Simultaneous extraction of oil and tea saponin from Camellia oleifera Abel. seeds under subcritical water conditions
Camellia oleifera Abel. (Camellia oleifera) seeds oil and tea saponin were simultaneously extracted under subcritical water extraction (SWE) conditions. A response surface methodology (RSM) was used for optimizing the SWE process by varying independent variables temperature (×1: 110–150 °C), extract...
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| Published in | Fuel processing technology Vol. 174; pp. 88 - 94 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.06.2018
Elsevier Science Ltd |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Camellia oleifera Abel. (Camellia oleifera) seeds oil and tea saponin were simultaneously extracted under subcritical water extraction (SWE) conditions. A response surface methodology (RSM) was used for optimizing the SWE process by varying independent variables temperature (×1: 110–150 °C), extraction time (×2: 20–40 min) and solvent to material ratios (×3: 5:1–15:1 mL/g). The highest extraction yield of oil is 94.07% at the condition of 133.59 °C, 32.03 min, 10.79 mL/g with the tea saponin yield 71.38%, and the highest extraction yield of tea saponin is 74.21% with the oil yield 91.27% of the total content at the condition of 121.11 °C, 32.07 min, 8.33 mL/g. Analytical results showed that extracted oil has a similar fatty acid profile and quality as those of the cold Soxhlet extraction(SE) oils, and the oils extracted by SWE were even more resistant to lipid oxidation and more abundant valuable bioactive compounds than those of the cold-pressed(CP) oils.
Treatment procedure of Camellia oleifera Abel. seeds with SWE. [Display omitted]
•Simultaneous extraction of oil and tea saponin from Camellia oleosa seeds by SWE•Optimization of the subcritical water extraction process by RSM.•Oil extraction yield of 94.07% and tea saponin yield of is 74.21% at optimal conditions•Similar fatty acid profiles and better anti-oxidation stability of the oil obtained by SWE |
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| AbstractList | Camellia oleifera Abel. (Camellia oleifera) seeds oil and tea saponin were simultaneously extracted under subcritical water extraction (SWE) conditions. A response surface methodology (RSM) was used for optimizing the SWE process by varying independent variables temperature (×1: 110–150 °C), extraction time (×2: 20–40 min) and solvent to material ratios (×3: 5:1–15:1 mL/g). The highest extraction yield of oil is 94.07% at the condition of 133.59 °C, 32.03 min, 10.79 mL/g with the tea saponin yield 71.38%, and the highest extraction yield of tea saponin is 74.21% with the oil yield 91.27% of the total content at the condition of 121.11 °C, 32.07 min, 8.33 mL/g. Analytical results showed that extracted oil has a similar fatty acid profile and quality as those of the cold Soxhlet extraction(SE) oils, and the oils extracted by SWE were even more resistant to lipid oxidation and more abundant valuable bioactive compounds than those of the cold-pressed(CP) oils. Camellia oleifera Abel. (Camellia oleifera) seeds oil and tea saponin were simultaneously extracted under subcritical water extraction (SWE) conditions. A response surface methodology (RSM) was used for optimizing the SWE process by varying independent variables temperature (×1: 110–150 °C), extraction time (×2: 20–40 min) and solvent to material ratios (×3: 5:1–15:1 mL/g). The highest extraction yield of oil is 94.07% at the condition of 133.59 °C, 32.03 min, 10.79 mL/g with the tea saponin yield 71.38%, and the highest extraction yield of tea saponin is 74.21% with the oil yield 91.27% of the total content at the condition of 121.11 °C, 32.07 min, 8.33 mL/g. Analytical results showed that extracted oil has a similar fatty acid profile and quality as those of the cold Soxhlet extraction(SE) oils, and the oils extracted by SWE were even more resistant to lipid oxidation and more abundant valuable bioactive compounds than those of the cold-pressed(CP) oils. Treatment procedure of Camellia oleifera Abel. seeds with SWE. [Display omitted] •Simultaneous extraction of oil and tea saponin from Camellia oleosa seeds by SWE•Optimization of the subcritical water extraction process by RSM.•Oil extraction yield of 94.07% and tea saponin yield of is 74.21% at optimal conditions•Similar fatty acid profiles and better anti-oxidation stability of the oil obtained by SWE |
| Author | Li, Changzhu Liu, Rukuan Li, Zhenmei Ma, Li Li, Jilie Xiao, Zhihong Wu, Hong Deng, Shuguang Zhang, Aihua |
| Author_xml | – sequence: 1 givenname: Hong surname: Wu fullname: Wu, Hong organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 2 givenname: Changzhu surname: Li fullname: Li, Changzhu organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 3 givenname: Zhenmei surname: Li fullname: Li, Zhenmei organization: Key Laboratory of Cultivation and Protection Co-constructed for Non-wood Forest Trees, Ministry of Education, Central South University of Forestry and Technology, Changsha 410004, China – sequence: 4 givenname: Rukuan surname: Liu fullname: Liu, Rukuan organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 5 givenname: Aihua surname: Zhang fullname: Zhang, Aihua organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 6 givenname: Zhihong surname: Xiao fullname: Xiao, Zhihong email: xzhh1015@163.com organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 7 givenname: Li surname: Ma fullname: Ma, Li organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China – sequence: 8 givenname: Jilie surname: Li fullname: Li, Jilie organization: Key Laboratory of Cultivation and Protection Co-constructed for Non-wood Forest Trees, Ministry of Education, Central South University of Forestry and Technology, Changsha 410004, China – sequence: 9 givenname: Shuguang surname: Deng fullname: Deng, Shuguang email: shuguang.deng@asu.edu organization: National Engineering Research Center for Oil-tea Camellia, Hunan Academy of Forestry, Changsha 410004, Hunan, China |
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| Keywords | Camellia oleifera Simultaneous extraction Oil properties Subcritical water extraction Tea saponin |
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| SubjectTerms | Camellia oleifera Cold pressing Independent variables Oil Oil properties Oxidation Oxidation resistance Response surface methodology Seeds Simultaneous extraction Studies Subcritical water extraction Tea saponin |
| Title | Simultaneous extraction of oil and tea saponin from Camellia oleifera Abel. seeds under subcritical water conditions |
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