Discrete One-Stage Mechanochemical Synthesis of Titanium-Nitride in a High-Energy Mill

• Published in: Metals (Basel ) Vol. 11; no. 11; p. 1743
• Main Authors: Lapshin, Oleg, Shkoda, Olga, Ivanova, Oksana, Zelepugin, Sergey
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 01.11.2021
• Subjects: Chemical reactions; Chemical synthesis; Energy; experiment; Heat; high-energy mill; Inverse problems; Mathematical analysis; mathematical model; Mathematical models; mechanical activation; mechanochemical synthesis; Nitrogen; Particle size; Phase transitions; Radiation; Reagents; Temperature effects; Titanium; Titanium nitride; Belgium; Russia

Discrete (discontinuous) mechanochemical synthesis of titanium nitride was experimentally investigated. The experimental results show that mechanical activation intensifies the chemical conversion in the Ti-N system, and the discrete synthesis of the final product is conducted under “soft” controlle...