Influences of cerium on structure and catalytic performance of n-heptane hydroisomerization of Ni-HPW/MCM-48
By means of X-ray diffraction（XRD）, N2 adsorption-desorption, Fourier transform infrared spectroscopy（FT-IR）, scanning electron microscopy（SEM）, NH3-temperature（NH3-TPD）, Py-infrared（Py-IR） and thermogravimetry-differential scanning calorimetry（TG/DTA） techniques, the influences of Ce on the structu...
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| Published in | Journal of rare earths Vol. 33; no. 1; pp. 46 - 55 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
2015
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(14)60382-3 |
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| Abstract | By means of X-ray diffraction（XRD）, N2 adsorption-desorption, Fourier transform infrared spectroscopy（FT-IR）, scanning electron microscopy（SEM）, NH3-temperature（NH3-TPD）, Py-infrared（Py-IR） and thermogravimetry-differential scanning calorimetry（TG/DTA） techniques, the influences of Ce on the structure, acidity, stability and hydroisomerization performance of Ni-HPW/MCM-48 and Ni-HPW/Ce-MCM-48 catalysts were studied. The results showed that introduction of appropriate content of Ce into MCM-48 could improve the crystallinity, acidity and stability of mesoporous silica. The acidity and stability of the Ni-HPW/Ce-MCM-48 catalyst was also increased. Besides, the catalytic performance of the Ni-HPW/Ce-MCM-48 catalyst for n-heptane hydroisomerization was promoted. The conversion and selectivity of the Ni-HPW/Ce-MCM-48 catalyst reached 41% and 91% respectively at the preparation conditions of 4 wt.% Ni, 20 wt.% HPW, 0.03 Ce/Si molar ratio. |
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| AbstractList | By means of X-ray diffraction（XRD）, N2 adsorption-desorption, Fourier transform infrared spectroscopy（FT-IR）, scanning electron microscopy（SEM）, NH3-temperature（NH3-TPD）, Py-infrared（Py-IR） and thermogravimetry-differential scanning calorimetry（TG/DTA） techniques, the influences of Ce on the structure, acidity, stability and hydroisomerization performance of Ni-HPW/MCM-48 and Ni-HPW/Ce-MCM-48 catalysts were studied. The results showed that introduction of appropriate content of Ce into MCM-48 could improve the crystallinity, acidity and stability of mesoporous silica. The acidity and stability of the Ni-HPW/Ce-MCM-48 catalyst was also increased. Besides, the catalytic performance of the Ni-HPW/Ce-MCM-48 catalyst for n-heptane hydroisomerization was promoted. The conversion and selectivity of the Ni-HPW/Ce-MCM-48 catalyst reached 41% and 91% respectively at the preparation conditions of 4 wt.% Ni, 20 wt.% HPW, 0.03 Ce/Si molar ratio. By means of X-ray diffraction (XRD), N2 adsorption-desorption, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), NH3-temperature (NH3-TPD), Py-infrared (Py-IR) and thermogravimetry-differential scanning calorimetry (TG/DTA) techniques, the influences of Ce on the structure, acidity, stability and hydroisomerization performance of Ni-HPW/MCM-48 and Ni-HPW/Ce-MCM-48 catalysts were studied. The results showed that introduction of appropriate content of Ce into MCM-48 could improve the crystallinity, acidity and stability of mesoporous silica. The acidity and stability of the Ni-HPW/Ce-MCM-48 catalyst was also increased. Besides, the catalytic performance of the Ni-HPW/Ce-MCM-48 catalyst for n-heptane hydroisomerization was promoted. The conversion and selectivity of the Ni-HPW/Ce-MCM-48 catalyst reached 41% and 91% respectively at the preparation conditions of 4 wt.% Ni, 20 wt.% HPW, 0.03 Ce/Si molar ratio. Comparison of catalytic performance of Ni-HPW/MCM-48 (1), Ni-HPW/Ce-MCM-48-0.01 (2), Ni-HPW/Ce-MCM-48-0.03 (3) and Ni-HPW/Ce-MCM-48-0.05 (4) (catalyst 0.2 g, reduction temperature=673 K, reduction time=4 h, reaction temperature=553 K, WHSV=3.52 h−1, n(H2)/n(n-C7)=12) By means of X-ray diffraction (XRD), N sub(2) adsorption-desorption, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), (NH sub(3)-temperature (NH sub(3)-TPD), Py-infrared (Py-IR) and thermogravimetry-differential scanning calorimetry (TG/DTA) techniques, the influences of Ce on the structure, acidity, stability and hydroisomerization performance of Ni-HPW/MCM-48 and Ni-HPW/Ce-MCM-48 catalysts were studied. The results showed that introduction of appropriate content of Ce into MCM-48 could improve the crystallinity, acidity and stability of mesoporous silica. The acidity and stability of the Ni-HPW/Ce-MCM-48 catalyst was also increased. Besides, the catalytic performance of the Ni-FIPW/Ce-MCM-48 catalyst for n-heptane hydroisomerization was promoted. The conversion and selectivity of the Ni-HPW/Ce-MCM-48 catalyst reached 41% and 91% respectively at the preparation conditions of 4 wt.% Ni, 20 wt.% HPW, 0.03 Ce/Si molar ratio. |
| Author | 汪颖军 崔莹雪 所艳华 张微 |
| AuthorAffiliation | College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing 163318, China |
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| Keywords | MCM-48 cerium hydroisomerization n-heptane rare earths |
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| Notes | 11-2788/TF n-heptane; hydroisomerization; MCM-48; cerium; rare earths By means of X-ray diffraction（XRD）, N2 adsorption-desorption, Fourier transform infrared spectroscopy（FT-IR）, scanning electron microscopy（SEM）, NH3-temperature（NH3-TPD）, Py-infrared（Py-IR） and thermogravimetry-differential scanning calorimetry（TG/DTA） techniques, the influences of Ce on the structure, acidity, stability and hydroisomerization performance of Ni-HPW/MCM-48 and Ni-HPW/Ce-MCM-48 catalysts were studied. The results showed that introduction of appropriate content of Ce into MCM-48 could improve the crystallinity, acidity and stability of mesoporous silica. The acidity and stability of the Ni-HPW/Ce-MCM-48 catalyst was also increased. Besides, the catalytic performance of the Ni-HPW/Ce-MCM-48 catalyst for n-heptane hydroisomerization was promoted. The conversion and selectivity of the Ni-HPW/Ce-MCM-48 catalyst reached 41% and 91% respectively at the preparation conditions of 4 wt.% Ni, 20 wt.% HPW, 0.03 Ce/Si molar ratio. WANG Yingjun, CUI Yingxue, SUO Yanhua, ZHANG Wei （College of Chemistry and Chemical Engineering, Northeast Petroleum University, Daqing 163318, China） ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| SubjectTerms | Calorimetry Catalysis Catalysts cerium Diffraction HPW hydroisomerization MCM-48 n-heptane Nickel Rare earth metals rare earths Scanning electron microscopy Stability 傅立叶变换红外光谱 催化剂性能 加氢异构化 扫描电子显微镜 正庚烷 结构 |
| Title | Influences of cerium on structure and catalytic performance of n-heptane hydroisomerization of Ni-HPW/MCM-48 |
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