Construction of 2D/1D Cu7S4 nanosheets/Mn0.3Cd0.7S nanorods heterojunction for highly efficient photocatalytic hydrogen evolution
[Display omitted] Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu7S4/Mn0.3Cd0.7S hierarchical heterostruct...
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| Published in | Journal of colloid and interface science Vol. 653; no. Pt B; pp. 1304 - 1316 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.01.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu7S4/Mn0.3Cd0.7S hierarchical heterostructures are designed and fabricated to achieve efficient and robust photocatalytic H2 evolution by coupling one-dimensional (1D) Mn0.3Cd0.7S nanorods with two-dimensional (2D) Cu7S4 nanosheets through a facile sonochemical strategy. Benefiting from dimensionality and cocatalyst effects, the constructed 2D/1D Cu7S4/Mn0.3Cd0.7S heterojunction photocatalyst containing 1.5 wt% Cu7S4 displays excellent photostability and superior photocatalytic H2 evolution rate up to 914.3 μmol h−1, which is 4.43 and 2.22-folds increment relative to bare Mn0.3Cd0.7S and the 3 wt% Pt/Mn0.3Cd0.7S, respectively. The various characterization results reveal that the utilization of semimetallic Cu7S4 nanosheets as the cocatalyst to form a Schottky heterojunction can promote the light-harvesting capability, suppress charge carrier recombination, and provide sufficient reaction sites for hydrogen generation, thereby resulting in the dramatically improved photocatalytic performance. This work clarifies the role of Cu7S4 nanosheets as the robust and cost-effective cocatalyst in the photocatalytic reaction and opens a new horizon for designing other Cu7S4-based cocatalyst/semiconductor Schottky heterostructures for efficient solar-to-fuel conversion. |
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| AbstractList | Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu7S4/Mn0.3Cd0.7S hierarchical heterostructures are designed and fabricated to achieve efficient and robust photocatalytic H2 evolution by coupling one-dimensional (1D) Mn0.3Cd0.7S nanorods with two-dimensional (2D) Cu7S4 nanosheets through a facile sonochemical strategy. Benefiting from dimensionality and cocatalyst effects, the constructed 2D/1D Cu7S4/Mn0.3Cd0.7S heterojunction photocatalyst containing 1.5 wt% Cu7S4 displays excellent photostability and superior photocatalytic H2 evolution rate up to 914.3 μmol h-1, which is 4.43 and 2.22-folds increment relative to bare Mn0.3Cd0.7S and the 3 wt% Pt/Mn0.3Cd0.7S, respectively. The various characterization results reveal that the utilization of semimetallic Cu7S4 nanosheets as the cocatalyst to form a Schottky heterojunction can promote the light-harvesting capability, suppress charge carrier recombination, and provide sufficient reaction sites for hydrogen generation, thereby resulting in the dramatically improved photocatalytic performance. This work clarifies the role of Cu7S4 nanosheets as the robust and cost-effective cocatalyst in the photocatalytic reaction and opens a new horizon for designing other Cu7S4-based cocatalyst/semiconductor Schottky heterostructures for efficient solar-to-fuel conversion.Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu7S4/Mn0.3Cd0.7S hierarchical heterostructures are designed and fabricated to achieve efficient and robust photocatalytic H2 evolution by coupling one-dimensional (1D) Mn0.3Cd0.7S nanorods with two-dimensional (2D) Cu7S4 nanosheets through a facile sonochemical strategy. Benefiting from dimensionality and cocatalyst effects, the constructed 2D/1D Cu7S4/Mn0.3Cd0.7S heterojunction photocatalyst containing 1.5 wt% Cu7S4 displays excellent photostability and superior photocatalytic H2 evolution rate up to 914.3 μmol h-1, which is 4.43 and 2.22-folds increment relative to bare Mn0.3Cd0.7S and the 3 wt% Pt/Mn0.3Cd0.7S, respectively. The various characterization results reveal that the utilization of semimetallic Cu7S4 nanosheets as the cocatalyst to form a Schottky heterojunction can promote the light-harvesting capability, suppress charge carrier recombination, and provide sufficient reaction sites for hydrogen generation, thereby resulting in the dramatically improved photocatalytic performance. This work clarifies the role of Cu7S4 nanosheets as the robust and cost-effective cocatalyst in the photocatalytic reaction and opens a new horizon for designing other Cu7S4-based cocatalyst/semiconductor Schottky heterostructures for efficient solar-to-fuel conversion. [Display omitted] Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu7S4/Mn0.3Cd0.7S hierarchical heterostructures are designed and fabricated to achieve efficient and robust photocatalytic H2 evolution by coupling one-dimensional (1D) Mn0.3Cd0.7S nanorods with two-dimensional (2D) Cu7S4 nanosheets through a facile sonochemical strategy. Benefiting from dimensionality and cocatalyst effects, the constructed 2D/1D Cu7S4/Mn0.3Cd0.7S heterojunction photocatalyst containing 1.5 wt% Cu7S4 displays excellent photostability and superior photocatalytic H2 evolution rate up to 914.3 μmol h−1, which is 4.43 and 2.22-folds increment relative to bare Mn0.3Cd0.7S and the 3 wt% Pt/Mn0.3Cd0.7S, respectively. The various characterization results reveal that the utilization of semimetallic Cu7S4 nanosheets as the cocatalyst to form a Schottky heterojunction can promote the light-harvesting capability, suppress charge carrier recombination, and provide sufficient reaction sites for hydrogen generation, thereby resulting in the dramatically improved photocatalytic performance. This work clarifies the role of Cu7S4 nanosheets as the robust and cost-effective cocatalyst in the photocatalytic reaction and opens a new horizon for designing other Cu7S4-based cocatalyst/semiconductor Schottky heterostructures for efficient solar-to-fuel conversion. Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy for effectively converting solar energy into desired fuels. Herein, a series of Cu₇S₄/Mn₀.₃Cd₀.₇S hierarchical heterostructures are designed and fabricated to achieve efficient and robust photocatalytic H₂ evolution by coupling one-dimensional (1D) Mn₀.₃Cd₀.₇S nanorods with two-dimensional (2D) Cu₇S₄ nanosheets through a facile sonochemical strategy. Benefiting from dimensionality and cocatalyst effects, the constructed 2D/1D Cu₇S₄/Mn₀.₃Cd₀.₇S heterojunction photocatalyst containing 1.5 wt% Cu₇S₄ displays excellent photostability and superior photocatalytic H₂ evolution rate up to 914.3 μmol h⁻¹, which is 4.43 and 2.22-folds increment relative to bare Mn₀.₃Cd₀.₇S and the 3 wt% Pt/Mn₀.₃Cd₀.₇S, respectively. The various characterization results reveal that the utilization of semimetallic Cu₇S₄ nanosheets as the cocatalyst to form a Schottky heterojunction can promote the light-harvesting capability, suppress charge carrier recombination, and provide sufficient reaction sites for hydrogen generation, thereby resulting in the dramatically improved photocatalytic performance. This work clarifies the role of Cu₇S₄ nanosheets as the robust and cost-effective cocatalyst in the photocatalytic reaction and opens a new horizon for designing other Cu₇S₄-based cocatalyst/semiconductor Schottky heterostructures for efficient solar-to-fuel conversion. |
| Author | Wang, Guangtao Zhang, Fubiao Wang, Lanlan Wang, Gongke Lv, Hua Zhan, Mingyan Liu, Yumin Shen, Qinhui Li, Guanyong |
| Author_xml | – sequence: 1 givenname: Hua surname: Lv fullname: Lv, Hua organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 2 givenname: Fubiao surname: Zhang fullname: Zhang, Fubiao organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 3 givenname: Lanlan surname: Wang fullname: Wang, Lanlan organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 4 givenname: Qinhui surname: Shen fullname: Shen, Qinhui organization: College of Physics, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 5 givenname: Guanyong surname: Li fullname: Li, Guanyong organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 6 givenname: Mingyan surname: Zhan fullname: Zhan, Mingyan organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 7 givenname: Gongke surname: Wang fullname: Wang, Gongke email: wanggongke@126.com organization: School of Materials Science and Engineering, Henan Engineering Research Center of Design and Recycle for Advanced Electrochemical Energy Storage Materials, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 8 givenname: Guangtao surname: Wang fullname: Wang, Guangtao email: wangtao@htu.cn organization: College of Physics, Henan Normal University, Xinxiang, Henan 453007, China – sequence: 9 givenname: Yumin orcidid: 0000-0003-0953-2532 surname: Liu fullname: Liu, Yumin email: ymliu2007@163.com organization: Collaborative Innovation Center of Henan Province for Green Manufacturing of Fine Chemicals, Key Laboratory of Green Chemical Media and Reactions, Ministry of Education, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China |
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Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is... Developing cost-effective cocatalyst-modified photocatalytic systems with boosted carrier separation and rapid surface catalytic reaction is an ideal strategy... |
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| SubjectTerms | Cocatalyst cost effectiveness Cu7S4 Heterojunction hydrogen production Mechanism Mn0.3Cd0.7S nanorods nanosheets photocatalysis photocatalysts photostability semiconductors solar energy |
| Title | Construction of 2D/1D Cu7S4 nanosheets/Mn0.3Cd0.7S nanorods heterojunction for highly efficient photocatalytic hydrogen evolution |
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