Surface Restructuring Prussian Blue Analog-derived Bimetallic CoFe Phosphides by N-doped Graphene Quantum Dots for Electroactive Hydrogen Evolving Catalyst
[Display omitted] •A novel PBA-derived CoFe phosphides has been developed for hydrogen evolution reaction.•The catalytic activity of the PBA-derived phosphides has been significantly enhanced by NGQD.•The role of NGQD in inducing surface restructuring of the CoFeP has been investigated by XAS.•The s...
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| Published in | Journal of colloid and interface science Vol. 654; no. Pt A; pp. 677 - 687 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
15.01.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•A novel PBA-derived CoFe phosphides has been developed for hydrogen evolution reaction.•The catalytic activity of the PBA-derived phosphides has been significantly enhanced by NGQD.•The role of NGQD in inducing surface restructuring of the CoFeP has been investigated by XAS.•The surface-restructuring NGQD/CoFeP exhibit remarkable HER activity and stability.
As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application, alternating platinum in the acidic environment. Transition metal phosphides (TMPs) are one kind of earth-abundant, nonprecious-based catalyst which has been classified as a viable alternative and active for HER. While the performance remains inferior to Pt which primarily targets durability under high current density, pinpointing the reconfiguration strategy would be critical to their catalytic competency. Herein, we reported engineered N-doped graphene quantum dots (NGQD) on the surface of bimetallic CoFe phosphide (CoFeP) derived from bimetallic cobalt iron Prussian blue analogue (CoFePBA) as an efficient HER. By introducing the NGQD, the surface architect and electronic state of the transition metal are altered through an adjusted electronic configuration and thus, improving the electrocatalytic activity. The X-ray absorption spectroscopy (XAS) highlighting the role of NGQD, which successfully induced the electron density of Co atoms, further expedites its conductivity and electroactivity. The optimized NGQD/CoFeP substantially surpasses an overpotential of 70 mV (vs. RHE) at the current density of 10 mA cm-2 in 0.5M H2SO4. Furthermore, the NGQD/CoFeP maintains its exceptional stability under an extremely high current density of 600 mA cm-2 after 12 hours of continuous operation. Our findings show that NGQD/CoFeP might demonstrate as a viable alternative to the conventional Pt electrocatalyst in commercial water splitting for hydrogen generation. |
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| AbstractList | [Display omitted]
•A novel PBA-derived CoFe phosphides has been developed for hydrogen evolution reaction.•The catalytic activity of the PBA-derived phosphides has been significantly enhanced by NGQD.•The role of NGQD in inducing surface restructuring of the CoFeP has been investigated by XAS.•The surface-restructuring NGQD/CoFeP exhibit remarkable HER activity and stability.
As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application, alternating platinum in the acidic environment. Transition metal phosphides (TMPs) are one kind of earth-abundant, nonprecious-based catalyst which has been classified as a viable alternative and active for HER. While the performance remains inferior to Pt which primarily targets durability under high current density, pinpointing the reconfiguration strategy would be critical to their catalytic competency. Herein, we reported engineered N-doped graphene quantum dots (NGQD) on the surface of bimetallic CoFe phosphide (CoFeP) derived from bimetallic cobalt iron Prussian blue analogue (CoFePBA) as an efficient HER. By introducing the NGQD, the surface architect and electronic state of the transition metal are altered through an adjusted electronic configuration and thus, improving the electrocatalytic activity. The X-ray absorption spectroscopy (XAS) highlighting the role of NGQD, which successfully induced the electron density of Co atoms, further expedites its conductivity and electroactivity. The optimized NGQD/CoFeP substantially surpasses an overpotential of 70 mV (vs. RHE) at the current density of 10 mA cm-2 in 0.5M H2SO4. Furthermore, the NGQD/CoFeP maintains its exceptional stability under an extremely high current density of 600 mA cm-2 after 12 hours of continuous operation. Our findings show that NGQD/CoFeP might demonstrate as a viable alternative to the conventional Pt electrocatalyst in commercial water splitting for hydrogen generation. As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application, alternating Pt in the acidic environment. Transition metal phosphides (TMPs) are one kind of earth-abundant, nonprecious-based catalyst which has been classified as a viable alternative and active for HER. While the performance remains inferior to Pt which primarily targets durability under high current density, pinpointing the reconfiguration strategy would be critical to their catalytic competency. Herein, we reported engineered N-doped graphene quantum dots (NGQD) on the surface of bimetallic CoFe phosphide (CoFeP) derived from cobalt iron Prussian blue analogue (CoFePBA) as an efficient HER. By introducing the NGQD, the surface architect and electronic state of the transition metal are altered through an adjusted electronic configuration and thus, improving the electrocatalytic activity for HER. The X-ray absorption spectroscopy (XAS) highlighting the role of NGQD, which successfully induced the electron density of Co atoms, further expedites its conductivity and electroactivity. The optimized NGQD/CoFeP substantially surpasses an overpotential of 70 mV (vs. RHE) at the current density of 10 mA cm⁻² in 0.5 M H₂SO₄. Furthermore, the NGQD/CoFeP maintains its exceptional stability under an extremely high current density of 600 mA cm⁻² after 12 h of continuous operation. Our findings show that NGQD/CoFeP might demonstrate as a viable alternative to the conventional Pt electrocatalyst in commercial water splitting for hydrogen generation. As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application, alternating Pt in the acidic environment. Transition metal phosphides (TMPs) are one kind of earth-abundant, nonprecious-based catalyst which has been classified as a viable alternative and active for HER. While the performance remains inferior to Pt which primarily targets durability under high current density, pinpointing the reconfiguration strategy would be critical to their catalytic competency. Herein, we reported engineered N-doped graphene quantum dots (NGQD) on the surface of bimetallic CoFe phosphide (CoFeP) derived from cobalt iron Prussian blue analogue (CoFePBA) as an efficient HER. By introducing the NGQD, the surface architect and electronic state of the transition metal are altered through an adjusted electronic configuration and thus, improving the electrocatalytic activity for HER. The X-ray absorption spectroscopy (XAS) highlighting the role of NGQD, which successfully induced the electron density of Co atoms, further expedites its conductivity and electroactivity. The optimized NGQD/CoFeP substantially surpasses an overpotential of 70 mV (vs. RHE) at the current density of 10 mA cm-2 in 0.5 M H2SO4. Furthermore, the NGQD/CoFeP maintains its exceptional stability under an extremely high current density of 600 mA cm-2 after 12 h of continuous operation. Our findings show that NGQD/CoFeP might demonstrate as a viable alternative to the conventional Pt electrocatalyst in commercial water splitting for hydrogen generation.As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application, alternating Pt in the acidic environment. Transition metal phosphides (TMPs) are one kind of earth-abundant, nonprecious-based catalyst which has been classified as a viable alternative and active for HER. While the performance remains inferior to Pt which primarily targets durability under high current density, pinpointing the reconfiguration strategy would be critical to their catalytic competency. Herein, we reported engineered N-doped graphene quantum dots (NGQD) on the surface of bimetallic CoFe phosphide (CoFeP) derived from cobalt iron Prussian blue analogue (CoFePBA) as an efficient HER. By introducing the NGQD, the surface architect and electronic state of the transition metal are altered through an adjusted electronic configuration and thus, improving the electrocatalytic activity for HER. The X-ray absorption spectroscopy (XAS) highlighting the role of NGQD, which successfully induced the electron density of Co atoms, further expedites its conductivity and electroactivity. The optimized NGQD/CoFeP substantially surpasses an overpotential of 70 mV (vs. RHE) at the current density of 10 mA cm-2 in 0.5 M H2SO4. Furthermore, the NGQD/CoFeP maintains its exceptional stability under an extremely high current density of 600 mA cm-2 after 12 h of continuous operation. Our findings show that NGQD/CoFeP might demonstrate as a viable alternative to the conventional Pt electrocatalyst in commercial water splitting for hydrogen generation. |
| Author | Lin, Wei-Shiang Chen, Jeng-Lung Rinawati, Mia Chang, Ching-Cheng Cheng, Yao-Sheng Yeh, Min-Hsin Huang, Wei-Hsiang Chang, Chia-Yu Chang, Ling-Yu Su, Wei-Nien |
| Author_xml | – sequence: 1 givenname: Wei-Shiang surname: Lin fullname: Lin, Wei-Shiang organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 2 givenname: Mia surname: Rinawati fullname: Rinawati, Mia organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 3 givenname: Wei-Hsiang surname: Huang fullname: Huang, Wei-Hsiang organization: National Synchrotron Radiation Research Center, Hsinchu 30076, Taiwan – sequence: 4 givenname: Chia-Yu surname: Chang fullname: Chang, Chia-Yu organization: Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 5 givenname: Ling-Yu surname: Chang fullname: Chang, Ling-Yu email: linui1008@gmail.com organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 6 givenname: Yao-Sheng surname: Cheng fullname: Cheng, Yao-Sheng organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 7 givenname: Ching-Cheng surname: Chang fullname: Chang, Ching-Cheng organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 8 givenname: Jeng-Lung orcidid: 0000-0002-0223-5538 surname: Chen fullname: Chen, Jeng-Lung organization: National Synchrotron Radiation Research Center, Hsinchu 30076, Taiwan – sequence: 9 givenname: Wei-Nien surname: Su fullname: Su, Wei-Nien email: wsu@mail.ntust.edu.tw organization: Graduate Institute of Applied Science and Technology, National Taiwan University of Science and Technology, Taipei 10607, Taiwan – sequence: 10 givenname: Min-Hsin orcidid: 0000-0002-6150-4750 surname: Yeh fullname: Yeh, Min-Hsin email: mhyeh@mail.ntust.edu.tw organization: Department of Chemical Engineering, National Taiwan University of Science and Technology, Taipei 10607, Taiwan |
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| Keywords | N-doped graphene quantum dots electrocatalyst Prussian blue analogues transition metal phosphides X-ray absorption spectroscopy hydrogen evolution reaction |
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•A novel PBA-derived CoFe phosphides has been developed for hydrogen evolution reaction.•The catalytic activity of the PBA-derived phosphides... As a crucial stage of electrochemical water splitting, hydrogen evolution reaction (HER) favour catalyst to attain rapid kinetics for its broader application,... |
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| SubjectTerms | catalysts cobalt durability electrocatalyst electrochemistry graphene hydrogen hydrogen evolution reaction hydrogen production N-doped graphene quantum dots phosphides Prussian blue analogues transition metal phosphides X-ray absorption spectroscopy |
| Title | Surface Restructuring Prussian Blue Analog-derived Bimetallic CoFe Phosphides by N-doped Graphene Quantum Dots for Electroactive Hydrogen Evolving Catalyst |
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