Surface-engineered N-doped carbon nanotubes with B-doped graphene quantum dots: Strategies to develop highly-efficient noble metal-free electrocatalyst for online-monitoring dissolved oxygen biosensor
Dissolved oxygen (DO) is an essential indicator for evaluating water quality, the exquisitely sensitive electrochemical DO sensor could accurately record response which was based on oxygen reduction reaction (ORR) with a sluggish reaction rate. Thus, high-efficient ORR electrocatalysts are urgently...
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| Published in | Carbon (New York) Vol. 186; pp. 406 - 415 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Elsevier Ltd
01.01.2022
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Dissolved oxygen (DO) is an essential indicator for evaluating water quality, the exquisitely sensitive electrochemical DO sensor could accurately record response which was based on oxygen reduction reaction (ORR) with a sluggish reaction rate. Thus, high-efficient ORR electrocatalysts are urgently needed for broad applications. As a matter of fact, graphene quantum dots (GQDs) have attracted a great deal of attention, several heteroatoms are extensively introduced in GQDs fragments to regulate their inherent chemical and electrical properties by adjusting their electronic structure. However, B–N–C moieties always exist for some BN-codoped carbons due to the intermolecular force that might prohibit its electrocatalytic activity. Therefore, this research design a strategy to solve this problem; despite substantial efforts, this study shows a metal-free B-doped GQD/N-doped carbon nanotubes (BGQD/NCNTs) electrode significantly influences ORR electrocatalytic activity due to the synergistic effect and abundant active sites. Herein, BGQD/NCNTs exhibit an excellent ORR performance with an onset potential of 0.91 V (vs. RHE), exceeding most reported GQDs-introduced electrocatalysts; it also outperformed the commercial electrocatalyst in terms of long-term stability. For seawater DO sensing, BGQD/NCNTs exhibit ultra-high sensitivity of 0.011 mA/cm2ppm and further integrate into an online detection platform to accomplish the aim of continuous monitoring via a wireless connection.
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•A novel strategy to lower B–N moieties in B,N-codoped carbon based electrocatalyst was proposed.•BGQDs/NCNTs display better onset potential toward ORR than pristine CNTs.•BGQD/NCNTs shows promising sensitivity and stability for dissolved oxygen sensing in seawater.•The aim of continuous online monitoring was achieved via a wireless connection. |
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| AbstractList | Dissolved oxygen (DO) is an essential indicator for evaluating water quality, the exquisitely sensitive electrochemical DO sensor could accurately record response which was based on oxygen reduction reaction (ORR) with a sluggish reaction rate. Thus, high-efficient ORR electrocatalysts are urgently needed for broad applications. As a matter of fact, graphene quantum dots (GQDs) have attracted a great deal of attention, several heteroatoms are extensively introduced in GQDs fragments to regulate their inherent chemical and electrical properties by adjusting their electronic structure. However, B–N–C moieties always exist for some BN-codoped carbons due to the intermolecular force that might prohibit its electrocatalytic activity. Therefore, this research design a strategy to solve this problem; despite substantial efforts, this study shows a metal-free B-doped GQD/N-doped carbon nanotubes (BGQD/NCNTs) electrode significantly influences ORR electrocatalytic activity due to the synergistic effect and abundant active sites. Herein, BGQD/NCNTs exhibit an excellent ORR performance with an onset potential of 0.91 V (vs. RHE), exceeding most reported GQDs-introduced electrocatalysts; it also outperformed the commercial electrocatalyst in terms of long-term stability. For seawater DO sensing, BGQD/NCNTs exhibit ultra-high sensitivity of 0.011 mA/cm²ppm and further integrate into an online detection platform to accomplish the aim of continuous monitoring via a wireless connection. Dissolved oxygen (DO) is an essential indicator for evaluating water quality, the exquisitely sensitive electrochemical DO sensor could accurately record response which was based on oxygen reduction reaction (ORR) with a sluggish reaction rate. Thus, high-efficient ORR electrocatalysts are urgently needed for broad applications. As a matter of fact, graphene quantum dots (GQDs) have attracted a great deal of attention, several heteroatoms are extensively introduced in GQDs fragments to regulate their inherent chemical and electrical properties by adjusting their electronic structure. However, B–N–C moieties always exist for some BN-codoped carbons due to the intermolecular force that might prohibit its electrocatalytic activity. Therefore, this research design a strategy to solve this problem; despite substantial efforts, this study shows a metal-free B-doped GQD/N-doped carbon nanotubes (BGQD/NCNTs) electrode significantly influences ORR electrocatalytic activity due to the synergistic effect and abundant active sites. Herein, BGQD/NCNTs exhibit an excellent ORR performance with an onset potential of 0.91 V (vs. RHE), exceeding most reported GQDs-introduced electrocatalysts; it also outperformed the commercial electrocatalyst in terms of long-term stability. For seawater DO sensing, BGQD/NCNTs exhibit ultra-high sensitivity of 0.011 mA/cm2ppm and further integrate into an online detection platform to accomplish the aim of continuous monitoring via a wireless connection. [Display omitted] •A novel strategy to lower B–N moieties in B,N-codoped carbon based electrocatalyst was proposed.•BGQDs/NCNTs display better onset potential toward ORR than pristine CNTs.•BGQD/NCNTs shows promising sensitivity and stability for dissolved oxygen sensing in seawater.•The aim of continuous online monitoring was achieved via a wireless connection. Dissolved oxygen (DO) is an essential indicator for evaluating water quality, the exquisitely sensitive electrochemical DO sensor could accurately record response which was based on oxygen reduction reaction (ORR) with a sluggish reaction rate. Thus, high-efficient ORR electrocatalysts are urgently needed for broad applications. As a matter of fact, graphene quantum dots (GQDs) have attracted a great deal of attention, several heteroatoms are extensively introduced in GQDs fragments to regulate their inherent chemical and electrical properties by adjusting their electronic structure. However, B–N–C moieties always exist for some BN-codoped carbons due to the intermolecular force that might prohibit its electrocatalytic activity. Therefore, this research design a strategy to solve this problem; despite substantial efforts, this study shows a metal-free B-doped GQD/N-doped carbon nanotubes (BGQD/NCNTs) electrode significantly influences ORR electrocatalytic activity due to the synergistic effect and abundant active sites. Herein, BGQD/NCNTs exhibit an excellent ORR performance with an onset potential of 0.91 V (vs. RHE), exceeding most reported GQDs-introduced electrocatalysts; it also outperformed the commercial electrocatalyst in terms of long-term stability. For seawater DO sensing, BGQD/NCNTs exhibit ultra-high sensitivity of 0.011 mA/cm2ppm and further integrate into an online detection platform to accomplish the aim of continuous monitoring via a wireless connection. |
| Author | Wang, Yu-Xuan Rinawati, Mia Lin, Pin-Hsuan Cheng, Yao-Sheng Chen, Kuan-Jung Ho, Kuo-Chuan Yeh, Min-Hsin Huang, Wei-Hsiang Chang, Ling-Yu Su, Wei-Nien |
| Author_xml | – sequence: 1 givenname: Yu-Xuan surname: Wang fullname: Wang, Yu-Xuan organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan – sequence: 2 givenname: Mia surname: Rinawati fullname: Rinawati, Mia organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan – sequence: 3 givenname: Wei-Hsiang surname: Huang fullname: Huang, Wei-Hsiang organization: Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan – sequence: 4 givenname: Yao-Sheng surname: Cheng fullname: Cheng, Yao-Sheng organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan – sequence: 5 givenname: Pin-Hsuan surname: Lin fullname: Lin, Pin-Hsuan organization: Mighty Electronic Co, Ltd, Hsinchu City, Taiwan – sequence: 6 givenname: Kuan-Jung surname: Chen fullname: Chen, Kuan-Jung organization: Mighty Electronic Co, Ltd, Hsinchu City, Taiwan – sequence: 7 givenname: Ling-Yu surname: Chang fullname: Chang, Ling-Yu organization: Institute of Polymer Science and Engineering, National Taiwan University, Taipei, 10617, Taiwan – sequence: 8 givenname: Kuo-Chuan surname: Ho fullname: Ho, Kuo-Chuan organization: Institute of Polymer Science and Engineering, National Taiwan University, Taipei, 10617, Taiwan – sequence: 9 givenname: Wei-Nien surname: Su fullname: Su, Wei-Nien organization: Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan – sequence: 10 givenname: Min-Hsin orcidid: 0000-0002-6150-4750 surname: Yeh fullname: Yeh, Min-Hsin email: mhyeh@mail.ntust.edu.tw organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan |
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| Keywords | Carbon nanotubes Online monitoring Dissolved oxygen measurement Heteroatom doping Oxygen reduction reaction Graphene quantum dots |
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| SubjectTerms | Biosensors Carbon Carbon nanotubes Dissolved oxygen Dissolved oxygen measurement Electrical properties Electrocatalysis Electrocatalysts electrochemistry electrodes Electronic structure Graphene Graphene quantum dots Heteroatom doping Intermolecular forces Monitoring Nanotubes Noble metals Online monitoring Oxygen Oxygen reduction reaction Oxygen reduction reactions Quantum dots Seawater synergism Synergistic effect Water quality |
| Title | Surface-engineered N-doped carbon nanotubes with B-doped graphene quantum dots: Strategies to develop highly-efficient noble metal-free electrocatalyst for online-monitoring dissolved oxygen biosensor |
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