Modifying Polyvinylidene Chloride Resin with Fluorine Monomer and Cross‐Linking Monomers

Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fouri...

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Published inMacromolecular rapid communications. Vol. 45; no. 21; pp. e2400402 - n/a
Main Authors Gao, Fengjun, Zhang, Zhifeng, Song, Qianqian, Abo‐Dief, Hala M., Alzahrani, Eman, Wang, Shouyang, Liu, Yan, Shao, Qian, Yang, Jing, Guo, Zhanhu, El‐Bahy, Zeinhom M., Ge, Ruixiang
Format Journal Article
LanguageEnglish
Published Germany Wiley Subscription Services, Inc 01.11.2024
Subjects
Contact angle
Cross-Linking Reagents - chemistry
Emulsion polymerization
Emulsions
Energy distribution
Fluorine
Fluorine - chemistry
fluorine monomers
Fourier transforms
Infrared analysis
Infrared spectroscopy
Mechanical properties
Methacrylates - chemistry
modification
Monomers
Photoelectron spectroscopy
Photoelectrons
Polymerization
Polyvinyl Chloride - analogs & derivatives
Polyvinyl Chloride - chemistry
polyvinylidene chloride resin
Polyvinylidene chlorides
Polyvinyls - chemistry
Resins
Resins, Synthetic - chemistry
Room temperature
Scanning electron microscopy
Spectrum analysis
Storage stability
Surface Properties
Thermal stability
Trimethylolpropane trimethacrylate
Water resistance
water resistance performance
X ray photoelectron spectroscopy
polyvinylidene chloride resin
fluorine monomers
water resistance performance
modification
trimethylolpropane trimethacrylate
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Abstract Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fourier transform infrared spectroscopy (FTIR) and X‐ray photoelectron spectroscopy (XPS) analyses. Scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and XPS were utilized to investigate the element distribution in the modified monomer emulsion and the mechanism of monomer modification. The results demonstrated that the fluorine monomer was reacted in the resin, and mainly concentrated on the surface of the resin. The addition of octafluoropentyl methacrylate and trimethylolpropane trimethacrylate improved the water resistance of the resin. Compared to unmodified PVDC resin, the contact angle of the modified PVDC resin increased from 89.46° to 109.51°, and the water resistance at room temperature increased from 120 to 500 h. Furthermore, the modified resin exhibited excellent mechanical properties, thermal stability, and storage stability. The polyvinylidene chloride resin was modified with fluorine monomer and cross‐linking monomers to achieve enhanced properties.
AbstractList Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fourier transform infrared spectroscopy (FTIR) and X‐ray photoelectron spectroscopy (XPS) analyses. Scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and XPS were utilized to investigate the element distribution in the modified monomer emulsion and the mechanism of monomer modification. The results demonstrated that the fluorine monomer was reacted in the resin, and mainly concentrated on the surface of the resin. The addition of octafluoropentyl methacrylate and trimethylolpropane trimethacrylate improved the water resistance of the resin. Compared to unmodified PVDC resin, the contact angle of the modified PVDC resin increased from 89.46° to 109.51°, and the water resistance at room temperature increased from 120 to 500 h. Furthermore, the modified resin exhibited excellent mechanical properties, thermal stability, and storage stability. The polyvinylidene chloride resin was modified with fluorine monomer and cross‐linking monomers to achieve enhanced properties.
Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fourier transform infrared spectroscopy (FTIR) and X‐ray photoelectron spectroscopy (XPS) analyses. Scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and XPS were utilized to investigate the element distribution in the modified monomer emulsion and the mechanism of monomer modification. The results demonstrated that the fluorine monomer was reacted in the resin, and mainly concentrated on the surface of the resin. The addition of octafluoropentyl methacrylate and trimethylolpropane trimethacrylate improved the water resistance of the resin. Compared to unmodified PVDC resin, the contact angle of the modified PVDC resin increased from 89.46° to 109.51°, and the water resistance at room temperature increased from 120 to 500 h. Furthermore, the modified resin exhibited excellent mechanical properties, thermal stability, and storage stability.
Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS) analyses. Scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and XPS were utilized to investigate the element distribution in the modified monomer emulsion and the mechanism of monomer modification. The results demonstrated that the fluorine monomer was reacted in the resin, and mainly concentrated on the surface of the resin. The addition of octafluoropentyl methacrylate and trimethylolpropane trimethacrylate improved the water resistance of the resin. Compared to unmodified PVDC resin, the contact angle of the modified PVDC resin increased from 89.46° to 109.51°, and the water resistance at room temperature increased from 120 to 500 h. Furthermore, the modified resin exhibited excellent mechanical properties, thermal stability, and storage stability.Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers through seeded emulsion polymerization. The successful incorporation of octafluoropentyl methacrylate into the PVDC resin was confirmed by Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS) analyses. Scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and XPS were utilized to investigate the element distribution in the modified monomer emulsion and the mechanism of monomer modification. The results demonstrated that the fluorine monomer was reacted in the resin, and mainly concentrated on the surface of the resin. The addition of octafluoropentyl methacrylate and trimethylolpropane trimethacrylate improved the water resistance of the resin. Compared to unmodified PVDC resin, the contact angle of the modified PVDC resin increased from 89.46° to 109.51°, and the water resistance at room temperature increased from 120 to 500 h. Furthermore, the modified resin exhibited excellent mechanical properties, thermal stability, and storage stability.
Author Liu, Yan
Alzahrani, Eman
El‐Bahy, Zeinhom M.
Song, Qianqian
Abo‐Dief, Hala M.
Yang, Jing
Ge, Ruixiang
Gao, Fengjun
Wang, Shouyang
Shao, Qian
Guo, Zhanhu
Zhang, Zhifeng
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  organization: Shandong University of Science and Technology
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Issue 21
Keywords polyvinylidene chloride resin
fluorine monomers
water resistance performance
modification
trimethylolpropane trimethacrylate
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e_1_2_8_61_1
e_1_2_8_82_1
e_1_2_8_18_1
e_1_2_8_39_1
Liu Z. (e_1_2_8_8_1) 2022; 17
Colorado H. A. (e_1_2_8_9_1) 2024; 27
e_1_2_8_14_1
e_1_2_8_35_1
e_1_2_8_16_1
e_1_2_8_37_1
e_1_2_8_79_1
Sivasankarapillai V. S. (e_1_2_8_89_1) 2022; 15
Izah S. C. (e_1_2_8_1_1) 2023; 14
e_1_2_8_92_1
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40396642 - Macromol Rapid Commun. 2025 May 21:e2500356. doi: 10.1002/marc.202500356.
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Snippet Modified polyvinylidene chloride (PVDC) resin was prepared using octafluoropentyl methacrylate and trimethylolpropane trimethacrylate as modifying monomers...
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wiley
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StartPage e2400402
SubjectTerms Contact angle
Cross-Linking Reagents - chemistry
Emulsion polymerization
Emulsions
Energy distribution
Fluorine
Fluorine - chemistry
fluorine monomers
Fourier transforms
Infrared analysis
Infrared spectroscopy
Mechanical properties
Methacrylates - chemistry
modification
Monomers
Photoelectron spectroscopy
Photoelectrons
Polymerization
Polyvinyl Chloride - analogs & derivatives
Polyvinyl Chloride - chemistry
polyvinylidene chloride resin
Polyvinylidene chlorides
Polyvinyls - chemistry
Resins
Resins, Synthetic - chemistry
Room temperature
Scanning electron microscopy
Spectrum analysis
Storage stability
Surface Properties
Thermal stability
Trimethylolpropane trimethacrylate
Water resistance
water resistance performance
X ray photoelectron spectroscopy
Title Modifying Polyvinylidene Chloride Resin with Fluorine Monomer and Cross‐Linking Monomers
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fmarc.202400402
https://www.ncbi.nlm.nih.gov/pubmed/39235433
https://www.proquest.com/docview/3125970703
https://www.proquest.com/docview/3100919486
Volume 45
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