Effects of hydrothermal-alkali and freezing-thawing pre-treatments on modification of corn starch with octenyl succinic anhydride

•HA pre-treatment increased reaction efficiency of OSA modification.•F/T pre-treatment decreased efficiency of OSA modification of starch.•OSA-HAF-starch had higher pasting viscosities than other OSA-starches.•OSA modification disrupted mainly the short range structural order of starch. Pre-treatmen...

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Published inCarbohydrate polymers Vol. 175; pp. 361 - 369
Main Authors Wang, Shujun, Li, Tiangui, Wang, Shuo, Copeland, Les
Format Journal Article
LanguageEnglish
Published England Elsevier Ltd 01.11.2017
Subjects
Freezing-thawing
Hydrothermal-alkali
LCM-Raman spectra
OSA-starch
Pasting properties
Freezing-thawing
Hydrothermal-alkali
OSA-starch
Pasting properties
LCM-Raman spectra
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Abstract •HA pre-treatment increased reaction efficiency of OSA modification.•F/T pre-treatment decreased efficiency of OSA modification of starch.•OSA-HAF-starch had higher pasting viscosities than other OSA-starches.•OSA modification disrupted mainly the short range structural order of starch. Pre-treatments by freezing/thawing (F/T) and hydrothermal-alkali (HA) were used in the modification of starch with octenyl succinic anhydride (OSA). In comparison with OSA-modified starch prepared without pre-treatment (degree of substitution, DS=0.0172; reaction efficiency, RE=73.9%), HA pre-treatment increased the DS of OSA-starch and RE of subsequent OSA modification (0.0185 and 79.7%, respectively). In contrast, F/T pre-treatment gave the opposite results (0.0152 and 65.5%, respectively). OSA modification markedly increased the viscosities but decreased the gelatinization parameters of native starch. Esterification of starch by OSA was confirmed with Fourier transform infrared and Raman spectroscopy, which indicated markedly decreased short-range molecular orders of native starch. The present study showed that HA pre-treatment before OSA modification is an efficient way to improve the reaction efficiency of OSA with starch and thereby to modify the pasting properties of starch. F/T pre-treatment did not increase the reaction efficiency of starch with OSA.
AbstractList •HA pre-treatment increased reaction efficiency of OSA modification.•F/T pre-treatment decreased efficiency of OSA modification of starch.•OSA-HAF-starch had higher pasting viscosities than other OSA-starches.•OSA modification disrupted mainly the short range structural order of starch. Pre-treatments by freezing/thawing (F/T) and hydrothermal-alkali (HA) were used in the modification of starch with octenyl succinic anhydride (OSA). In comparison with OSA-modified starch prepared without pre-treatment (degree of substitution, DS=0.0172; reaction efficiency, RE=73.9%), HA pre-treatment increased the DS of OSA-starch and RE of subsequent OSA modification (0.0185 and 79.7%, respectively). In contrast, F/T pre-treatment gave the opposite results (0.0152 and 65.5%, respectively). OSA modification markedly increased the viscosities but decreased the gelatinization parameters of native starch. Esterification of starch by OSA was confirmed with Fourier transform infrared and Raman spectroscopy, which indicated markedly decreased short-range molecular orders of native starch. The present study showed that HA pre-treatment before OSA modification is an efficient way to improve the reaction efficiency of OSA with starch and thereby to modify the pasting properties of starch. F/T pre-treatment did not increase the reaction efficiency of starch with OSA.
Pre-treatments by freezing/thawing (F/T) and hydrothermal-alkali (HA) were used in the modification of starch with octenyl succinic anhydride (OSA). In comparison with OSA-modified starch prepared without pre-treatment (degree of substitution, DS=0.0172; reaction efficiency, RE=73.9%), HA pre-treatment increased the DS of OSA-starch and RE of subsequent OSA modification (0.0185 and 79.7%, respectively). In contrast, F/T pre-treatment gave the opposite results (0.0152 and 65.5%, respectively). OSA modification markedly increased the viscosities but decreased the gelatinization parameters of native starch. Esterification of starch by OSA was confirmed with Fourier transform infrared and Raman spectroscopy, which indicated markedly decreased short-range molecular orders of native starch. The present study showed that HA pre-treatment before OSA modification is an efficient way to improve the reaction efficiency of OSA with starch and thereby to modify the pasting properties of starch. F/T pre-treatment did not increase the reaction efficiency of starch with OSA.
Author Wang, Shuo
Wang, Shujun
Copeland, Les
Li, Tiangui
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  organization: Sydney Institute of Agriculture, School of Life and Environmental Sciences, University of Sydney, NSW 2006, Australia
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Keywords Freezing-thawing
Hydrothermal-alkali
OSA-starch
Pasting properties
LCM-Raman spectra
Language English
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  doi: 10.1016/j.carbpol.2004.10.011
  contributor:
    fullname: Ortega-Ojeda
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Snippet •HA pre-treatment increased reaction efficiency of OSA modification.•F/T pre-treatment decreased efficiency of OSA modification of starch.•OSA-HAF-starch had...
Pre-treatments by freezing/thawing (F/T) and hydrothermal-alkali (HA) were used in the modification of starch with octenyl succinic anhydride (OSA). In...
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SubjectTerms Freezing-thawing
Hydrothermal-alkali
LCM-Raman spectra
OSA-starch
Pasting properties
Title Effects of hydrothermal-alkali and freezing-thawing pre-treatments on modification of corn starch with octenyl succinic anhydride
URI https://dx.doi.org/10.1016/j.carbpol.2017.08.014
https://www.ncbi.nlm.nih.gov/pubmed/28917877
https://search.proquest.com/docview/1940199125
Volume 175
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