Dynamic mechanical and ultrasonic properties of polyurea
► We present the storage and loss moduli of polyurea at various temperatures and frequencies. ► The master curves of the moduli are derived. ► The relaxation spectra are calculated by means of two approximate models. ► The ultrasonic wave propagation is tested at low temperatures and high frequencie...
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Published in | Mechanics of materials Vol. 43; no. 10; pp. 598 - 607 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.10.2011
Elsevier |
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Abstract | ► We present the storage and loss moduli of polyurea at various temperatures and frequencies. ► The master curves of the moduli are derived. ► The relaxation spectra are calculated by means of two approximate models. ► The ultrasonic wave propagation is tested at low temperatures and high frequencies. ► The two sets of results are compared using time–temperature superposition principle.
Dynamic mechanical analysis (DMA) and ultrasonic measurements were carried out to study the temperature and frequency dependences of viscoelastic properties of polyurea. Master curves of Young’s storage and loss moduli were developed from the DMA data. Relaxation spectra were subsequently calculated by means of two approximate models, and the apparent activation energy of molecular rearrangements was also determined based on the temperature dependence of the time–temperature shift factor. Velocity and attenuation of longitudinal and shear ultrasonic waves in polyurea were measured in the 0.5–2
MHz frequency range between −60 and 30
°C temperatures. The complex longitudinal and shear moduli were computed from these measurements. Combining these results provided an estimate of the complex bulk and Young’s moduli at high frequencies. The results of the DMA and temperature and frequency shifted ultrasonic measurements are compared and similarities and deviations are discussed. |
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AbstractList | ► We present the storage and loss moduli of polyurea at various temperatures and frequencies. ► The master curves of the moduli are derived. ► The relaxation spectra are calculated by means of two approximate models. ► The ultrasonic wave propagation is tested at low temperatures and high frequencies. ► The two sets of results are compared using time–temperature superposition principle.
Dynamic mechanical analysis (DMA) and ultrasonic measurements were carried out to study the temperature and frequency dependences of viscoelastic properties of polyurea. Master curves of Young’s storage and loss moduli were developed from the DMA data. Relaxation spectra were subsequently calculated by means of two approximate models, and the apparent activation energy of molecular rearrangements was also determined based on the temperature dependence of the time–temperature shift factor. Velocity and attenuation of longitudinal and shear ultrasonic waves in polyurea were measured in the 0.5–2
MHz frequency range between −60 and 30
°C temperatures. The complex longitudinal and shear moduli were computed from these measurements. Combining these results provided an estimate of the complex bulk and Young’s moduli at high frequencies. The results of the DMA and temperature and frequency shifted ultrasonic measurements are compared and similarities and deviations are discussed. Dynamic mechanical analysis (DMA) and ultrasonic measurements were carried out to study the temperature and frequency dependences of viscoelastic properties of polyurea. Master curves of Young's storage and loss moduli were developed from the DMA data. Relaxation spectra were subsequently calculated by means of two approximate models, and the apparent activation energy of molecular rearrangements was also determined based on the temperature dependence of the time-temperature shift factor. Velocity and attenuation of longitudinal and shear ultrasonic waves in polyurea were measured in the 0.5-2MHz frequency range between -60 and 30 degree C temperatures. The complex longitudinal and shear moduli were computed from these measurements. Combining these results provided an estimate of the complex bulk and Young's moduli at high frequencies. The results of the DMA and temperature and frequency shifted ultrasonic measurements are compared and similarities and deviations are discussed. |
Author | Amirkhizi, Alireza V. Schaaf, Kristin Wu, Gaohui Qiao, Jing Nemat-Nasser, Sia |
Author_xml | – sequence: 1 givenname: Jing surname: Qiao fullname: Qiao, Jing email: jingqiao.hit@gmail.com organization: School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China – sequence: 2 givenname: Alireza V. surname: Amirkhizi fullname: Amirkhizi, Alireza V. organization: Mechanical and Aerospace Engineering, Center of Excellence for Advanced Materials, University of California, San Diego, CA 92093, USA – sequence: 3 givenname: Kristin surname: Schaaf fullname: Schaaf, Kristin organization: Mechanical and Aerospace Engineering, Center of Excellence for Advanced Materials, University of California, San Diego, CA 92093, USA – sequence: 4 givenname: Sia surname: Nemat-Nasser fullname: Nemat-Nasser, Sia organization: Mechanical and Aerospace Engineering, Center of Excellence for Advanced Materials, University of California, San Diego, CA 92093, USA – sequence: 5 givenname: Gaohui surname: Wu fullname: Wu, Gaohui organization: School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China |
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Keywords | Polyurea Mechanical properties Time–temperature superposition Viscoelasticity Master equation Elastic modulus Frequency dependence Shear modulus Urea polymer Time-temperature superposition Dynamic mechanical analysis Time dependence Strain wave Activation energy Ultrasonic method |
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Snippet | ► We present the storage and loss moduli of polyurea at various temperatures and frequencies. ► The master curves of the moduli are derived. ► The relaxation... Dynamic mechanical analysis (DMA) and ultrasonic measurements were carried out to study the temperature and frequency dependences of viscoelastic properties of... |
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SubjectTerms | Applied sciences Deviation Dynamic mechanical properties Dynamics Exact sciences and technology Mathematical models Mechanical analysis Mechanical properties Physical properties Polymer industry, paints, wood Polyurea Polyureas Properties and testing Shear Technology of polymers Temperature dependence Time–temperature superposition |
Title | Dynamic mechanical and ultrasonic properties of polyurea |
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