Spectroscopic identification of alizarin in a mixture of organic red dyes by incorporation in Zr-Ormosil
Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The selective incorporation of alizarin into a Zr‐Ormosil polymer induced intense Raman spectra that allow an easy, quick and unequivocal identification...
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| Published in | Journal of Raman spectroscopy Vol. 36; no. 5; pp. 420 - 426 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Chichester, UK
John Wiley & Sons, Ltd
01.05.2005
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| Abstract | Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The selective incorporation of alizarin into a Zr‐Ormosil polymer induced intense Raman spectra that allow an easy, quick and unequivocal identification of this dye. Therefore, this method can be applied to the separation and identification of dyes, which is an important issue in the field of archaeometry. Raman spectroscopy was used to identify alizarin in Zr‐Ormosil at different pH values, solvents and dye concentrations. The best conditions for composite formation were determined. Moreover, the Raman spectra allow us to propose an interaction model for the alizarin–Zr complexes where the monoanionic alizarin forms a chelate with Zr cations in the doped Ormosil similar to the alizarin–Al chelate formed in lacs and alizarin–Ag chelate formed in SERS experiments. Copyright © 2005 John Wiley & Sons, Ltd. |
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| AbstractList | Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The selective incorporation of alizarin into a Zr‐Ormosil polymer induced intense Raman spectra that allow an easy, quick and unequivocal identification of this dye. Therefore, this method can be applied to the separation and identification of dyes, which is an important issue in the field of archaeometry. Raman spectroscopy was used to identify alizarin in Zr‐Ormosil at different pH values, solvents and dye concentrations. The best conditions for composite formation were determined. Moreover, the Raman spectra allow us to propose an interaction model for the alizarin–Zr complexes where the monoanionic alizarin forms a chelate with Zr cations in the doped Ormosil similar to the alizarin–Al chelate formed in lacs and alizarin–Ag chelate formed in SERS experiments. Copyright © 2005 John Wiley & Sons, Ltd. Raman and UV-visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The selective incorporation of alizarin into a Zr-Ormosil polymer induced intense Raman spectra that allow an easy, quick and unequivocal identification of this dye. Therefore, this method can be applied to the separation and identification of dyes, which is an important issue in the field of archaeometry. Raman spectroscopy was used to identify alizarin in Zr-Ormosil at different pH values, solvents and dye concentrations. The best conditions for composite formation were determined. Moreover, the Raman spectra allow us to propose an interaction model for the alizarin-Zr complexes where the monoanionic alizarin forms a chelate with Zr cations in the doped Ormosil similar to the alizarin-Al chelate formed in lacs and alizarin-Ag chelate formed in SERS experiments. Abstract Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The selective incorporation of alizarin into a Zr‐Ormosil polymer induced intense Raman spectra that allow an easy, quick and unequivocal identification of this dye. Therefore, this method can be applied to the separation and identification of dyes, which is an important issue in the field of archaeometry. Raman spectroscopy was used to identify alizarin in Zr‐Ormosil at different pH values, solvents and dye concentrations. The best conditions for composite formation were determined. Moreover, the Raman spectra allow us to propose an interaction model for the alizarin–Zr complexes where the monoanionic alizarin forms a chelate with Zr cations in the doped Ormosil similar to the alizarin–Al chelate formed in lacs and alizarin–Ag chelate formed in SERS experiments. Copyright © 2005 John Wiley & Sons, Ltd. |
| Author | Domingo, C. Garcia-Ramos, J. V. Cañamares, M. V. Sanchez-Cortes, S. Murcia-Mascarós, S. |
| Author_xml | – sequence: 1 givenname: S. surname: Murcia-Mascarós fullname: Murcia-Mascarós, S. email: sonia.mascaros@uv.es organization: Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006 Madrid, Spain – sequence: 2 givenname: C. surname: Domingo fullname: Domingo, C. organization: Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006 Madrid, Spain – sequence: 3 givenname: S. surname: Sanchez-Cortes fullname: Sanchez-Cortes, S. organization: Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006 Madrid, Spain – sequence: 4 givenname: M. V. surname: Cañamares fullname: Cañamares, M. V. organization: Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006 Madrid, Spain – sequence: 5 givenname: J. V. surname: Garcia-Ramos fullname: Garcia-Ramos, J. V. organization: Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006 Madrid, Spain |
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| Cites_doi | 10.1179/sic.1985.30.3.119 10.1002/jrs.1228 10.1016/S0022-3093(99)00365-8 10.1002/(SICI)1099-1395(200003)13:3<141::AID-POC220>3.0.CO;2-J 10.1179/019713692806066637 10.1016/j.jas.2004.02.008 10.1016/S0584-8547(01)00215-4 10.1023/A:1027442627485 10.1023/A:1020720831098 10.1021/j150668a042 10.1016/S0021-9797(03)00339-4 10.2307/1506159 10.1002/jssc.200301484 10.1002/jrs.1199 10.1002/jms.549 10.1016/S0003-2670(00)88607-9 10.1002/jrs.1250180508 10.1016/S0021-9673(03)01170-1 |
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| Snippet | Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The... Abstract Raman and UV–visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The... Raman and UV-visible spectroscopy were applied to the study of a mixture of alizarin and carminic acid, two highly fluorescent anthraquinone dyes. The... |
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| SubjectTerms | Alizarin carminic acid Chelating Dyes Raman spectra Raman spectroscopy Solvents Spectroscopy Zirconium Zr-Ormosil |
| Title | Spectroscopic identification of alizarin in a mixture of organic red dyes by incorporation in Zr-Ormosil |
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