Sustainable thermoplastic elastomers derived from cellulose, fatty acid and furfural via ATRP and click chemistry
[Display omitted] •Thermoplastic elastomers (TPEs) are derived from sustainable Cellulose, Fatty Acid and Furfuryl.•ATRP and Click Chemistry are combined to fabricate the sustainable TPEs with different side chain composition.•Cellulose afford the TPEs with improved mechanical property.•This work pr...
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| Published in | Carbohydrate polymers Vol. 176; pp. 83 - 90 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Elsevier Ltd
15.11.2017
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Thermoplastic elastomers (TPEs) are derived from sustainable Cellulose, Fatty Acid and Furfuryl.•ATRP and Click Chemistry are combined to fabricate the sustainable TPEs with different side chain composition.•Cellulose afford the TPEs with improved mechanical property.•This work provides a sustainable avenue to develop full bio-base materials.
Cellulose-based thermoplastic elastomers (TPEs) have attracted considerable attention because of their rigid backbone, good mechanical properties, renewable nature and abundance. In the present study, sustainable TPEs based on ethyl cellulose (EC), fatty acid and furfural were generated by the combination of ATRP and “click chemistry”. To fabricate sustainable TPEs with higher toughness, a range of polymers, including mono random-copolymer poly(tetrahydrofurfuryl methacrylate-co-lauryl methacrylate) (P(THFMA-co-LMA), dual polymer side chains PTHFMA and PLMA, and mono-block copolymer PTHFMA-b-PLMA, were designed as side chains to fabricate EC brush copolymers with random, dual or block side chain architectures using the “grafting from” and “grafting onto” methods. The multi-armed structures, chemical compositions and phase separation of these EC brush copolymers were confirmed by FT-IR, 1H NMR, GPC, DSC, TEM and SEM. Overall, three types of EC brush copolymers all exhibited the desired mechanical properties of TPEs. In addition, the EC brush copolymers with dual/block side chain architectures showed higher tensile strength than that of the random polymers with similar compositions. |
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| AbstractList | Cellulose-based thermoplastic elastomers (TPEs) have attracted considerable attention because of their rigid backbone, good mechanical properties, renewable nature and abundance. In the present study, sustainable TPEs based on ethyl cellulose (EC), fatty acid and furfural were generated by the combination of ATRP and "click chemistry". To fabricate sustainable TPEs with higher toughness, a range of polymers, including mono random-copolymer poly(tetrahydrofurfuryl methacrylate-co-lauryl methacrylate) (P(THFMA-co-LMA), dual polymer side chains PTHFMA and PLMA, and mono-block copolymer PTHFMA-b-PLMA, were designed as side chains to fabricate EC brush copolymers with random, dual or block side chain architectures using the "grafting from" and "grafting onto" methods. The multi-armed structures, chemical compositions and phase separation of these EC brush copolymers were confirmed by FT-IR,
H NMR, GPC, DSC, TEM and SEM. Overall, three types of EC brush copolymers all exhibited the desired mechanical properties of TPEs. In addition, the EC brush copolymers with dual/block side chain architectures showed higher tensile strength than that of the random polymers with similar compositions. Cellulose-based thermoplastic elastomers (TPEs) have attracted considerable attention because of their rigid backbone, good mechanical properties, renewable nature and abundance. In the present study, sustainable TPEs based on ethyl cellulose (EC), fatty acid and furfural were generated by the combination of ATRP and "click chemistry". To fabricate sustainable TPEs with higher toughness, a range of polymers, including mono random-copolymer poly(tetrahydrofurfuryl methacrylate-co-lauryl methacrylate) (P(THFMA-co-LMA), dual polymer side chains PTHFMA and PLMA, and mono-block copolymer PTHFMA-b-PLMA, were designed as side chains to fabricate EC brush copolymers with random, dual or block side chain architectures using the "grafting from" and "grafting onto" methods. The multi-armed structures, chemical compositions and phase separation of these EC brush copolymers were confirmed by FT-IR, 1H NMR, GPC, DSC, TEM and SEM. Overall, three types of EC brush copolymers all exhibited the desired mechanical properties of TPEs. In addition, the EC brush copolymers with dual/block side chain architectures showed higher tensile strength than that of the random polymers with similar compositions. [Display omitted] •Thermoplastic elastomers (TPEs) are derived from sustainable Cellulose, Fatty Acid and Furfuryl.•ATRP and Click Chemistry are combined to fabricate the sustainable TPEs with different side chain composition.•Cellulose afford the TPEs with improved mechanical property.•This work provides a sustainable avenue to develop full bio-base materials. Cellulose-based thermoplastic elastomers (TPEs) have attracted considerable attention because of their rigid backbone, good mechanical properties, renewable nature and abundance. In the present study, sustainable TPEs based on ethyl cellulose (EC), fatty acid and furfural were generated by the combination of ATRP and “click chemistry”. To fabricate sustainable TPEs with higher toughness, a range of polymers, including mono random-copolymer poly(tetrahydrofurfuryl methacrylate-co-lauryl methacrylate) (P(THFMA-co-LMA), dual polymer side chains PTHFMA and PLMA, and mono-block copolymer PTHFMA-b-PLMA, were designed as side chains to fabricate EC brush copolymers with random, dual or block side chain architectures using the “grafting from” and “grafting onto” methods. The multi-armed structures, chemical compositions and phase separation of these EC brush copolymers were confirmed by FT-IR, 1H NMR, GPC, DSC, TEM and SEM. Overall, three types of EC brush copolymers all exhibited the desired mechanical properties of TPEs. In addition, the EC brush copolymers with dual/block side chain architectures showed higher tensile strength than that of the random polymers with similar compositions. |
| Author | Wang, Chunpeng Chu, Fuxiang Fan, Yimin Lu, Chuanwei Yu, Juan Wang, Jifu |
| Author_xml | – sequence: 1 givenname: Juan surname: Yu fullname: Yu, Juan organization: Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Jiangsu Key Lab of Biomass-Based Green Fuel and Chemicals, College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China – sequence: 2 givenname: Chuanwei surname: Lu fullname: Lu, Chuanwei organization: Institute of Chemical Industry of Forest Products, CAF, National Engineering Laboratory of Biomass Chemical Utilization, Key and Laboratory of Forest Chemical Engineering, SFA, Key Laboratory of Biomass Energy and Material, Nanjing, Jiangsu Province 210042, China – sequence: 3 givenname: Chunpeng surname: Wang fullname: Wang, Chunpeng organization: Institute of Chemical Industry of Forest Products, CAF, National Engineering Laboratory of Biomass Chemical Utilization, Key and Laboratory of Forest Chemical Engineering, SFA, Key Laboratory of Biomass Energy and Material, Nanjing, Jiangsu Province 210042, China – sequence: 4 givenname: Jifu surname: Wang fullname: Wang, Jifu email: wjf118@hotmail.com, wjf118@126.com organization: Institute of Chemical Industry of Forest Products, CAF, National Engineering Laboratory of Biomass Chemical Utilization, Key and Laboratory of Forest Chemical Engineering, SFA, Key Laboratory of Biomass Energy and Material, Nanjing, Jiangsu Province 210042, China – sequence: 5 givenname: Yimin surname: Fan fullname: Fan, Yimin organization: Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources, Jiangsu Key Lab of Biomass-Based Green Fuel and Chemicals, College of Chemical Engineering, Nanjing Forestry University, Nanjing 210037, China – sequence: 6 givenname: Fuxiang surname: Chu fullname: Chu, Fuxiang organization: Institute of Chemical Industry of Forest Products, CAF, National Engineering Laboratory of Biomass Chemical Utilization, Key and Laboratory of Forest Chemical Engineering, SFA, Key Laboratory of Biomass Energy and Material, Nanjing, Jiangsu Province 210042, China |
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| Keywords | Thermoplastic elastomers Brush copolymers Click chemistry Atom transfer radical polymerization (ATRP) Ethyl cellulose |
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•Thermoplastic elastomers (TPEs) are derived from sustainable Cellulose, Fatty Acid and Furfuryl.•ATRP and Click Chemistry are combined to... Cellulose-based thermoplastic elastomers (TPEs) have attracted considerable attention because of their rigid backbone, good mechanical properties, renewable... |
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| SubjectTerms | Atom transfer radical polymerization (ATRP) Brush copolymers Cellulose - chemistry Click Chemistry Elastomers - chemistry Ethyl cellulose Fatty Acids - chemistry Furaldehyde - chemistry Polymers Spectroscopy, Fourier Transform Infrared Thermoplastic elastomers |
| Title | Sustainable thermoplastic elastomers derived from cellulose, fatty acid and furfural via ATRP and click chemistry |
| URI | https://dx.doi.org/10.1016/j.carbpol.2017.08.060 https://www.ncbi.nlm.nih.gov/pubmed/28927630 https://search.proquest.com/docview/1941091851 |
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