Ultrafast laser diode thermal desorption method for analysis of representative pharmaceuticals in soil leachate samples

We developed and evaluated a novel analytical method combining ambient ionization technique - laser diode thermal desorption with chemical ionization (LDTD-APCI) and tandem mass spectrometry detection. The LDTD/APCI-MS/MS method was developed for determination of representative pharmaceuticals from...

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Published inTalanta (Oxford) Vol. 208; p. 120382
Main Authors Borik, A., Vojs Stanova, A., Kodesova, R., Brooks, B.W., Grabicova, K., Novakova, P., Grabic, R.
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 01.02.2020
Subjects
Ambient ionization
Analytical method comparison
Green chemistry
Laser diode thermal desorption
Pharmaceuticals
Soil sorption
Ambient ionization
Green chemistry
Soil sorption
Analytical method comparison
Laser diode thermal desorption
Pharmaceuticals
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Abstract We developed and evaluated a novel analytical method combining ambient ionization technique - laser diode thermal desorption with chemical ionization (LDTD-APCI) and tandem mass spectrometry detection. The LDTD/APCI-MS/MS method was developed for determination of representative pharmaceuticals from different classes (carbamazepine, sulfamethoxazole, irbesartan, fexofenadine) in leachate samples from soil sorption experimentation. We then optimized laser pattern, laser energy and spiked sample volume, which are crucial parameters for this LDTD/APCI-MS/MS method. We further identified utility of a chelating agent (Na2-EDTA) to obtain the highest achievable and reproducible signal of target analytes. Achieved method performance parameters (LODs, LOQs, trueness and precision) were comparable with those obtained from LC-MS/MS. However, application of this novel LDTD/APCI-MS/MS method reduced analysis time by two orders of magnitude (to 12 s), compared to more conventional LC-MS/MS approaches, without use of organic solvents. We expect this novel method will reduce costs and increase throughput for future analyses of pharmaceuticals in the environment while advancing a timely principle of green chemistry. [Display omitted] •A newly developed LDTD-APCI-MSMS method increases analysis speed to 12 s per sample.•This LDTD-APCI-MSMS method allows quantification of drugs from different classes.•Instrument response for some analytes was improved by addition of Na2-EDTA.•Performance parameters are comparable with gold standard LC-HESI-MSMS methods.
AbstractList We developed and evaluated a novel analytical method combining ambient ionization technique - laser diode thermal desorption with chemical ionization (LDTD-APCI) and tandem mass spectrometry detection. The LDTD/APCI-MS/MS method was developed for determination of representative pharmaceuticals from different classes (carbamazepine, sulfamethoxazole, irbesartan, fexofenadine) in leachate samples from soil sorption experimentation. We then optimized laser pattern, laser energy and spiked sample volume, which are crucial parameters for this LDTD/APCI-MS/MS method. We further identified utility of a chelating agent (Na2-EDTA) to obtain the highest achievable and reproducible signal of target analytes. Achieved method performance parameters (LODs, LOQs, trueness and precision) were comparable with those obtained from LC-MS/MS. However, application of this novel LDTD/APCI-MS/MS method reduced analysis time by two orders of magnitude (to 12 s), compared to more conventional LC-MS/MS approaches, without use of organic solvents. We expect this novel method will reduce costs and increase throughput for future analyses of pharmaceuticals in the environment while advancing a timely principle of green chemistry. [Display omitted] •A newly developed LDTD-APCI-MSMS method increases analysis speed to 12 s per sample.•This LDTD-APCI-MSMS method allows quantification of drugs from different classes.•Instrument response for some analytes was improved by addition of Na2-EDTA.•Performance parameters are comparable with gold standard LC-HESI-MSMS methods.
We developed and evaluated a novel analytical method combining ambient ionization technique - laser diode thermal desorption with chemical ionization (LDTD-APCI) and tandem mass spectrometry detection. The LDTD/APCI-MS/MS method was developed for determination of representative pharmaceuticals from different classes (carbamazepine, sulfamethoxazole, irbesartan, fexofenadine) in leachate samples from soil sorption experimentation. We then optimized laser pattern, laser energy and spiked sample volume, which are crucial parameters for this LDTD/APCI-MS/MS method. We further identified utility of a chelating agent (Na -EDTA) to obtain the highest achievable and reproducible signal of target analytes. Achieved method performance parameters (LODs, LOQs, trueness and precision) were comparable with those obtained from LC-MS/MS. However, application of this novel LDTD/APCI-MS/MS method reduced analysis time by two orders of magnitude (to 12 s), compared to more conventional LC-MS/MS approaches, without use of organic solvents. We expect this novel method will reduce costs and increase throughput for future analyses of pharmaceuticals in the environment while advancing a timely principle of green chemistry.
ArticleNumber 120382
Author Grabicova, K.
Brooks, B.W.
Grabic, R.
Novakova, P.
Borik, A.
Kodesova, R.
Vojs Stanova, A.
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  organization: University of South Bohemia in Ceske Budejovice, Faculty of Fisheries and Protection of Waters, South Bohemian Research Center of Aquaculture and Biodiversity of Hydrocenoses, Zatisi 728/II, 389 25, Vodnany, Czech Republic
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  givenname: R.
  surname: Kodesova
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  organization: Czech University of Life Sciences Prague, Faculty of Agrobiology, Food and Natural Resources, Dept. of Soil Science and Soil Protection, Kamycka 129, Prague 6, 16500, Czech Republic
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/31816693$$D View this record in MEDLINE/PubMed
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Keywords Ambient ionization
Green chemistry
Soil sorption
Analytical method comparison
Laser diode thermal desorption
Pharmaceuticals
Language English
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Snippet We developed and evaluated a novel analytical method combining ambient ionization technique - laser diode thermal desorption with chemical ionization...
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StartPage 120382
SubjectTerms Ambient ionization
Analytical method comparison
Green chemistry
Laser diode thermal desorption
Pharmaceuticals
Soil sorption
Title Ultrafast laser diode thermal desorption method for analysis of representative pharmaceuticals in soil leachate samples
URI https://dx.doi.org/10.1016/j.talanta.2019.120382
https://www.ncbi.nlm.nih.gov/pubmed/31816693
https://search.proquest.com/docview/2323465635
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