Degradation of tetracycline hydrochloride (TCH) by active photocatalyst rich in oxygen vacancies: Performance, transformation product and mechanism

[Display omitted] •Oxygen vacancies (OVs) occurred on the photocatalyst surface during solvent removing.•The hierarchical 3D BiOBr microspheres were obtained by solvothermal reaction.•Rich reactive oxygen species were produced by OVs under sunlight irradiation.•TCH can be effectively degraded and it...

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Published inApplied surface science Vol. 589; p. 152902
Main Authors Wang, Liwei, Hu, Anjie, Liu, Hongjie, Yu, Kefu, Wang, Shaopeng, Deng, Xianwang, Huang, Dahua
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.07.2022
Subjects
BiOBr microsphere
Oxygen vacancy
Photodegradation
Self-assembly
Solvent coordination
Tetracycline hydrochloride
BiOBr microsphere
Photodegradation
Self-assembly
Tetracycline hydrochloride
Oxygen vacancy
Solvent coordination
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Abstract [Display omitted] •Oxygen vacancies (OVs) occurred on the photocatalyst surface during solvent removing.•The hierarchical 3D BiOBr microspheres were obtained by solvothermal reaction.•Rich reactive oxygen species were produced by OVs under sunlight irradiation.•TCH can be effectively degraded and its degradation mechanism is rationally raised. Regulation of oxygen defects, in addition to the adjustment of spatial arrangement and bandgap in the materials can effectively improve the materials’ photocatalytic performance. Bismuth oxybromide (BiOBr) are widely used in the field of photocatalysis because of its abundant active sites and the regulable surface area. Herein, a novel introducing oxygen vacancies (OVs) strategy was developed to synthesize hierarchical 3D BiOBr microsphere constructed by nanopetals, and a serious of tests were used to characterize and quantify OVs. Moreover, the applications of BiOBr with different concentrations of OVs in water antibiotic pollution was discussed, and specific effect of OVs on the photocatalytic performance was also analyzed simply. Benefiting from its rich OVs, the UV–vis light-driving tetracycline hydrochloride degradation efficiency increased to 86.8% within 20 min irradiation. Hence, this work provides theoretical guidance for the regulation of OVs, and the prospect of photocatalyst containing OVs in the photocatalytic field were suggested.
AbstractList [Display omitted] •Oxygen vacancies (OVs) occurred on the photocatalyst surface during solvent removing.•The hierarchical 3D BiOBr microspheres were obtained by solvothermal reaction.•Rich reactive oxygen species were produced by OVs under sunlight irradiation.•TCH can be effectively degraded and its degradation mechanism is rationally raised. Regulation of oxygen defects, in addition to the adjustment of spatial arrangement and bandgap in the materials can effectively improve the materials’ photocatalytic performance. Bismuth oxybromide (BiOBr) are widely used in the field of photocatalysis because of its abundant active sites and the regulable surface area. Herein, a novel introducing oxygen vacancies (OVs) strategy was developed to synthesize hierarchical 3D BiOBr microsphere constructed by nanopetals, and a serious of tests were used to characterize and quantify OVs. Moreover, the applications of BiOBr with different concentrations of OVs in water antibiotic pollution was discussed, and specific effect of OVs on the photocatalytic performance was also analyzed simply. Benefiting from its rich OVs, the UV–vis light-driving tetracycline hydrochloride degradation efficiency increased to 86.8% within 20 min irradiation. Hence, this work provides theoretical guidance for the regulation of OVs, and the prospect of photocatalyst containing OVs in the photocatalytic field were suggested.
ArticleNumber 152902
Author Wang, Shaopeng
Yu, Kefu
Hu, Anjie
Liu, Hongjie
Wang, Liwei
Huang, Dahua
Deng, Xianwang
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Keywords BiOBr microsphere
Photodegradation
Self-assembly
Tetracycline hydrochloride
Oxygen vacancy
Solvent coordination
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Snippet [Display omitted] •Oxygen vacancies (OVs) occurred on the photocatalyst surface during solvent removing.•The hierarchical 3D BiOBr microspheres were obtained...
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StartPage 152902
SubjectTerms BiOBr microsphere
Oxygen vacancy
Photodegradation
Self-assembly
Solvent coordination
Tetracycline hydrochloride
Title Degradation of tetracycline hydrochloride (TCH) by active photocatalyst rich in oxygen vacancies: Performance, transformation product and mechanism
URI https://dx.doi.org/10.1016/j.apsusc.2022.152902
Volume 589
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