A novel chitosan-alginate@Fe/Mn mixed oxide nanocomposite for highly efficient removal of Cr (VI) from wastewater: Experiment and adsorption mechanism

In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr removal was reported. The physicochemical properties of the obtained materials were analyzed using the following methods: SEM-EDX, XRD, FTIR, X...

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Published inInternational journal of biological macromolecules Vol. 263; no. Pt 2; p. 129989
Main Authors Alqarni, Laila S., Algethami, Jari S., EL Kaim Billah, Rachid, Alorabi, Ali Q., Alnaam, Yaser A., Algethami, Faisal K., Bahsis, Lahoucine, Jawad, Ali H., Wasilewska, Małgorzata, López-Maldonado, Eduardo Alberto
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 01.04.2024
Subjects
Chitosan-alginate@Fe/Mn mixed oxide nanocomposite
Cr (VI)
Wastewater treatment
Chitosan-alginate@Fe/Mn mixed oxide nanocomposite
Wastewater treatment
Cr (VI)
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Abstract In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr removal was reported. The physicochemical properties of the obtained materials were analyzed using the following methods: SEM-EDX, XRD, FTIR, XPS, pH drift measurements, and thermal analysis. The adsorption properties were estimated based on equilibrium and adsorption kinetics measurements. The Langmuir, Freundlich and Temkin isotherms were applied to analyze the equilibrium data. The thermodynamic analysis of adsorption isotherms was performed. A number of equations and kinetic models were used to describe the adsorption rate data, including pseudo-first (PFOE) and pseudo-second (PSOE) order kinetic equations. The obtained test results show that the synthesized biomaterial, compared to pure chitosan, is characterized by greater resistance to high temperatures. Moreover, this biomaterial had excellent adsorption properties. For the adsorption of Cr (VI), the equilibrium state was reached after 120 min, and the sorption capacity was 455.9 mg/g. In addition, DFT calculations and NCI analyses were performed to get more light on the adsorption mechanism of Cr (VI) on the prepared biocomposite. •Analysis of physicochemical properties and morphology of the Cs.Alg@Fe/Mn biocomposite•Cs.Alg@Fe/Mn has a more developed structure than pure Cs.•Cs.Alg@Fe/Mn is resistant to high temperatures.•Cs.Alg@Fe/Mn is a highly effective adsorbent for Cr (VI) removal.•The adsorption of Cr (VI) on Cs.Alg@Fe/Mn is spontaneous, endothermic and chemisorption process.
AbstractList In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr removal was reported. The physicochemical properties of the obtained materials were analyzed using the following methods: SEM-EDX, XRD, FTIR, XPS, pH drift measurements, and thermal analysis. The adsorption properties were estimated based on equilibrium and adsorption kinetics measurements. The Langmuir, Freundlich and Temkin isotherms were applied to analyze the equilibrium data. The thermodynamic analysis of adsorption isotherms was performed. A number of equations and kinetic models were used to describe the adsorption rate data, including pseudo-first (PFOE) and pseudo-second (PSOE) order kinetic equations. The obtained test results show that the synthesized biomaterial, compared to pure chitosan, is characterized by greater resistance to high temperatures. Moreover, this biomaterial had excellent adsorption properties. For the adsorption of Cr (VI), the equilibrium state was reached after 120 min, and the sorption capacity was 455.9 mg/g. In addition, DFT calculations and NCI analyses were performed to get more light on the adsorption mechanism of Cr (VI) on the prepared biocomposite.
In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr removal was reported. The physicochemical properties of the obtained materials were analyzed using the following methods: SEM-EDX, XRD, FTIR, XPS, pH drift measurements, and thermal analysis. The adsorption properties were estimated based on equilibrium and adsorption kinetics measurements. The Langmuir, Freundlich and Temkin isotherms were applied to analyze the equilibrium data. The thermodynamic analysis of adsorption isotherms was performed. A number of equations and kinetic models were used to describe the adsorption rate data, including pseudo-first (PFOE) and pseudo-second (PSOE) order kinetic equations. The obtained test results show that the synthesized biomaterial, compared to pure chitosan, is characterized by greater resistance to high temperatures. Moreover, this biomaterial had excellent adsorption properties. For the adsorption of Cr (VI), the equilibrium state was reached after 120 min, and the sorption capacity was 455.9 mg/g. In addition, DFT calculations and NCI analyses were performed to get more light on the adsorption mechanism of Cr (VI) on the prepared biocomposite.
In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr removal was reported. The physicochemical properties of the obtained materials were analyzed using the following methods: SEM-EDX, XRD, FTIR, XPS, pH drift measurements, and thermal analysis. The adsorption properties were estimated based on equilibrium and adsorption kinetics measurements. The Langmuir, Freundlich and Temkin isotherms were applied to analyze the equilibrium data. The thermodynamic analysis of adsorption isotherms was performed. A number of equations and kinetic models were used to describe the adsorption rate data, including pseudo-first (PFOE) and pseudo-second (PSOE) order kinetic equations. The obtained test results show that the synthesized biomaterial, compared to pure chitosan, is characterized by greater resistance to high temperatures. Moreover, this biomaterial had excellent adsorption properties. For the adsorption of Cr (VI), the equilibrium state was reached after 120 min, and the sorption capacity was 455.9 mg/g. In addition, DFT calculations and NCI analyses were performed to get more light on the adsorption mechanism of Cr (VI) on the prepared biocomposite. •Analysis of physicochemical properties and morphology of the Cs.Alg@Fe/Mn biocomposite•Cs.Alg@Fe/Mn has a more developed structure than pure Cs.•Cs.Alg@Fe/Mn is resistant to high temperatures.•Cs.Alg@Fe/Mn is a highly effective adsorbent for Cr (VI) removal.•The adsorption of Cr (VI) on Cs.Alg@Fe/Mn is spontaneous, endothermic and chemisorption process.
ArticleNumber 129989
Author EL Kaim Billah, Rachid
Wasilewska, Małgorzata
Algethami, Jari S.
Jawad, Ali H.
Algethami, Faisal K.
Alorabi, Ali Q.
Alnaam, Yaser A.
López-Maldonado, Eduardo Alberto
Alqarni, Laila S.
Bahsis, Lahoucine
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  fullname: López-Maldonado, Eduardo Alberto
  email: elopez92@uabc.edu.mx
  organization: Faculty of Chemical Sciences and Engineering, Autonomous University of Baja, California, Tijuana 22390, Baja California, Mexico
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Keywords Chitosan-alginate@Fe/Mn mixed oxide nanocomposite
Wastewater treatment
Cr (VI)
Language English
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Snippet In this study, the synthesis and experimental theoretical evaluation of a new chitosan/alginate/hydrozyapatite nanocomposite doped with Mn2 and Fe2O3 for Cr...
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SubjectTerms Chitosan-alginate@Fe/Mn mixed oxide nanocomposite
Cr (VI)
Wastewater treatment
Title A novel chitosan-alginate@Fe/Mn mixed oxide nanocomposite for highly efficient removal of Cr (VI) from wastewater: Experiment and adsorption mechanism
URI https://dx.doi.org/10.1016/j.ijbiomac.2024.129989
https://www.ncbi.nlm.nih.gov/pubmed/38354916
https://search.proquest.com/docview/2927214179
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