Heat-treated 2,2′-bipyridine iron complex supported on polypyrrole-coated carbon for oxygen reduction reaction
Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2′-bipyridine iron complex on polypyrrole-coated carbon support followed by pyrolysis at various temperatures (600, 700, 850, and 1000 °C). The prepared catalysts and support are characteri...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 17; no. 2; pp. 304 - 309 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.03.2011
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1226-086X 1876-794X |
| DOI | 10.1016/j.jiec.2011.02.028 |
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| Abstract | Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2′-bipyridine iron complex on polypyrrole-coated carbon support followed by pyrolysis at various temperatures (600, 700, 850, and 1000
°C). The prepared catalysts and support are characterized by IR, elementary analysis, TEM, and XPS. Revealed is that the contents of pyridinic nitrogen on a catalyst would not be a determining factor for ORR activity. The concentration of pyridinic nitrogen diminishes with the increasing pyrolysis temperature, while the ORR performance is observed to be enhanced with a maximum at 850
°C. It is believed that the pyridinic nitrogen added as a precursor should be activated to serve as an active site for ORR, indicating that an increasing pyrolysis temperature is favored to form a highly active site. However, the pyrolysis at too high of temperature (1000
°C) turns out to be undesirable due to a considerable loss of active nitrogen. |
|---|---|
| AbstractList | Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2′-bipyridine iron complex on polypyrrole-coated carbon support followed by pyrolysis at various temperatures (600, 700, 850, and 1000
°C). The prepared catalysts and support are characterized by IR, elementary analysis, TEM, and XPS. Revealed is that the contents of pyridinic nitrogen on a catalyst would not be a determining factor for ORR activity. The concentration of pyridinic nitrogen diminishes with the increasing pyrolysis temperature, while the ORR performance is observed to be enhanced with a maximum at 850
°C. It is believed that the pyridinic nitrogen added as a precursor should be activated to serve as an active site for ORR, indicating that an increasing pyrolysis temperature is favored to form a highly active site. However, the pyrolysis at too high of temperature (1000
°C) turns out to be undesirable due to a considerable loss of active nitrogen. Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2'-bipyridine iron complex on polypyrrole-coated carbon support followed by pyrolysis at various temperatures (600, 700, 850, and 1000 [deg]C). The prepared catalysts and support are characterized by IR, elementary analysis, TEM, and XPS. Revealed is that the contents of pyridinic nitrogen on a catalyst would not be a determining factor for ORR activity. The concentration of pyridinic nitrogen diminishes with the increasing pyrolysis temperature, while the ORR performance is observed to be enhanced with a maximum at 850 [deg]C. It is believed that the pyridinic nitrogen added as a precursor should be activated to serve as an active site for ORR, indicating that an increasing pyrolysis temperature is favored to form a highly active site. However, the pyrolysis at too high of temperature (1000 [deg]C) turns out to be undesirable due to a considerable loss of active nitrogen. Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,20-bipyridine iron complex on polypyrrole-coated carbon support followed by pyrolysis at various temperatures (600, 700, 850, and 1000 8C). The prepared catalysts and support are characterized by IR, elementary analysis, TEM, and XPS. Revealed is that the contents of pyridinic nitrogen on a catalyst would not be a determining factor for ORR activity. The concentration of pyridinic nitrogen diminishes with the increasing pyrolysis temperature, while the ORR performance is observed to be enhanced with a maximum at 850 8C. It is believed that the pyridinic nitrogen added as a precursor should be activated to serve as an active site for ORR, indicating that an increasing pyrolysis temperature is favored to form a highly active site. However, the pyrolysis at too high of temperature (1000 8C) turns out to be undesirable due to a considerable loss of active nitrogen. KCI Citation Count: 10 |
| Author | Heo, Kyu Chul Kim, Pil Nahm, Kee Suk Lee, Soo-Hyoung |
| Author_xml | – sequence: 1 givenname: Kyu Chul surname: Heo fullname: Heo, Kyu Chul organization: Department of Hydrogen and Fuel Cell Engineering, Specialized Graduate School, Chonbuk National University, Jeonju 561-756, South Korea – sequence: 2 givenname: Kee Suk surname: Nahm fullname: Nahm, Kee Suk organization: Department of Hydrogen and Fuel Cell Engineering, Specialized Graduate School, Chonbuk National University, Jeonju 561-756, South Korea – sequence: 3 givenname: Soo-Hyoung surname: Lee fullname: Lee, Soo-Hyoung email: shlee66@chonbuk.ac.kr organization: Department of Hydrogen and Fuel Cell Engineering, Specialized Graduate School, Chonbuk National University, Jeonju 561-756, South Korea – sequence: 4 givenname: Pil surname: Kim fullname: Kim, Pil email: kimpil1@chonbuk.ac.kr organization: Department of Hydrogen and Fuel Cell Engineering, Specialized Graduate School, Chonbuk National University, Jeonju 561-756, South Korea |
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| CitedBy_id | crossref_primary_10_1039_C7NJ01898C crossref_primary_10_1134_S1070427213100054 crossref_primary_10_1149_2_0961814jes crossref_primary_10_1016_j_elecom_2017_05_001 crossref_primary_10_1016_j_jiec_2016_08_004 crossref_primary_10_1007_s10562_012_0881_6 crossref_primary_10_1016_j_electacta_2015_08_104 crossref_primary_10_1016_j_jiec_2017_03_019 crossref_primary_10_1021_acsami_9b22615 |
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| Keywords | Pt alternative catalyst Non-noble ORR catalyst Polymer electrolyte fuel cells (PEMFCs) Bipyridine Oxygen reduction reaction (ORR) |
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| Snippet | Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2′-bipyridine iron complex on polypyrrole-coated... Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,2'-bipyridine iron complex on polypyrrole-coated... Nitrogen-containing non-noble metal catalysts for oxygen reduction reaction (ORR) are prepared by supporting 2,20-bipyridine iron complex on polypyrrole-coated... |
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| SubjectTerms | Bipyridine Carbon Catalysis Catalysts Heat treatment Iron Non-noble ORR catalyst Oxygen reduction reaction (ORR) Polymer electrolyte fuel cells (PEMFCs) Pt alternative catalyst Pyrolysis Reduction X-ray photoelectron spectroscopy 화학공학 |
| Title | Heat-treated 2,2′-bipyridine iron complex supported on polypyrrole-coated carbon for oxygen reduction reaction |
| URI | https://dx.doi.org/10.1016/j.jiec.2011.02.028 https://www.proquest.com/docview/889434645 https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART001552052 |
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