Surface modification of thin film composite forward osmosis membrane using tris(2-aminoethyl)amine for enhanced ammonium recovery

In this study, we aimed to develop a forward osmosis (FO) thin film composite (TFC) membrane which could retain NH4+ from wastewater. The conventional TFC membrane has a microporous polymer support and a selective layer for salt rejection; however, the polyamide selective layer is known to not be ab...

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Published inDesalination Vol. 541; p. 116002
Main Authors Li, Jing, Gonzales, Ralph Rolly, Takagi, Ryosuke, Yao, Xuesong, Zhang, Pengfei, Istirokhatun, Titik, Zhang, Jinhui, Matsuyama, Hideto
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.11.2022
Subjects
Ammonium recovery
Forward osmosis
Surface modification
Thin-film composite membrane
Tris(2-aminoethyl)amine
Ammonium recovery
Surface modification
Thin-film composite membrane
Forward osmosis
Tris(2-aminoethyl)amine
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Abstract In this study, we aimed to develop a forward osmosis (FO) thin film composite (TFC) membrane which could retain NH4+ from wastewater. The conventional TFC membrane has a microporous polymer support and a selective layer for salt rejection; however, the polyamide selective layer is known to not be able to reject NH4+. Our strategy was to develop tris(2-aminoethyl)amine (TAEA)-modified TFC membranes via secondary interfacial polymerization, and the modification factors were optimized. The NH4+ rejection of the optimized membrane significantly increased from 64.9 % (pristine TFC) to 94.7 %. TAEA modification resulted in a smoother surface and thinner polyamide selective layers. The mechanism of NH4+ rejection during FO operation was investigated and was found to be influenced by membrane surface carboxylic group density and the polyamide crosslinking, cation exchange between the draw and feed solutions, and size sieving. In conclusion, the TAEA-modified membrane showed high selectivity against NH4+ and applicability for NH4+ recovery. In the future, the TAEA-modified membrane may be applied for NH4+ enrichment and recovery from real wastewater systems. [Display omitted] •Thin film composite (TFC) membrane was modified with tris(2-aminoethyl)amine (TAEA).•Secondary interfacial polymerization with TAEA was optimized by membrane performance.•Optimum TAEA-modified TFC membrane exhibited 94.7 % NH4+ rejection in forward osmosis.•Size sieving, cation exchange, and carboxylic group density influenced NH4+ selectivity.
AbstractList In this study, we aimed to develop a forward osmosis (FO) thin film composite (TFC) membrane which could retain NH4+ from wastewater. The conventional TFC membrane has a microporous polymer support and a selective layer for salt rejection; however, the polyamide selective layer is known to not be able to reject NH4+. Our strategy was to develop tris(2-aminoethyl)amine (TAEA)-modified TFC membranes via secondary interfacial polymerization, and the modification factors were optimized. The NH4+ rejection of the optimized membrane significantly increased from 64.9 % (pristine TFC) to 94.7 %. TAEA modification resulted in a smoother surface and thinner polyamide selective layers. The mechanism of NH4+ rejection during FO operation was investigated and was found to be influenced by membrane surface carboxylic group density and the polyamide crosslinking, cation exchange between the draw and feed solutions, and size sieving. In conclusion, the TAEA-modified membrane showed high selectivity against NH4+ and applicability for NH4+ recovery. In the future, the TAEA-modified membrane may be applied for NH4+ enrichment and recovery from real wastewater systems. [Display omitted] •Thin film composite (TFC) membrane was modified with tris(2-aminoethyl)amine (TAEA).•Secondary interfacial polymerization with TAEA was optimized by membrane performance.•Optimum TAEA-modified TFC membrane exhibited 94.7 % NH4+ rejection in forward osmosis.•Size sieving, cation exchange, and carboxylic group density influenced NH4+ selectivity.
ArticleNumber 116002
Author Matsuyama, Hideto
Istirokhatun, Titik
Takagi, Ryosuke
Gonzales, Ralph Rolly
Yao, Xuesong
Li, Jing
Zhang, Jinhui
Zhang, Pengfei
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Keywords Ammonium recovery
Surface modification
Thin-film composite membrane
Forward osmosis
Tris(2-aminoethyl)amine
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SSID ssj0012933
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Snippet In this study, we aimed to develop a forward osmosis (FO) thin film composite (TFC) membrane which could retain NH4+ from wastewater. The conventional TFC...
SourceID crossref
elsevier
SourceType Aggregation Database
Publisher
StartPage 116002
SubjectTerms Ammonium recovery
Forward osmosis
Surface modification
Thin-film composite membrane
Tris(2-aminoethyl)amine
Title Surface modification of thin film composite forward osmosis membrane using tris(2-aminoethyl)amine for enhanced ammonium recovery
URI https://dx.doi.org/10.1016/j.desal.2022.116002
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