Au@Carbon quantum Dots-MXene nanocomposite as an electrochemical sensor for sensitive detection of nitrite
[Display omitted] A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles...
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| Published in | Journal of colloid and interface science Vol. 607; no. Pt 2; pp. 1313 - 1322 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.02.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles (Au@CQDs). MXene of good electrical conductivity was used as the immobilized matrix to fabricate Au@CQDs-MXene nanocomposites with the advantages of good electrical conductivity and electrocatalysis. An electrochemical sensor for nitrite monitor was obtained by loading the Au@CQDs-MXene on a glassy carbon electrode. The sensor presents high sensitivity, good stability, wide linear range, and excellent selectivity due to the high catalytic activity of AuNPs and CQDs, the large specific surface area of MXene, and exceptional electrical conductivity of AuNPs and MXene. Under the optimal condition, the linear detection range of the sensor was from 1 μM to 3200 μM with a detection limit of 0.078 μM (S/N = 3), which was superior to most reported sensors using differential pulse voltammetry (DPV) method. Furthermore, this sensor was successfully applied to detect nitrite in tap water and salted vegetables with satisfactory recoveries. This modified electrocatalytic sensor shows a new pathway to fabricate nitrite detection sensor with feasibility for practical application. |
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| AbstractList | A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles (Au@CQDs). MXene of good electrical conductivity was used as the immobilized matrix to fabricate Au@CQDs-MXene nanocomposites with the advantages of good electrical conductivity and electrocatalysis. An electrochemical sensor for nitrite monitor was obtained by loading the Au@CQDs-MXene on a glassy carbon electrode. The sensor presents high sensitivity, good stability, wide linear range, and excellent selectivity due to the high catalytic activity of AuNPs and CQDs, the large specific surface area of MXene, and exceptional electrical conductivity of AuNPs and MXene. Under the optimal condition, the linear detection range of the sensor was from 1 μM to 3200 μM with a detection limit of 0.078 μM (S/N = 3), which was superior to most reported sensors using differential pulse voltammetry (DPV) method. Furthermore, this sensor was successfully applied to detect nitrite in tap water and salted vegetables with satisfactory recoveries. This modified electrocatalytic sensor shows a new pathway to fabricate nitrite detection sensor with feasibility for practical application.A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles (Au@CQDs). MXene of good electrical conductivity was used as the immobilized matrix to fabricate Au@CQDs-MXene nanocomposites with the advantages of good electrical conductivity and electrocatalysis. An electrochemical sensor for nitrite monitor was obtained by loading the Au@CQDs-MXene on a glassy carbon electrode. The sensor presents high sensitivity, good stability, wide linear range, and excellent selectivity due to the high catalytic activity of AuNPs and CQDs, the large specific surface area of MXene, and exceptional electrical conductivity of AuNPs and MXene. Under the optimal condition, the linear detection range of the sensor was from 1 μM to 3200 μM with a detection limit of 0.078 μM (S/N = 3), which was superior to most reported sensors using differential pulse voltammetry (DPV) method. Furthermore, this sensor was successfully applied to detect nitrite in tap water and salted vegetables with satisfactory recoveries. This modified electrocatalytic sensor shows a new pathway to fabricate nitrite detection sensor with feasibility for practical application. A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles (Au@CQDs). MXene of good electrical conductivity was used as the immobilized matrix to fabricate Au@CQDs-MXene nanocomposites with the advantages of good electrical conductivity and electrocatalysis. An electrochemical sensor for nitrite monitor was obtained by loading the Au@CQDs-MXene on a glassy carbon electrode. The sensor presents high sensitivity, good stability, wide linear range, and excellent selectivity due to the high catalytic activity of AuNPs and CQDs, the large specific surface area of MXene, and exceptional electrical conductivity of AuNPs and MXene. Under the optimal condition, the linear detection range of the sensor was from 1 μM to 3200 μM with a detection limit of 0.078 μM (S/N = 3), which was superior to most reported sensors using differential pulse voltammetry (DPV) method. Furthermore, this sensor was successfully applied to detect nitrite in tap water and salted vegetables with satisfactory recoveries. This modified electrocatalytic sensor shows a new pathway to fabricate nitrite detection sensor with feasibility for practical application. [Display omitted] A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique. Xylan-based carbon quantum dots (CQDs) were used as green in situ reducing agent to prepare CQDs capped gold nanoparticles (Au@CQDs). MXene of good electrical conductivity was used as the immobilized matrix to fabricate Au@CQDs-MXene nanocomposites with the advantages of good electrical conductivity and electrocatalysis. An electrochemical sensor for nitrite monitor was obtained by loading the Au@CQDs-MXene on a glassy carbon electrode. The sensor presents high sensitivity, good stability, wide linear range, and excellent selectivity due to the high catalytic activity of AuNPs and CQDs, the large specific surface area of MXene, and exceptional electrical conductivity of AuNPs and MXene. Under the optimal condition, the linear detection range of the sensor was from 1 μM to 3200 μM with a detection limit of 0.078 μM (S/N = 3), which was superior to most reported sensors using differential pulse voltammetry (DPV) method. Furthermore, this sensor was successfully applied to detect nitrite in tap water and salted vegetables with satisfactory recoveries. This modified electrocatalytic sensor shows a new pathway to fabricate nitrite detection sensor with feasibility for practical application. |
| Author | Han, Guangda Cai, Jihai Feng, Xiwen Wang, Xiaoying |
| Author_xml | – sequence: 1 givenname: Xiwen surname: Feng fullname: Feng, Xiwen – sequence: 2 givenname: Guangda surname: Han fullname: Han, Guangda – sequence: 3 givenname: Jihai surname: Cai fullname: Cai, Jihai – sequence: 4 givenname: Xiaoying surname: Wang fullname: Wang, Xiaoying email: xyw@scut.edu.cn |
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| Copyright | 2021 Elsevier Inc. Copyright © 2021 Elsevier Inc. All rights reserved. |
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| Keywords | Au@CQDs-MXene nanocomposites Sensitive detection One-pot green synthesis |
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A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the... A highly sensitive electrochemical sensor was developed through a one-pot green synthesis method for nitrite detection based on the electrochemical technique.... |
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| SubjectTerms | Au@CQDs-MXene nanocomposites catalytic activity detection limit electrical conductivity electrochemistry glassy carbon electrode nanocomposites nanogold nitrites One-pot green synthesis Sensitive detection sensors (equipment) surface area tap water voltammetry |
| Title | Au@Carbon quantum Dots-MXene nanocomposite as an electrochemical sensor for sensitive detection of nitrite |
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