Characterization of Fe2O3 thin film on highly oriented pyrolytic graphite by AFM, Ellipsometry and XPS
Graphite finds use in a large amount of nanoscale applications, including as a substrate for thin film and nanomaterial deposition. With its excellent properties for usage in nanoscale and given the regularity of structure of highly oriented pyrolytic graphite (HOPG), the possibility of use to acqui...
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| Published in | Applied surface science Vol. 493; pp. 673 - 678 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.11.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Graphite finds use in a large amount of nanoscale applications, including as a substrate for thin film and nanomaterial deposition. With its excellent properties for usage in nanoscale and given the regularity of structure of highly oriented pyrolytic graphite (HOPG), the possibility of use to acquire more precise and detailed results is high. To this end the basic topographical and structural properties of HOPG and thin Fe2O3 have been explored. Methods used were atomic force microscopy, ellipsometry and x-ray photoelectron spectroscopy. Documentation of the results allows for further examination of HOPG usage possibilities, uncoated or coated with Fe2O3 thin film, as well as a substrate for carbon fiber or nanotube growth in future projects.
•Fe2O3 layer is of even thickness over the whole sample due to regularity of HOPG surface.•Fe2O3 forms shortly after exposure to atmospheric oxygen.•Changes in XPS, AFM and Ellipsometry results between clean HOPG and one with Fe2O3 layer clearly visible•Rare artifacts on the surface can cause the appearance of unexpected chemical bonds.•Material provides good starting point for nanomaterial research. |
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| AbstractList | Graphite finds use in a large amount of nanoscale applications, including as a substrate for thin film and nanomaterial deposition. With its excellent properties for usage in nanoscale and given the regularity of structure of highly oriented pyrolytic graphite (HOPG), the possibility of use to acquire more precise and detailed results is high. To this end the basic topographical and structural properties of HOPG and thin Fe2O3 have been explored. Methods used were atomic force microscopy, ellipsometry and x-ray photoelectron spectroscopy. Documentation of the results allows for further examination of HOPG usage possibilities, uncoated or coated with Fe2O3 thin film, as well as a substrate for carbon fiber or nanotube growth in future projects.
•Fe2O3 layer is of even thickness over the whole sample due to regularity of HOPG surface.•Fe2O3 forms shortly after exposure to atmospheric oxygen.•Changes in XPS, AFM and Ellipsometry results between clean HOPG and one with Fe2O3 layer clearly visible•Rare artifacts on the surface can cause the appearance of unexpected chemical bonds.•Material provides good starting point for nanomaterial research. |
| Author | Kaspar, Pavel Ramazanov, Shikhgasan Dallaev, Rashid Sobola, Dinara Nebojsa, Alois Rezaee, Sahar Grmela, Lubomír |
| Author_xml | – sequence: 1 givenname: Pavel orcidid: 0000-0003-1757-2382 surname: Kaspar fullname: Kaspar, Pavel email: kasparp@feec.vutbr.cz organization: Department of Physics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Technická 2848/8, 616 00 Brno, Czech Republic – sequence: 2 givenname: Dinara surname: Sobola fullname: Sobola, Dinara organization: Department of Physics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Technická 2848/8, 616 00 Brno, Czech Republic – sequence: 3 givenname: Rashid surname: Dallaev fullname: Dallaev, Rashid organization: Department of Physics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Technická 2848/8, 616 00 Brno, Czech Republic – sequence: 4 givenname: Shikhgasan surname: Ramazanov fullname: Ramazanov, Shikhgasan organization: Faculty of Physics, Dagestan State University, 367015 Makhachkala, st. M. Gadjieva 43-a, Dagestan Republic, Russia – sequence: 5 givenname: Alois surname: Nebojsa fullname: Nebojsa, Alois organization: Central European Institute of Technology BUT, Purkyňova 123, 612 00 Brno, Czech Republic – sequence: 6 givenname: Sahar orcidid: 0000-0001-5034-0810 surname: Rezaee fullname: Rezaee, Sahar organization: Department of Physics, Kermanshah Branch, Islamic Azad University, Kermanshah, Iran – sequence: 7 givenname: Lubomír surname: Grmela fullname: Grmela, Lubomír organization: Department of Physics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Technická 2848/8, 616 00 Brno, Czech Republic |
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| Title | Characterization of Fe2O3 thin film on highly oriented pyrolytic graphite by AFM, Ellipsometry and XPS |
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