Microwave and spark plasma sintering of carbon nanotube and graphene reinforced aluminum matrix composite

Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma sintering (SPS), microwave (MW) and conventional techniques. The initial compositions of Al-1wt% CNT, Al-1wt% GNP and Al-1wt% CNT–1wt% GNP wer...

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Published inArchives of Civil and Mechanical Engineering Vol. 18; no. 4; pp. 1042 - 1054
Main Authors Ghasali, Ehsan, Sangpour, Parvaneh, Jam, Alireza, Rajaei, Hosein, Shirvanimoghaddam, Kamyar, Ebadzadeh, Touradj
Format Journal Article
LanguageEnglish
Published London Elsevier B.V 01.09.2018
Springer London
Springer Nature B.V
Subjects
Online AccessGet full text
ISSN1644-9665
2083-3318
DOI10.1016/j.acme.2018.02.006

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Abstract Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma sintering (SPS), microwave (MW) and conventional techniques. The initial compositions of Al-1wt% CNT, Al-1wt% GNP and Al-1wt% CNT–1wt% GNP were mixed by a high energy ultrasonic device and mixer mill to achieve homogenous dispersion. The SPS, MW and conventional processes were conducted at almost 450, 600 and 700°C, respectively. The maximum relative density (99.7±0.2% of theoretical density) and bending strength (337±11MPa) obtained by SPS, while maximum microhardness of 221±11 Vickers achieved by microwave for Al-1wt% CNT–1wt% GNP hybrid composite. X-ray diffraction (XRD) examinations identified Al as the only dominant phase accompanied by very low intensity peaks of Al4C3. Field emission scanning electron microscopy (FESEM) micrographs demonstrated uniform distribution of GNP as well as CNT reinforcement in spark plasma sintered samples.
AbstractList Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma sintering (SPS), microwave (MW) and conventional techniques. The initial compositions of Al-1 wt% CNT, Al-1 wt% GNP and Al-1 wt% CNT-1 wt% GNP were mixed by a high energy ultrasonic device and mixer mill to achieve homogenous dispersion. The SPS, MW and conventional processes were conducted at almost 450, 600 and 700 °C, respectively. The maximum relative density (99.7 ± 0.2% of theoretical density) and bending strength (337 ± 11 MPa) obtained by SPS, while maximum microhardness of 221 ± 11 Vickers achieved by microwave for Al-1 wt% CNT-1 wt% GNP hybrid composite. X-ray diffraction (XRD) examinations identified Al as the only dominant phase accompanied by very low intensity peaks of Al4C3. Field emission scanning electron microscopy (FESEM) micrographs demonstrated uniform distribution of GNP as well as CNT reinforcement in spark plasma sintered samples.
Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma sintering (SPS), microwave (MW) and conventional techniques. The initial compositions of Al-1 wt% CNT, Al-1 wt% GNP and Al-1 wt% CNT-1 wt% GNP were mixed by a high energy ultrasonic device and mixer mill to achieve homogenous dispersion. The SPS, MW and conventional processes were conducted at almost 450, 600 and 700 °C, respectively. The maximum relative density (99.7 ± 0.2% of theoretical density) and bending strength (337 ± 11 MPa) obtained by SPS, while maximum microhardness of 221 ± 11 Vickers achieved by microwave for Al-1 wt% CNT-1 wt% GNP hybrid composite. X-ray diffraction (XRD) examinations identified Al as the only dominant phase accompanied by very low intensity peaks of Al 4 C 3 . Field emission scanning electron microscopy (FESEM) micrographs demonstrated uniform distribution of GNP as well as CNT reinforcement in spark plasma sintered samples.
Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma sintering (SPS), microwave (MW) and conventional techniques. The initial compositions of Al-1wt% CNT, Al-1wt% GNP and Al-1wt% CNT–1wt% GNP were mixed by a high energy ultrasonic device and mixer mill to achieve homogenous dispersion. The SPS, MW and conventional processes were conducted at almost 450, 600 and 700°C, respectively. The maximum relative density (99.7±0.2% of theoretical density) and bending strength (337±11MPa) obtained by SPS, while maximum microhardness of 221±11 Vickers achieved by microwave for Al-1wt% CNT–1wt% GNP hybrid composite. X-ray diffraction (XRD) examinations identified Al as the only dominant phase accompanied by very low intensity peaks of Al4C3. Field emission scanning electron microscopy (FESEM) micrographs demonstrated uniform distribution of GNP as well as CNT reinforcement in spark plasma sintered samples.
Author Jam, Alireza
Ghasali, Ehsan
Shirvanimoghaddam, Kamyar
Sangpour, Parvaneh
Rajaei, Hosein
Ebadzadeh, Touradj
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  givenname: Parvaneh
  surname: Sangpour
  fullname: Sangpour, Parvaneh
  organization: Ceramic Department, Materials and Energy Research Center, Alborz, Iran
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  fullname: Jam, Alireza
  organization: Ceramic Department, Materials and Energy Research Center, Alborz, Iran
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  surname: Ebadzadeh
  fullname: Ebadzadeh, Touradj
  organization: Ceramic Department, Materials and Energy Research Center, Alborz, Iran
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Microwave
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Snippet Graphene and carbon nanotube due to their outstanding mechanical performance were used as reinforcement in aluminum (Al) based composite through spark plasma...
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SubjectTerms Aluminum
Aluminum base alloys
Aluminum carbide
Aluminum matrix composites
Bend strength
Carbon nanotube
Carbon nanotubes
Civil Engineering
Engineering
Field emission microscopy
Graphene
Hybrid composites
Mechanical Engineering
Mechanical properties
Microwave
Original Research Article
Photomicrographs
Plasma sintering
Spark plasma sintering
Specific gravity
Structural Materials
Theoretical density
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Title Microwave and spark plasma sintering of carbon nanotube and graphene reinforced aluminum matrix composite
URI https://dx.doi.org/10.1016/j.acme.2018.02.006
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