Sonochemical degradation of chlorophenols in water
Sonochemical degradation of dilute aqueous solutions of 2-, 3- and 4-chlorophenol and pentachlorophenol has been investigated under air or argon atmosphere. The degradation follows first-order kinetics in the initial state with rates in the range 4.5–6.6 μM min −1 under air and 6.0–7.2 μM min −1 und...
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Published in | Ultrasonics sonochemistry Vol. 7; no. 3; pp. 115 - 120 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Netherlands
Elsevier B.V
01.07.2000
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Abstract | Sonochemical degradation of dilute aqueous solutions of 2-, 3- and 4-chlorophenol and pentachlorophenol has been investigated under air or argon atmosphere. The degradation follows first-order kinetics in the initial state with rates in the range 4.5–6.6
μM
min
−1 under air and 6.0–7.2
μM
min
−1 under argon at a concentration of 100
μM of chlorophenols. The rate of OH radical formation from water is 19.8
μM
min
−1 under argon and 14.7
μM
min
−1 under air in the same sonolysis conditions. The sonolysis of chlorophenols is effectively inhibited, but not completely, by the addition of t-BuOH, which is known to be an efficient OH radical scavenger in aqueous sonolysis. This suggests that the main degradation of chlorophenols proceeds via reaction with OH radicals; a thermal reaction also occurs, although its contribution is small. The addition of appropriate amounts of Fe(II) ions accelerates the degradation. This is probably due to the regeneration of OH radicals from hydrogen peroxide, which would be formed from recombination of OH radicals and which may contribute a little to the degradation. The ability to inhibit bacterial multiplication of pentachlorophenol decreases with ultrasonic irradiation. |
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AbstractList | Sonochemical degradation of dilute aqueous solutions of 2-, 3- and 4-chlorophenol and pentachlorophenol has been investigated under air or argon atmosphere. The degradation follows first-order kinetics in the initial state with rates in the range 4.5–6.6
μM
min
−1 under air and 6.0–7.2
μM
min
−1 under argon at a concentration of 100
μM of chlorophenols. The rate of OH radical formation from water is 19.8
μM
min
−1 under argon and 14.7
μM
min
−1 under air in the same sonolysis conditions. The sonolysis of chlorophenols is effectively inhibited, but not completely, by the addition of t-BuOH, which is known to be an efficient OH radical scavenger in aqueous sonolysis. This suggests that the main degradation of chlorophenols proceeds via reaction with OH radicals; a thermal reaction also occurs, although its contribution is small. The addition of appropriate amounts of Fe(II) ions accelerates the degradation. This is probably due to the regeneration of OH radicals from hydrogen peroxide, which would be formed from recombination of OH radicals and which may contribute a little to the degradation. The ability to inhibit bacterial multiplication of pentachlorophenol decreases with ultrasonic irradiation. Sonochemical degradation of dilute aqueous solutions of 2-, 3- and 4-chlorophenol and pentachlorophenol has been investigated under air or argon atmosphere. The degradation follows first-order kinetics in the initial state with rates in the range 4.5-6.6 microM min-1 under air and 6.0-7.2 microM min-1 under argon at a concentration of 100 microM of chlorophenols. The rate of OH radical formation from water is 19.8 microM min-1 under argon and 14.7 microM min-1 under air in the same sonolysis conditions. The sonolysis of chlorophenols is effectively inhibited, but not completely, by the addition of t-BuOH, which is known to be an efficient OH radical scavenger in aqueous sonolysis. This suggests that the main degradation of chlorophenols proceeds via reaction with OH radicals; a thermal reaction also occurs, although its contribution is small. The addition of appropriate amounts of Fe(II) ions accelerates the degradation. This is probably due to the regeneration of OH radicals from hydrogen peroxide, which would be formed from recombination of OH radicals and which may contribute a little to the degradation. The ability to inhibit bacterial multiplication of pentachlorophenol decreases with ultrasonic irradiation. |
Author | Okuno, Hiroshi Nagata, Yoshio Nakagawa, Michiyo Yim, Bongbeen Maeda, Yasuaki Mizukoshi, Yoshiteru |
Author_xml | – sequence: 1 givenname: Yoshio surname: Nagata fullname: Nagata, Yoshio email: nagata@riast.osakafu-u.ac.jp organization: Research Institute for Advanced Science and Technology, Osaka Prefecture University, Gakuen-cho 1-2, Sakai, Osaka 599-8570, Japan – sequence: 2 givenname: Michiyo surname: Nakagawa fullname: Nakagawa, Michiyo organization: Department of Applied Materials Science, College of Engineering, Osaka Prefecture University, Gakuen-cho 1-1, Sakai, Osaka 599-8530, Japan – sequence: 3 givenname: Hiroshi surname: Okuno fullname: Okuno, Hiroshi organization: Department of Applied Materials Science, College of Engineering, Osaka Prefecture University, Gakuen-cho 1-1, Sakai, Osaka 599-8530, Japan – sequence: 4 givenname: Yoshiteru surname: Mizukoshi fullname: Mizukoshi, Yoshiteru organization: Department of Applied Materials Science, College of Engineering, Osaka Prefecture University, Gakuen-cho 1-1, Sakai, Osaka 599-8530, Japan – sequence: 5 givenname: Bongbeen surname: Yim fullname: Yim, Bongbeen organization: Department of Applied Materials Science, College of Engineering, Osaka Prefecture University, Gakuen-cho 1-1, Sakai, Osaka 599-8530, Japan – sequence: 6 givenname: Yasuaki surname: Maeda fullname: Maeda, Yasuaki organization: Department of Applied Materials Science, College of Engineering, Osaka Prefecture University, Gakuen-cho 1-1, Sakai, Osaka 599-8530, Japan |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/10909729$$D View this record in MEDLINE/PubMed |
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Keywords | Chlorophenols Pentachlorophenol Sonochemical degradation |
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Snippet | Sonochemical degradation of dilute aqueous solutions of 2-, 3- and 4-chlorophenol and pentachlorophenol has been investigated under air or argon atmosphere.... |
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SubjectTerms | Chlorophenols Pentachlorophenol Sonochemical degradation |
Title | Sonochemical degradation of chlorophenols in water |
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