Spectrum imaging measurements with semi-parallel detection using an AES apparatus
•Auger spectrum imaging data cube acquisition is demonstrated.•An HSA with semi-parallel detection is used.•Example imaging spectrum data is acquired for a sample with an uneven surface. We have developed a method to obtain a data cube using a semi-parallel detection scheme and an electrostatic hemi...
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Published in | Ultramicroscopy Vol. 233; p. 113450 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
Published |
Netherlands
Elsevier B.V
01.03.2022
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Subjects | |
Online Access | Get full text |
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Summary: | •Auger spectrum imaging data cube acquisition is demonstrated.•An HSA with semi-parallel detection is used.•Example imaging spectrum data is acquired for a sample with an uneven surface.
We have developed a method to obtain a data cube using a semi-parallel detection scheme and an electrostatic hemispherical analyzer (HSA) with multi-channel detection. By improving the Auger intensity map measurement scheme, the number of detector energy sweeps is reduced, and faster measurement is achieved. The gain differences among the detection channel are corrected by post-processing, and a data cube of Auger electron spectra is constructed. A data cube was obtained for an example of a sample with a non-flat surface, lead-free solder. It was demonstrated to be possible to extract spectra from any position within the measurement area and create the elemental distribution maps. |
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Bibliography: | ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
ISSN: | 0304-3991 1879-2723 |
DOI: | 10.1016/j.ultramic.2021.113450 |