Preparation of colloidal carbon nanotube dispersions and their characterisation using a disc centrifuge
After their synthesis, carbon nanotubes are usually obtained as mechanically entangled solid bodies or subsequently associate themselves into aggregates. This leads to the demand of an effective dispersing method for the preparation of CNT-based composites. This paper studies selected dispersing mec...
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| Published in | Carbon (New York) Vol. 46; no. 11; pp. 1384 - 1392 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
01.09.2008
Elsevier Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | After their synthesis, carbon nanotubes are usually obtained as mechanically entangled solid bodies or subsequently associate themselves into aggregates. This leads to the demand of an effective dispersing method for the preparation of CNT-based composites. This paper studies selected dispersing mechanisms such as cavitation and high shear forces for the preparation of colloidal CNT/epoxy dispersions, which were subject to a particle size analysis using a differential sedimentation based disc centrifuge. Due to the remarkable shape of carbon nanotubes the measurement routines had to be adjusted and a validation of measurement results was performed. The fact that the disc centrifuge is suitable for the detection of residual agglomerates in CNT dispersions was shown by monitoring the dispersing methods ultrasonication and calendering. |
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| AbstractList | After their synthesis, carbon nanotubes are usually obtained as mechanically entangled solid bodies or subsequently associate themselves into aggregates. This leads to the demand of an effective dispersing method for the preparation of CNT-based composites. This paper studies selected dispersing mechanisms such as cavitation and high shear forces for the preparation of colloidal CNT/epoxy dispersions, which were subject to a particle size analysis using a differential sedimentation based disc centrifuge. Due to the remarkable shape of carbon nanotubes the measurement routines had to be adjusted and a validation of measurement results was performed. The fact that the disc centrifuge is suitable for the detection of residual agglomerates in CNT dispersions was shown by monitoring the dispersing methods ultrasonication and calendering. |
| Author | Kwade, Arno Mahrholz, Thorsten Schilde, Carsten Nadler, Michael Riedel, Ulrich |
| Author_xml | – sequence: 1 givenname: Michael surname: Nadler fullname: Nadler, Michael email: correspondence@belucha.de, michaelnadler@gmx.de organization: Institute of Lightweight Engineering and Polymer Technology, TU Dresden, Holbeinstraße 3, 01062 Dresden, Germany – sequence: 2 givenname: Thorsten surname: Mahrholz fullname: Mahrholz, Thorsten organization: German Aerospace Center (DLR), Institute of Composite Structures and Adaptive Systems, Lilienthalplatz 7, 38108 Braunschweig, Germany – sequence: 3 givenname: Ulrich surname: Riedel fullname: Riedel, Ulrich organization: German Aerospace Center (DLR), Institute of Composite Structures and Adaptive Systems, Lilienthalplatz 7, 38108 Braunschweig, Germany – sequence: 4 givenname: Carsten surname: Schilde fullname: Schilde, Carsten organization: Institute of Particle Technology, TU Braunschweig, Volkmaroder Straße 5, 38104 Braunschweig, Germany – sequence: 5 givenname: Arno surname: Kwade fullname: Kwade, Arno organization: Institute of Particle Technology, TU Braunschweig, Volkmaroder Straße 5, 38104 Braunschweig, Germany |
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| Keywords | Validation Particle size Shear Shape Carbon nanotubes Solid body Colloidal dispersion Forces Cavitation Sedimentation Mechanism Composite materials Synthesis Preparation Aggregate |
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| Snippet | After their synthesis, carbon nanotubes are usually obtained as mechanically entangled solid bodies or subsequently associate themselves into aggregates. This... |
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| SubjectTerms | Chemistry Colloidal state and disperse state Cross-disciplinary physics: materials science; rheology Exact sciences and technology Fullerenes and related materials; diamonds, graphite General and physical chemistry Materials science Physical and chemical studies. Granulometry. Electrokinetic phenomena Physics Specific materials |
| Title | Preparation of colloidal carbon nanotube dispersions and their characterisation using a disc centrifuge |
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