Biodegradable epoxy resin from vanillin with excellent flame-retardant and outstanding mechanical properties
•A bio-based aromatic thermoset epoxy resin(MVE) was synthesized from Schiff base compound.•Schiff base and melamine structure promote carbonization and reduce fire hazard of thermoset epoxy resin.•The new epoxy thermoset exhibits superior mechanical properties and advantageous degradability.•This p...
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| Published in | Polymer degradation and stability Vol. 201; p. 109989 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.07.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | •A bio-based aromatic thermoset epoxy resin(MVE) was synthesized from Schiff base compound.•Schiff base and melamine structure promote carbonization and reduce fire hazard of thermoset epoxy resin.•The new epoxy thermoset exhibits superior mechanical properties and advantageous degradability.•This paper provides a new strategy for simultaneously enhancing the mechanical properties and fire-safety performance.
In this work, the sustainable and biodegradable flame retardant epoxy resin was designed and prepared to replace resource-limited petrochemicals, especially, bisphenol A type epoxy resin (DGEBA). A renewable chemical, vanillin was condensation to produce Schiff-based compound (MAV) employing the novel epoxy resin (MVE) through the epoxidation reaction. The epoxy equivalent of MVE was approximately 217 g/eq and used non-isothermal differential scanning calorimetry (DSC) to study the curing kinetics of MVE/DDM (4,4′-Diaminodiphenylmethane). After curing by DDM, they exhibit outstanding mechanical property and a residual char rate as high as 41.77%, excellent inherent flame retardancy and limited oxygen index (LOI) value higher than 34%, far superior to DGEBA. The total heat release (THR) and smoke release rate (SPR) of MVE/DDM decreased by 67.44% and 64.69% compared with DGEBA/DDM, respectively. The mechanisms for the enhancement of flame retardancy by intrinsic flame retardant epoxy resin were investigated. Moreover, the sustainable epoxy crosslinking could degrade completely benefited from the structure of the Schiff base in the moderate conditions (THF: H2O = 6: 4, 50 °C) within few hours. Overall, this work contributes a multifunctional vanillin-based epoxy monomer and environmentally friendly thermosets with high mechanical property and enhanced flame retardancy.
Main performance roadmap of degradable epoxy resin. [Display omitted] |
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| AbstractList | In this work, the sustainable and biodegradable flame retardant epoxy resin was designed and prepared to replace resource-limited petrochemicals, especially, bisphenol A type epoxy resin (DGEBA). A renewable chemical, vanillin was condensation to produce Schiff-based compound (MAV) employing the novel epoxy resin (MVE) through the epoxidation reaction. The epoxy equivalent of MVE was approximately 217 g/eq and used non-isothermal differential scanning calorimetry (DSC) to study the curing kinetics of MVE/DDM (4,4′-Diaminodiphenylmethane). After curing by DDM, they exhibit outstanding mechanical property and a residual char rate as high as 41.77%, excellent inherent flame retardancy and limited oxygen index (LOI) value higher than 34%, far superior to DGEBA. The total heat release (THR) and smoke release rate (SPR) of MVE/DDM decreased by 67.44% and 64.69% compared with DGEBA/DDM, respectively. The mechanisms for the enhancement of flame retardancy by intrinsic flame retardant epoxy resin were investigated. Moreover, the sustainable epoxy crosslinking could degrade completely benefited from the structure of the Schiff base in the moderate conditions (THF: H₂O = 6: 4, 50 °C) within few hours. Overall, this work contributes a multifunctional vanillin-based epoxy monomer and environmentally friendly thermosets with high mechanical property and enhanced flame retardancy. •A bio-based aromatic thermoset epoxy resin(MVE) was synthesized from Schiff base compound.•Schiff base and melamine structure promote carbonization and reduce fire hazard of thermoset epoxy resin.•The new epoxy thermoset exhibits superior mechanical properties and advantageous degradability.•This paper provides a new strategy for simultaneously enhancing the mechanical properties and fire-safety performance. In this work, the sustainable and biodegradable flame retardant epoxy resin was designed and prepared to replace resource-limited petrochemicals, especially, bisphenol A type epoxy resin (DGEBA). A renewable chemical, vanillin was condensation to produce Schiff-based compound (MAV) employing the novel epoxy resin (MVE) through the epoxidation reaction. The epoxy equivalent of MVE was approximately 217 g/eq and used non-isothermal differential scanning calorimetry (DSC) to study the curing kinetics of MVE/DDM (4,4′-Diaminodiphenylmethane). After curing by DDM, they exhibit outstanding mechanical property and a residual char rate as high as 41.77%, excellent inherent flame retardancy and limited oxygen index (LOI) value higher than 34%, far superior to DGEBA. The total heat release (THR) and smoke release rate (SPR) of MVE/DDM decreased by 67.44% and 64.69% compared with DGEBA/DDM, respectively. The mechanisms for the enhancement of flame retardancy by intrinsic flame retardant epoxy resin were investigated. Moreover, the sustainable epoxy crosslinking could degrade completely benefited from the structure of the Schiff base in the moderate conditions (THF: H2O = 6: 4, 50 °C) within few hours. Overall, this work contributes a multifunctional vanillin-based epoxy monomer and environmentally friendly thermosets with high mechanical property and enhanced flame retardancy. Main performance roadmap of degradable epoxy resin. [Display omitted] |
| ArticleNumber | 109989 |
| Author | Yu, Liangliang Liu, Zhe Liu, Ning Ao, Yuhui Ma, Jinpeng Hua, Xueni Shang, Lei Li, Guanxi Zhang, Fan Chen, Xue |
| Author_xml | – sequence: 1 givenname: Jinpeng surname: Ma fullname: Ma, Jinpeng organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 2 givenname: Guanxi surname: Li fullname: Li, Guanxi organization: JiLin GuoXing Composite Materials Co., Ltd., Jilin, 132002, China – sequence: 3 givenname: Xueni surname: Hua fullname: Hua, Xueni organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 4 givenname: Ning surname: Liu fullname: Liu, Ning organization: JiLin GuoXing Composite Materials Co., Ltd., Jilin, 132002, China – sequence: 5 givenname: Zhe surname: Liu fullname: Liu, Zhe organization: JiLin GuoXing Composite Materials Co., Ltd., Jilin, 132002, China – sequence: 6 givenname: Fan surname: Zhang fullname: Zhang, Fan organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 7 givenname: Liangliang surname: Yu fullname: Yu, Liangliang organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 8 givenname: Xue surname: Chen fullname: Chen, Xue organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 9 givenname: Lei surname: Shang fullname: Shang, Lei email: shanglei@ccut.edu.cn organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China – sequence: 10 givenname: Yuhui surname: Ao fullname: Ao, Yuhui email: aoyuhui@ccut.edu.cn organization: College of Chemistry and Life Science, Jilin Province Key Laboratory of Carbon Fiber Development and Application, Changchun University of Technology, Changchun, 130012, People's Republic of China |
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| Snippet | •A bio-based aromatic thermoset epoxy resin(MVE) was synthesized from Schiff base compound.•Schiff base and melamine structure promote carbonization and reduce... In this work, the sustainable and biodegradable flame retardant epoxy resin was designed and prepared to replace resource-limited petrochemicals, especially,... |
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| SubjectTerms | Bio-based epoxy resin biodegradability bisphenol A crosslinking degradation epoxidation reactions epoxides flame retardants Flame-retardant material heat Mechanical properties oxygen polymers Schiff schiff bases smoke vanillin |
| Title | Biodegradable epoxy resin from vanillin with excellent flame-retardant and outstanding mechanical properties |
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