Aromatic homopolymers obtained by precipitation polycondensation: 1. Synthesis of naphthalene-containing polyketones
High molecular weight film-forming semicrystalline aromatic polyketones with a regular structure were obtained by precipitation electrophilic Friedel-Crafts polycondensation of 2,6-naphthalenedicarboxylic acid chloride with diphenyl ether, 1,4-bis( p-phenoxy) benzophenone and 1,4-bis( p-phenoxybenzo...
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| Published in | Polymer (Guilford) Vol. 36; no. 18; pp. 3575 - 3583 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
1995
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| Subjects | |
| Online Access | Get full text |
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| Abstract | High molecular weight film-forming semicrystalline aromatic polyketones with a regular structure were obtained by precipitation electrophilic Friedel-Crafts polycondensation of 2,6-naphthalenedicarboxylic acid chloride with diphenyl ether, 1,4-bis(
p-phenoxy) benzophenone and 1,4-bis(
p-phenoxybenzoyl) benzene. Using
1H and
13C n.m.r. spectroscopy, the polyketones obtained were shown to be linear with
para-substituted arylene fragments in the main chain. These polymers are soluble in strong protic acids and in common organic solvents, such as dichloroacetic acid and CHCl
3/CF
3CO
2H mixtures. Depending on the chemical structure, these ‘as-made’ polyketones were found to show multiple melting behaviour on heating. |
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| AbstractList | High molecular weight film-forming semicrystalline aromatic polyketones with a regular structure were obtained by precipitation electrophilic Friedel-Crafts polycondensation of 2,6-naphthalenedicarboxylic acid chloride with diphenyl ether, 1,4-bis(
p-phenoxy) benzophenone and 1,4-bis(
p-phenoxybenzoyl) benzene. Using
1H and
13C n.m.r. spectroscopy, the polyketones obtained were shown to be linear with
para-substituted arylene fragments in the main chain. These polymers are soluble in strong protic acids and in common organic solvents, such as dichloroacetic acid and CHCl
3/CF
3CO
2H mixtures. Depending on the chemical structure, these ‘as-made’ polyketones were found to show multiple melting behaviour on heating. |
| Author | Gileva, N.G. Villers, D. Zolotukhin, M.G. Fougnies, C. Fatykhov, A.A. Dosière, M. |
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| Keywords | synthesis poly(aryl ether ketone)s precipitation polycondensation |
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| Title | Aromatic homopolymers obtained by precipitation polycondensation: 1. Synthesis of naphthalene-containing polyketones |
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