One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles

• Published in: Science of sintering Vol. 52; no. 4; pp. 481 - 490
• Main Authors: Jeremic, Dejan, Andjelkovic, Ljubica, Milenkovic, Milica, Suljagic, Marija, Sumar-Ristovic, Maja, Ostojic, Sanja, Nikolic, Aleksandar, Vulic, Predrag, Brceski, Ilija, Pavlovic, Vladimir
• Format: Journal Article
• Language: English
• Published: Beograd International Institute for the Science of Sintering (IISS) 2020; International Institute for the Science of Sintering, Beograd
• Subjects: Camphor; camphor sulfonates; Chemical composition; Combustion synthesis; Coordination compounds; Crystal structure; Crystallites; Decomposition; Dispersion; Energy dispersive X ray spectroscopy; Ferric oxide; Fourier transforms; Hematite; Infrared analysis; Infrared spectroscopy; Investigations; Metal oxides; Morphology; Nanomaterials; Nanoparticles; nickel oxide; Nickel oxides; one-pot synthesis; Optics; Purity; Scanning electron microscopy; Solvents; Spectrum analysis; Thermal decomposition; Thermodynamic properties; Thermogravimetric analysis; Transition metals; X ray powder diffraction

This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (?-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier...