 4 givenname: M.M. surname: Brzhezinskaya fullname: Brzhezinskaya, M.M. organization: Helmholtz Zentrum Berlin, Albert-Einstein Strasse 15, 12489 Berlin, Germany – sequence: 5 givenname: M.V. surname: Kharlamova fullname: Kharlamova, M.V. organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 6 givenname: M.V. surname: Chernysheva fullname: Chernysheva, M.V. organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 7 givenname: A.V. surname: Lukashin fullname: Lukashin, A.V. organization: Department of Materials Science, Moscow State University, Leninskie gory 1/3, 119991 Moscow, Russia – sequence: 8 givenname: N.A. surname: Kiselev fullname: Kiselev, N.A. organization: Institute of Crystallography RAS, 119333 Moscow, Russia – sequence: 9 givenname: A.S. surname: Kumskov fullname: Kumskov, A.S. organization: Institute of Crystallography RAS, 119333 Moscow, Russia – sequence: 10 givenname: B. surname: Freitag fullname: Freitag, B. organization: FEI Company, 5651 Eindhoven, The Netherlands – sequence: 11 givenname: A.V. surname: Generalov fullname: Generalov, A.V. organization: V.A. Fock Institute of Physics, St. Petersburg State University, 198504 St. Petersburg, Russia – sequence: 12 givenname: A.S. surname: Vinogradov fullname: Vinogradov, A.S. organization: V.A. Fock Institute of Physics, St. Petersburg State University, 198504 St. Petersburg, Russia – sequence: 13 givenname: Y.V. surname: Zubavichus fullname: Zubavichus, Y.V. organization: RRC Kurchatov Institute, 123182 Moscow, Russia – sequence: 14 givenname: E. surname: Kleimenov fullname: Kleimenov, E. organization: SLS, Paul Scherrer Institut, 5232 Villigen PSI, Switzerland – sequence: 15 givenname: M. surname: Nachtegaal fullname: Nachtegaal, M. organization: SLS, Paul Scherrer Institut, 5232 Villigen PSI, Switzerland |
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