Mechanical Properties of TiB/Ti Composites by Spark Plasma Sintering

In-situ TiB whisker reinforced, pure Ti matrix composites have been fabricated by spark plasma sintering (SPS). The microstructure and morphology of the in-situ TiB whiskers in the matrix was observed by scanning electron microscopy (SEM). Mechanical properties, such as elevated-temperature tensile...

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Published inJournal of Solid Mechanics and Materials Engineering Vol. 2; no. 2; pp. 234 - 242
Main Authors IZUI, Hiroshi, KOMAKI, Shuhei, OKANO, Michiharu
Format Journal Article
LanguageEnglish
Published The Japan Society of Mechanical Engineers 2008
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Abstract In-situ TiB whisker reinforced, pure Ti matrix composites have been fabricated by spark plasma sintering (SPS). The microstructure and morphology of the in-situ TiB whiskers in the matrix was observed by scanning electron microscopy (SEM). Mechanical properties, such as elevated-temperature tensile strength, fatigue resistance at 600°C, and creep rupture strength at 600°C were investigated. When the composites (TiB/Ti) were sintered at 900°C with a pressure of 60 MPa for 30 min, most of TiB2 was transformed into TiB whiskers in the matrix. The composites sintered at 900°C with a pressure of 60 MPa for 30 min had the highest tensile strength at room temperature. The tensile strength of the composites sintered by SPS is higher than those produced by vacuum arc melting. The elastic modulus of the composites increased proportionally with the TiB volume fraction. The composites show the same or higher strength of Ti-15V-3Cr-3Al-3Sn sintered by SPS at less than 600°C. The fatigue and creep resistance of the composites at 600°C are relatively higher compared to those of Ti sintered by SPS.
AbstractList In-situ TiB whisker reinforced, pure Ti matrix composites have been fabricated by spark plasma sintering (SPS). The microstructure and morphology of the in-situ TiB whiskers in the matrix was observed by scanning electron microscopy (SEM). Mechanical properties, such as elevated-temperature tensile strength, fatigue resistance at 600°C, and creep rupture strength at 600°C were investigated. When the composites (TiB/Ti) were sintered at 900°C with a pressure of 60 MPa for 30 min, most of TiB2 was transformed into TiB whiskers in the matrix. The composites sintered at 900°C with a pressure of 60 MPa for 30 min had the highest tensile strength at room temperature. The tensile strength of the composites sintered by SPS is higher than those produced by vacuum arc melting. The elastic modulus of the composites increased proportionally with the TiB volume fraction. The composites show the same or higher strength of Ti-15V-3Cr-3Al-3Sn sintered by SPS at less than 600°C. The fatigue and creep resistance of the composites at 600°C are relatively higher compared to those of Ti sintered by SPS.
In-situ TiB whisker reinforced, pure Ti matrix composites have been fabricated by spark plasma sintering (SPS). The microstructure and morphology of the in-situ TiB whiskers in the matrix was observed by scanning electron microscopy (SEM). Mechanical properties, such as elevated-temperature tensile strength, fatigue resistance at 600C, and creep rupture strength at 600C were investigated. When the composites (TiB/Ti) were sintered at 900C with a pressure of 60 MPa for 30 min, most of TiB sub(2) was transformed into TiB whiskers in the matrix. The composites sintered at 900C with a pressure of 60 MPa for 30 min had the highest tensile strength at room temperature. The tensile strength of the composites sintered by SPS is higher than those produced by vacuum arc melting. The elastic modulus of the composites increased proportionally with the TiB volume fraction. The composites show the same or higher strength of Ti-15V-3Cr-3Al-3Sn sintered by SPS at less than 600C. The fatigue and creep resistance of the composites at 600C are relatively higher compared to those of Ti sintered by SPS.
Author KOMAKI, Shuhei
OKANO, Michiharu
IZUI, Hiroshi
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Snippet In-situ TiB whisker reinforced, pure Ti matrix composites have been fabricated by spark plasma sintering (SPS). The microstructure and morphology of the...
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SubjectTerms Creep Rupture Strength
Fatigue Resistance
Mechanical properties
Metal Matrix Composites
Particulate composites
Scanning electron microscopy
Sintering
Spark Plasma Sintering
Tensile strength
Tensile Strength at Elevated Temperature
TiB Whisker
Titanium
Whisker composites
Title Mechanical Properties of TiB/Ti Composites by Spark Plasma Sintering
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