Heavy metals immobilization of ternary geopolymer based on nickel slag, lithium slag and metakaolin

To solve heavy metals leaching problem in the utilization of various industrial solid wastes, this work investigated the heavy metals immobilization of ternary geopolymer prepared by nickel slag (NS), lithium slag (LS), and metakaolin (MK). Compressive strength was measured to determine the optimum...

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Published inJournal of hazardous materials Vol. 453; p. 131380
Main Authors Fan, Jinyuan, Yan, Jiahao, Zhou, Mengya, Xu, Yuan, Lu, Yuwei, Duan, Ping, Zhu, Yingcan, Zhang, Zuhua, Li, Wengui, Wang, Aiguo, Sun, Daosheng
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 05.07.2023
Subjects
Compressive strength
Heavy metals immobilization
Lithium slag
Nickel slag
Ternary geopolymer
Heavy metals immobilization
Nickel slag
Compressive strength
Lithium slag
Ternary geopolymer
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Abstract To solve heavy metals leaching problem in the utilization of various industrial solid wastes, this work investigated the heavy metals immobilization of ternary geopolymer prepared by nickel slag (NS), lithium slag (LS), and metakaolin (MK). Compressive strength was measured to determine the optimum and appropriate mix proportions. The leaching characteristics of typical heavy metals (Cu (Ⅱ), Pb (Ⅱ), and Cr (Ⅲ)) in acid, alkali, and salt environments were revealed by Inductively Coupled Plasma (ICP). The heavy metals immobilization mechanism was explored by Mercury Intrusion Porosimetry (MIP), X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), and Scanning Electron Microscopy (SEM) tests. The experimental results show that the group with a mass ratio of NS, LS and MK of 1:1:8 exhibits the highest compressive strength, which reaches 69.1 MPa at 28 d. The ternary geopolymer possesses a desirable capacity for immobilizing inherent heavy metals, where the immobilization rates of Cu and Pb reach 96.69 %, and that of Cr reaches 99.97 %. The leaching concentrations of Cr and Pb increase when the samples are exposed to acidic and alkaline environments. Cu and Pb are mainly physically encapsulated in geopolymer. Additionally, immobilization of Cr mainly involves physical encapsulation and chemical bonding. [Display omitted] •Using multiple industrial solid wastes as precursors to prepare ternary geopolymer.•28-day immobilization rates achieve 96.69 % for Cu and Pb and 99.97 % for Cr.•Compressive strength of the geopolymer with 2.0 wt % Cr decreases by 96.5 % at 28 d.•Acid, alkali, and salt environments exposure for ternary geopolymer.•Immobilization of Cr involves physically encapsulated and chemically bonded.
AbstractList To solve heavy metals leaching problem in the utilization of various industrial solid wastes, this work investigated the heavy metals immobilization of ternary geopolymer prepared by nickel slag (NS), lithium slag (LS), and metakaolin (MK). Compressive strength was measured to determine the optimum and appropriate mix proportions. The leaching characteristics of typical heavy metals (Cu (Ⅱ), Pb (Ⅱ), and Cr (Ⅲ)) in acid, alkali, and salt environments were revealed by Inductively Coupled Plasma (ICP). The heavy metals immobilization mechanism was explored by Mercury Intrusion Porosimetry (MIP), X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), and Scanning Electron Microscopy (SEM) tests. The experimental results show that the group with a mass ratio of NS, LS and MK of 1:1:8 exhibits the highest compressive strength, which reaches 69.1 MPa at 28 d. The ternary geopolymer possesses a desirable capacity for immobilizing inherent heavy metals, where the immobilization rates of Cu and Pb reach 96.69 %, and that of Cr reaches 99.97 %. The leaching concentrations of Cr and Pb increase when the samples are exposed to acidic and alkaline environments. Cu and Pb are mainly physically encapsulated in geopolymer. Additionally, immobilization of Cr mainly involves physical encapsulation and chemical bonding. [Display omitted] •Using multiple industrial solid wastes as precursors to prepare ternary geopolymer.•28-day immobilization rates achieve 96.69 % for Cu and Pb and 99.97 % for Cr.•Compressive strength of the geopolymer with 2.0 wt % Cr decreases by 96.5 % at 28 d.•Acid, alkali, and salt environments exposure for ternary geopolymer.•Immobilization of Cr involves physically encapsulated and chemically bonded.
To solve heavy metals leaching problem in the utilization of various industrial solid wastes, this work investigated the heavy metals immobilization of ternary geopolymer prepared by nickel slag (NS), lithium slag (LS), and metakaolin (MK). Compressive strength was measured to determine the optimum and appropriate mix proportions. The leaching characteristics of typical heavy metals (Cu (Ⅱ), Pb (Ⅱ), and Cr (Ⅲ)) in acid, alkali, and salt environments were revealed by Inductively Coupled Plasma (ICP). The heavy metals immobilization mechanism was explored by Mercury Intrusion Porosimetry (MIP), X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), and Scanning Electron Microscopy (SEM) tests. The experimental results show that the group with a mass ratio of NS, LS and MK of 1:1:8 exhibits the highest compressive strength, which reaches 69.1 MPa at 28 d. The ternary geopolymer possesses a desirable capacity for immobilizing inherent heavy metals, where the immobilization rates of Cu and Pb reach 96.69 %, and that of Cr reaches 99.97 %. The leaching concentrations of Cr and Pb increase when the samples are exposed to acidic and alkaline environments. Cu and Pb are mainly physically encapsulated in geopolymer. Additionally, immobilization of Cr mainly involves physical encapsulation and chemical bonding.
ArticleNumber 131380
Author Zhu, Yingcan
Zhang, Zuhua
Fan, Jinyuan
Duan, Ping
Lu, Yuwei
Xu, Yuan
Yan, Jiahao
Wang, Aiguo
Li, Wengui
Sun, Daosheng
Zhou, Mengya
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  fullname: Yan, Jiahao
  organization: Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430074, China
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  givenname: Mengya
  surname: Zhou
  fullname: Zhou, Mengya
  organization: Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430074, China
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  fullname: Xu, Yuan
  organization: Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430074, China
– sequence: 5
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  fullname: Lu, Yuwei
  organization: Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan 430074, China
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  orcidid: 0000-0003-4087-0169
  surname: Zhu
  fullname: Zhu, Yingcan
  email: zhuyc@geopoly.com.cn
  organization: Shanghai Geopoly New Materials Co., Ltd, Wisdom square, Jingan district, Shanghai 200042, China
– sequence: 8
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  fullname: Wang, Aiguo
  organization: Key Laboratory of Advanced Building Materials of Anhui Province, Anhui Jianzhu University, Hefei 230022, China
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  givenname: Daosheng
  surname: Sun
  fullname: Sun, Daosheng
  organization: Key Laboratory of Advanced Building Materials of Anhui Province, Anhui Jianzhu University, Hefei 230022, China
BackLink https://www.ncbi.nlm.nih.gov/pubmed/37043859$$D View this record in MEDLINE/PubMed
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Keywords Heavy metals immobilization
Nickel slag
Compressive strength
Lithium slag
Ternary geopolymer
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Snippet To solve heavy metals leaching problem in the utilization of various industrial solid wastes, this work investigated the heavy metals immobilization of ternary...
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SubjectTerms Compressive strength
Heavy metals immobilization
Lithium slag
Nickel slag
Ternary geopolymer
Title Heavy metals immobilization of ternary geopolymer based on nickel slag, lithium slag and metakaolin
URI https://dx.doi.org/10.1016/j.jhazmat.2023.131380
https://www.ncbi.nlm.nih.gov/pubmed/37043859
https://search.proquest.com/docview/2800626332
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