Characterisation of poly( p-phenylenebenzobisoxazole) fibres by solid state NMR
This work investigates the chemical composition and the structure of poly( p-phenylene-2,6-benzobisoxazole) (PBO) fibres using solid state NMR. CP-DD-MAS 13 C NMR including dephasing delay experiments permits to determine the chemical composition of PBO. Studying molecular dynamic of PBO (wide line...
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| Published in | European polymer journal Vol. 38; no. 8; pp. 1645 - 1651 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
01.08.2002
Elsevier |
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| Abstract | This work investigates the chemical composition and the structure of poly(
p-phenylene-2,6-benzobisoxazole) (PBO) fibres using solid state NMR. CP-DD-MAS
13
C
NMR including dephasing delay experiments permits to determine the chemical composition of PBO. Studying molecular dynamic of PBO (wide line
1
H
NMR), the structure of PBO is examined. According to the model of Kitagawa et al., the structure of PBO is then explained. |
|---|---|
| AbstractList | Polybenazoles have been developed by US Air Force researchers as super heat resistant polymer which could surpass the traditional aramid fibers. PBO has superior tensile strength and modulus. This work investigates the chemical composition and the structure of poly(p-phenylene-2,6-benzobisoxazole) (PBO) fibres using solid state NMR. CP-DD-MAS exp 13 C NMR including dephasing delay experiments permits to determine the chemical composition of PBO. Studying molecular dynamic of PBO (wide line exp 1 H NMR), the structure of PBO is examined. According to the model of Kitagawa et al., the structure of PBO is then explained. This work investigates the chemical composition and the structure of poly( p-phenylene-2,6-benzobisoxazole) (PBO) fibres using solid state NMR. CP-DD-MAS 13 C NMR including dephasing delay experiments permits to determine the chemical composition of PBO. Studying molecular dynamic of PBO (wide line 1 H NMR), the structure of PBO is examined. According to the model of Kitagawa et al., the structure of PBO is then explained. |
| Author | Bourbigot, Serge Flambard, Xavier Revel, Bertrand |
| Author_xml | – sequence: 1 givenname: Serge surname: Bourbigot fullname: Bourbigot, Serge email: serge.bourbigot@ensait.fr organization: Laboratoire de Génie et Matériaux Textiles (GEMTEX), UPRES-EA 2461, Ecole Nationale Supérieure des Arts et Industries Textiles (ENSAIT), 9 rue de l'Ermitage, BP 30329, 59056 Roubaix Cedex 01, France – sequence: 2 givenname: Xavier surname: Flambard fullname: Flambard, Xavier organization: Laboratoire de Génie et Matériaux Textiles (GEMTEX), UPRES-EA 2461, Ecole Nationale Supérieure des Arts et Industries Textiles (ENSAIT), 9 rue de l'Ermitage, BP 30329, 59056 Roubaix Cedex 01, France – sequence: 3 givenname: Bertrand surname: Revel fullname: Revel, Bertrand organization: Centre Commun de Mesures RMN, Université des Sciences et Technologies de Lille, 59650 Villeneuve d'Ascq, France |
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| Cites_doi | 10.1016/S0032-3861(97)10273-7 10.1039/ft9969200149 10.1002/1097-0126(200101)50:1<157::AID-PI617>3.0.CO;2-D 10.1016/0032-3861(74)90091-3 10.1016/0031-8914(49)90114-7 10.1021/bk-2001-0797.ch006 10.1016/0370-1573(80)90048-4 10.1016/0016-2361(79)90159-5 10.1021/ma00009a049 10.1088/0957-0233/7/4/002 10.1088/0370-1328/82/1/303 10.1002/pol.1981.230160105 10.1016/S0141-3910(01)00159-8 10.1016/S0141-3910(01)00175-6 10.1016/0301-0104(84)85115-0 10.1016/0032-3861(88)90297-2 10.1002/anie.198814681 10.6028/NBS.IR.82-2611 10.1016/S0032-3861(05)80003-5 10.1002/app.1981.070261115 10.1021/ma980113r 10.1002/(SICI)1099-0488(19980115)36:1<39::AID-POLB5>3.0.CO;2-P 10.1016/0032-3861(92)90880-6 10.1016/0032-3861(92)90879-2 10.1021/ja00513a079 |
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| Keywords | PBO Structure Solid state NMR Molecular dynamic Benzoxazole derivative polymer Solid state Supramolecular structure Synthetic fiber Aromatic polymer NMR spectrometry Fibrillar structure Experimental study Intramolecular mobility Rigid chain |
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| Snippet | This work investigates the chemical composition and the structure of poly(
p-phenylene-2,6-benzobisoxazole) (PBO) fibres using solid state NMR. CP-DD-MAS
13
C... Polybenazoles have been developed by US Air Force researchers as super heat resistant polymer which could surpass the traditional aramid fibers. PBO has... |
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| SubjectTerms | Applied sciences Composites Exact sciences and technology Forms of application and semi-finished materials Molecular dynamic PBO Polymer industry, paints, wood Solid state NMR Structure Technology of polymers |
| Title | Characterisation of poly( p-phenylenebenzobisoxazole) fibres by solid state NMR |
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