Sputtered YSZ based protective thin films for SOFCs
Protective Zr(Y)O 2-δ based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide fuel cells with silicate based solid electrolytes, where performance may suffer from surface decomposition processes in reducing atmospheres....
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Published in | Surface engineering Vol. 26; no. 8; pp. 584 - 589 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
London, England
Taylor & Francis
01.11.2010
SAGE Publications |
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Abstract | Protective Zr(Y)O
2-δ
based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide fuel cells with silicate based solid electrolytes, where performance may suffer from surface decomposition processes in reducing atmospheres. While as prepared Zr(Y)O
2-δ
films without copper additive were already crystallised and single phase, fresh Cu containing Zr(Y)O
2-δ
are essentially amorphous, requiring high temperature treatment in air for crystallisation. Deposition rate of 0·50-0·75 μm h
-1
at sputtering power of 300 W was achieved. Surface morphology studies using atomic force microscope revealed typical film structures with small (<50 nm) grains. The hardness of films decreases from 15·8 to 8·4 GPa with increasing copper content. Polarisation studies of electrochemical cell with cermet anodes, applied over protective films, suggested that electrochemical reaction is essentially governed by oxygen anion transfer from zirconia phase and/or hydrogen oxidation in vicinity of zirconia film surface. Copper incorporation into Zr(Y)O
2-δ
film leads to higher anode resistivity. |
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AbstractList | Protective Zr(Y)O
2-δ
based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide fuel cells with silicate based solid electrolytes, where performance may suffer from surface decomposition processes in reducing atmospheres. While as prepared Zr(Y)O
2-δ
films without copper additive were already crystallised and single phase, fresh Cu containing Zr(Y)O
2-δ
are essentially amorphous, requiring high temperature treatment in air for crystallisation. Deposition rate of 0·50-0·75 μm h
-1
at sputtering power of 300 W was achieved. Surface morphology studies using atomic force microscope revealed typical film structures with small (<50 nm) grains. The hardness of films decreases from 15·8 to 8·4 GPa with increasing copper content. Polarisation studies of electrochemical cell with cermet anodes, applied over protective films, suggested that electrochemical reaction is essentially governed by oxygen anion transfer from zirconia phase and/or hydrogen oxidation in vicinity of zirconia film surface. Copper incorporation into Zr(Y)O
2-δ
film leads to higher anode resistivity. Protective Zr(Y)O2–δ based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide fuel cells with silicate based solid electrolytes, where performance may suffer from surface decomposition processes in reducing atmospheres. While as prepared Zr(Y)O2–δ films without copper additive were already crystallised and single phase, fresh Cu containing Zr(Y)O2–δ are essentially amorphous, requiring high temperature treatment in air for crystallisation. Deposition rate of 0·50–0·75 μm h–1 at sputtering power of 300 W was achieved. Surface morphology studies using atomic force microscope revealed typical film structures with small (<50 nm) grains. The hardness of films decreases from 15·8 to 8·4 GPa with increasing copper content. Polarisation studies of electrochemical cell with cermet anodes, applied over protective films, suggested that electrochemical reaction is essentially governed by oxygen anion transfer from zirconia phase and/or hydrogen oxidation in vicinity of zirconia film surface. Copper incorporation into Zr(Y)O2–δ film leads to higher anode resistivity. Protective Zr(Y)O sub(2- delta ) based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide fuel cells with silicate based solid electrolytes, where performance may suffer from surface decomposition processes in reducing atmospheres. While as prepared Zr(Y)O sub(2- delta ) films without copper additive were already crystallised and single phase, fresh Cu containing Zr(Y)O sub(2- delta ) are essentially amorphous, requiring high temperature treatment in air for crystallisation. Deposition rate of 0.50-0.75 mu m h super(-1) at sputtering power of 300 W was achieved. Surface morphology studies using atomic force microscope revealed typical film structures with small (<50 nm) grains. The hardness of films decreases from 15.8 to 8.4 GPa with increasing copper content. Polarisation studies of electrochemical cell with cermet anodes, applied over protective films, suggested that electrochemical reaction is essentially governed by oxygen anion transfer from zirconia phase and/or hydrogen oxidation in vicinity of zirconia film surface. Copper incorporation into Zr(Y)O sub(2- delta ) film leads to higher anode resistivity. |
Author | Kharton, V. V. Kolotygin, V. A. Shaula, A. L. Cavaleiro, A. A. Oliveira, J. C. |
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CitedBy_id | crossref_primary_10_1016_j_apsusc_2014_03_163 crossref_primary_10_1016_j_surfcoat_2012_01_042 crossref_primary_10_1179_1743294412Y_0000000055 crossref_primary_10_1007_s10853_020_04497_7 |
Cites_doi | 10.1039/B315257J 10.1016/S0167-2738(96)00470-5 10.1016/j.ssi.2004.06.015 10.1002/ppap.200700042 10.1016/j.ssi.2004.04.013 10.1038/35005040 10.1039/b104006p 10.1016/j.jeurceramsoc.2005.03.106 10.1016/S0040-6090(96)08743-3 10.1016/S0040-6090(00)01381-X 10.1039/jm9950501801 10.1016/S0167-2738(01)00831-1 10.1016/j.jssc.2005.11.008 10.1016/j.surfcoat.2006.11.016 10.1007/s10008-003-0485-6 10.1016/S0167-2738(96)00524-3 10.1023/A:1004853019349 10.1016/j.jeurceramsoc.2005.03.114 10.1016/S0955-2219(01)00131-5 10.1016/S0167-2738(97)00248-8 10.1016/S0257-8972(96)03038-1 10.1016/S0167-2738(00)00386-6 10.1146/annurev.matsci.33.022802.091651 10.1016/j.vacuum.2006.11.001 10.1016/S0921-5107(98)00205-0 10.1016/j.tsf.2003.07.009 10.1016/j.jallcom.2004.12.180 10.1016/S0925-8388(01)01795-9 10.1016/S0257-8972(99)00501-0 10.1016/S0013-4686(00)00330-3 10.1002/1521-4095(200107)13:12/13<993::AID-ADMA993>3.0.CO;2-# 10.1149/1.1768948 10.1016/j.jssc.2005.04.018 |
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Keywords | HARDNESS YTTRIA STABILISED ZIRCONIA APATITE MAGNETRON SPUTTERING THIN FILM SOLID OXIDE FUEL CELL |
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Snippet | Protective Zr(Y)O
2-δ
based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide... Protective Zr(Y)O2–δ based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide... Protective Zr(Y)O 2– δ based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in solid oxide... Protective Zr(Y)O sub(2- delta ) based films, deposited using magnetron sputtering, onto apatite type ceramics, were appraised for potential applications in... |
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SubjectTerms | Anions Anodes APATITE Copper Crystallization Deposition HARDNESS MAGNETRON SPUTTERING Protective Protective coatings SOLID OXIDE FUEL CELL THIN FILM Thin films YTTRIA STABILISED ZIRCONIA Zirconium dioxide |
Title | Sputtered YSZ based protective thin films for SOFCs |
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