Synthesis and characterisation of LDH‐type anionic nanomaterials for the effective removal of doxycycline from aqueous media

In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH was investigated. Almost full characterisation of the prepared LDHs before and after adsorption was conducted using X‐ray diffraction, Fourie...

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Published inWater and environment journal : WEJ Vol. 34; no. S1; pp. 290 - 308
Main Authors Abdel Moaty, S. A., Mahmoud, Rehab K., Mohamed, Nada A., Gaber, Yasser, Farghali, Ahmed A., Abdel Wahed, Mahmoud S. M., Younes, Heba A.
Format Journal Article
LanguageEnglish
Published London Wiley Subscription Services, Inc 01.12.2020
Subjects
Adsorption
Aluminum
Analytical methods
Anions
Antibiotics
Aqueous solutions
Doxycycline
Electron microscopes
environment
equations
Field emission microscopy
Fourier transform infrared spectroscopy
geometry
Hydroxides
Infrared spectroscopy
Iron
Kinetics
LDH
Magnesium
Mathematical models
modified
multi‐walled carbon nanotubes
Nanomaterials
Nanotechnology
Removal
Scanning electron microscopy
surface area
transmission electron microscopes
water
X-ray diffraction
Zeta potential
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Abstract In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH was investigated. Almost full characterisation of the prepared LDHs before and after adsorption was conducted using X‐ray diffraction, Fourier‐transform infrared spectroscopy, zeta potential, Brunauer–Emmett–Teller used for detecting the surface area, high‐resolution transmission electron microscope (HRTEM) and field emission scanning electron microscope. The effect of different factors on doxycycline adsorption capacity was investigated. The removal percentages of doxycycline were 80, 82 and 92% by Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH, respectively. These results were attributed to the difference in the pore volume and geometry between the different LDHs. The isothermal and kinetic models of adsorption were also studied. The kinetics of adsorption were described by the second‐order equation with a better fit showed by a high R2 value. Mathematically, the Langmuir and Freundlich models best fitted the equilibrium data.
AbstractList In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH was investigated. Almost full characterisation of the prepared LDHs before and after adsorption was conducted using X‐ray diffraction, Fourier‐transform infrared spectroscopy, zeta potential, Brunauer–Emmett–Teller used for detecting the surface area, high‐resolution transmission electron microscope (HRTEM) and field emission scanning electron microscope. The effect of different factors on doxycycline adsorption capacity was investigated. The removal percentages of doxycycline were 80, 82 and 92% by Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH, respectively. These results were attributed to the difference in the pore volume and geometry between the different LDHs. The isothermal and kinetic models of adsorption were also studied. The kinetics of adsorption were described by the second‐order equation with a better fit showed by a high R² value. Mathematically, the Langmuir and Freundlich models best fitted the equilibrium data.
In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH was investigated. Almost full characterisation of the prepared LDHs before and after adsorption was conducted using X‐ray diffraction, Fourier‐transform infrared spectroscopy, zeta potential, Brunauer–Emmett–Teller used for detecting the surface area, high‐resolution transmission electron microscope (HRTEM) and field emission scanning electron microscope. The effect of different factors on doxycycline adsorption capacity was investigated. The removal percentages of doxycycline were 80, 82 and 92% by Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH, respectively. These results were attributed to the difference in the pore volume and geometry between the different LDHs. The isothermal and kinetic models of adsorption were also studied. The kinetics of adsorption were described by the second‐order equation with a better fit showed by a high R 2 value. Mathematically, the Langmuir and Freundlich models best fitted the equilibrium data.
In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH was investigated. Almost full characterisation of the prepared LDHs before and after adsorption was conducted using X‐ray diffraction, Fourier‐transform infrared spectroscopy, zeta potential, Brunauer–Emmett–Teller used for detecting the surface area, high‐resolution transmission electron microscope (HRTEM) and field emission scanning electron microscope. The effect of different factors on doxycycline adsorption capacity was investigated. The removal percentages of doxycycline were 80, 82 and 92% by Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH, respectively. These results were attributed to the difference in the pore volume and geometry between the different LDHs. The isothermal and kinetic models of adsorption were also studied. The kinetics of adsorption were described by the second‐order equation with a better fit showed by a high R2 value. Mathematically, the Langmuir and Freundlich models best fitted the equilibrium data.
Author Abdel Wahed, Mahmoud S. M.
Mahmoud, Rehab K.
Gaber, Yasser
Younes, Heba A.
Farghali, Ahmed A.
Mohamed, Nada A.
Abdel Moaty, S. A.
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  givenname: Nada A.
  surname: Mohamed
  fullname: Mohamed, Nada A.
  organization: Beni‐Suef University
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  surname: Younes
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  organization: Beni‐Suef University
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Snippet In this work, the removal of a model antibiotic named ‘doxycycline’ by three‐layered double hydroxides (LDHs) such as Mg–Fe LDH, Mg–Al LDH and Mg–Al/MWCNT LDH...
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SubjectTerms Adsorption
Aluminum
Analytical methods
Anions
Antibiotics
Aqueous solutions
Doxycycline
Electron microscopes
environment
equations
Field emission microscopy
Fourier transform infrared spectroscopy
geometry
Hydroxides
Infrared spectroscopy
Iron
Kinetics
LDH
Magnesium
Mathematical models
modified
multi‐walled carbon nanotubes
Nanomaterials
Nanotechnology
Removal
Scanning electron microscopy
surface area
transmission electron microscopes
water
X-ray diffraction
Zeta potential
Title Synthesis and characterisation of LDH‐type anionic nanomaterials for the effective removal of doxycycline from aqueous media
URI https://onlinelibrary.wiley.com/doi/abs/10.1111%2Fwej.12526
https://www.proquest.com/docview/2473421077
https://www.proquest.com/docview/2524241271
Volume 34
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