Effect of molecular weight between crosslinks on the fracture behavior of rubber-toughened epoxy adhesives
The effect of molecular weight between crosslinks, Mc, on the fracture behavior of rubber‐toughened epoxy adhesives was investigated and compared with the behavior of the bulk resins. In the liquid rubber‐toughened bulk system, fracture energy increased with increasing Mc. However, in the liquid rub...
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Published in | Journal of applied polymer science Vol. 79; no. 1; pp. 38 - 48 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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New York
John Wiley & Sons, Inc
03.01.2001
Wiley |
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Abstract | The effect of molecular weight between crosslinks, Mc, on the fracture behavior of rubber‐toughened epoxy adhesives was investigated and compared with the behavior of the bulk resins. In the liquid rubber‐toughened bulk system, fracture energy increased with increasing Mc. However, in the liquid rubber‐toughened adhesive system, with increasing Mc, the locus of joint fracture had a transition from cohesive failure, break in the bond layer, to interfacial failure, rupture of the bond layer from the surface of the substrate. Specimens fractured by cohesive failure exhibited larger fracture energies than those by interfacial failure. The occurrence of transition from cohesive to interfacial failure seemed to be caused by the increase in the ductility of matrix, the mismatch of elastic constant, and the agglomeration of rubber particles at the metal/epoxy interface. When core‐shell rubber, which did not agglomerate at the interface, was used as a toughening agent, fracture energy increased with Mc. © 2000 John Wiley & Sons, Inc. J Appl Polym Sci 79: 38–48, 2001 |
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AbstractList | The effect of molecular weight between crosslinks, Mc, on the fracture behavior of rubber‐toughened epoxy adhesives was investigated and compared with the behavior of the bulk resins. In the liquid rubber‐toughened bulk system, fracture energy increased with increasing Mc. However, in the liquid rubber‐toughened adhesive system, with increasing Mc, the locus of joint fracture had a transition from cohesive failure, break in the bond layer, to interfacial failure, rupture of the bond layer from the surface of the substrate. Specimens fractured by cohesive failure exhibited larger fracture energies than those by interfacial failure. The occurrence of transition from cohesive to interfacial failure seemed to be caused by the increase in the ductility of matrix, the mismatch of elastic constant, and the agglomeration of rubber particles at the metal/epoxy interface. When core‐shell rubber, which did not agglomerate at the interface, was used as a toughening agent, fracture energy increased with Mc. © 2000 John Wiley & Sons, Inc. J Appl Polym Sci 79: 38–48, 2001 |
Author | Lim, Soonho Lee, Sang-Soo Choe, Chul Rim Park, Min Jho, Jae Young Kim, Junkyung Kang, Byoung Un |
Author_xml | – sequence: 1 givenname: Byoung Un surname: Kang fullname: Kang, Byoung Un organization: School of Chemical Engineering, Seoul National University, Seoul 151-742, Korea – sequence: 2 givenname: Jae Young surname: Jho fullname: Jho, Jae Young organization: School of Chemical Engineering, Seoul National University, Seoul 151-742, Korea – sequence: 3 givenname: Junkyung surname: Kim fullname: Kim, Junkyung email: jkkim@kistmail.kist.re.kr organization: Polymer Hybrids Research Center, Korea Institute of Science and Technology, 39-1 Hawolgok-dong, Sungbuk-gu, Seoul 136-791, Korea – sequence: 4 givenname: Sang-Soo surname: Lee fullname: Lee, Sang-Soo organization: Polymer Hybrids Research Center, Korea Institute of Science and Technology, 39-1 Hawolgok-dong, Sungbuk-gu, Seoul 136-791, Korea – sequence: 5 givenname: Min surname: Park fullname: Park, Min organization: Polymer Hybrids Research Center, Korea Institute of Science and Technology, 39-1 Hawolgok-dong, Sungbuk-gu, Seoul 136-791, Korea – sequence: 6 givenname: Soonho surname: Lim fullname: Lim, Soonho organization: Polymer Hybrids Research Center, Korea Institute of Science and Technology, 39-1 Hawolgok-dong, Sungbuk-gu, Seoul 136-791, Korea – sequence: 7 givenname: Chul Rim surname: Choe fullname: Choe, Chul Rim organization: Polymer Hybrids Research Center, Korea Institute of Science and Technology, 39-1 Hawolgok-dong, Sungbuk-gu, Seoul 136-791, Korea |
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Keywords | Acrylic elastomer Crosslink density Morphology Mechanical properties Liquid rubber Epoxy resin Property structure relationship Nitrile rubber Experimental study Adhesive Fracture energy Modified material |
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SubjectTerms | Applied sciences Exact sciences and technology formulation interfacial failure Mechanical properties Organic polymers Physicochemistry of polymers Properties and characterization rubber agglomeration rubber-toughened epoxy adhesive |
Title | Effect of molecular weight between crosslinks on the fracture behavior of rubber-toughened epoxy adhesives |
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