Surface modification of FO membrane for improving ammoniacal nitrogen (NH4+-N) rejection: Investigating the factors influencing NH4+-N rejection
Forward osmosis (FO) has attracted attention for wastewater treatment owing to its energy-saving characteristics; however, the low rejection of ammoniacal nitrogen (NH4+-N) for normal polyamide thin-film composite (TFC) FO membranes limits their practical applications for NH4+-N recovery or concentr...
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Published in | Journal of membrane science Vol. 650; p. 120429 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
15.05.2022
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Abstract | Forward osmosis (FO) has attracted attention for wastewater treatment owing to its energy-saving characteristics; however, the low rejection of ammoniacal nitrogen (NH4+-N) for normal polyamide thin-film composite (TFC) FO membranes limits their practical applications for NH4+-N recovery or concentration from wastewater. Herein, ethylenediamine (EDA)- and 2-aminoethanol (AEA)-grafted TFC FO membranes were prepared to improve the NH4+-N rejection. EDA and AEA have similar molecular structures; however, their end groups differ. EDA has two primary amino groups, whereas AEA has one amino group and one hydroxy group. Both EDA- and AEA-grafted FO membranes significantly improved the NH4+-N rejection, and a further increase in NH4+-N rejection was noted (up to 97.5%) with increasing grafting times. These membranes showed high rejection, even at a feed solution with higher pH of 7.6 (89.7% and 83.0% for EDA- and AEA-grafted membranes, respectively). The carboxylic group density of the pristine and grafted membranes was measured to investigate the factors influencing the improvement in NH4+-N rejection. A significant correlation was found between the carboxylic group density and NH4+-N rejection, while the correlation between the surface zeta potential and NH4+-N rejection was unclear. This means not only positive charge chemical grafting can improve the NH4+-N rejection, but also the neutral chemical grafting can improve the NH4+-N rejection. It also indicates that reducing membrane surface carboxylic group density could alleviate cation exchange during FO process. This study clarified the factors influencing NH4+-N rejection and provided a novel idea for designing a FO membrane with high NH4+-N selectivity suitable for ammoniacal nitrogen concentration from wastewater.
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•High NH4+-N rejection TFC FO membrane was developed by grating EDA or AEA.•Membrane surface -COO- density was controlled via multiple times catalytic reaction.•A significant correlation between NH4+-N rejection and surface carboxylic group density was revealed.•Surface carboxylic group density is the decisive factor for NH4+-N rejection. |
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AbstractList | Forward osmosis (FO) has attracted attention for wastewater treatment owing to its energy-saving characteristics; however, the low rejection of ammoniacal nitrogen (NH4+-N) for normal polyamide thin-film composite (TFC) FO membranes limits their practical applications for NH4+-N recovery or concentration from wastewater. Herein, ethylenediamine (EDA)- and 2-aminoethanol (AEA)-grafted TFC FO membranes were prepared to improve the NH4+-N rejection. EDA and AEA have similar molecular structures; however, their end groups differ. EDA has two primary amino groups, whereas AEA has one amino group and one hydroxy group. Both EDA- and AEA-grafted FO membranes significantly improved the NH4+-N rejection, and a further increase in NH4+-N rejection was noted (up to 97.5%) with increasing grafting times. These membranes showed high rejection, even at a feed solution with higher pH of 7.6 (89.7% and 83.0% for EDA- and AEA-grafted membranes, respectively). The carboxylic group density of the pristine and grafted membranes was measured to investigate the factors influencing the improvement in NH4+-N rejection. A significant correlation was found between the carboxylic group density and NH4+-N rejection, while the correlation between the surface zeta potential and NH4+-N rejection was unclear. This means not only positive charge chemical grafting can improve the NH4+-N rejection, but also the neutral chemical grafting can improve the NH4+-N rejection. It also indicates that reducing membrane surface carboxylic group density could alleviate cation exchange during FO process. This study clarified the factors influencing NH4+-N rejection and provided a novel idea for designing a FO membrane with high NH4+-N selectivity suitable for ammoniacal nitrogen concentration from wastewater.
[Display omitted]
•High NH4+-N rejection TFC FO membrane was developed by grating EDA or AEA.•Membrane surface -COO- density was controlled via multiple times catalytic reaction.•A significant correlation between NH4+-N rejection and surface carboxylic group density was revealed.•Surface carboxylic group density is the decisive factor for NH4+-N rejection. |
ArticleNumber | 120429 |
Author | Matsuyama, Hideto Sasaki, Yuji Shen, Qin Shintani, Takuji Yao, Xuesong Gonzales, Ralph Rolly Zhang, Pengfei Nakagawa, Keizo Lin, Yuqing |
Author_xml | – sequence: 1 givenname: Xuesong surname: Yao fullname: Yao, Xuesong organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 2 givenname: Ralph Rolly surname: Gonzales fullname: Gonzales, Ralph Rolly organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 3 givenname: Yuji surname: Sasaki fullname: Sasaki, Yuji organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 4 givenname: Yuqing surname: Lin fullname: Lin, Yuqing organization: School of Resources and Environmental Engineering, East China University of Science and Technology, Shanghai, 200237, China – sequence: 5 givenname: Qin surname: Shen fullname: Shen, Qin organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 6 givenname: Pengfei surname: Zhang fullname: Zhang, Pengfei organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 7 givenname: Takuji orcidid: 0000-0002-8109-9932 surname: Shintani fullname: Shintani, Takuji organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 8 givenname: Keizo orcidid: 0000-0002-5323-0462 surname: Nakagawa fullname: Nakagawa, Keizo organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan – sequence: 9 givenname: Hideto orcidid: 0000-0003-2468-4905 surname: Matsuyama fullname: Matsuyama, Hideto email: matuyama@kobe-u.ac.jp organization: Research Center for Membrane and Film Technology, Kobe University, 1-1 Rokkodai, Nada, Kobe, 657-8501, Japan |
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Keywords | Thin-film composite membrane Forward osmosis Surface grafting Carboxylic group density Ammoniacal nitrogen concentration |
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Snippet | Forward osmosis (FO) has attracted attention for wastewater treatment owing to its energy-saving characteristics; however, the low rejection of ammoniacal... |
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SubjectTerms | Ammoniacal nitrogen concentration Carboxylic group density Forward osmosis Surface grafting Thin-film composite membrane |
Title | Surface modification of FO membrane for improving ammoniacal nitrogen (NH4+-N) rejection: Investigating the factors influencing NH4+-N rejection |
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