Synthesis and flocculation property in dye solutions of β-cyclodextrin–acrylic acid–[2-(Acryloyloxy)ethyl] trimethyl ammonium chloride copolymer

In aqueous solution a cationic copolymer, poly (β-CD–AA–DMC) was synthesized via free radical copolymerization of acrylic acid (AA) esterified β-CD (β-CD–AA), and a cationic monomer [2-(Acryloyloxy)ethyl] trimethyl ammonium chloride (DMC). The copolymer's structure, morphology and thermal stabi...

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Published inCarbohydrate polymers Vol. 87; no. 3; pp. 1956 - 1962
Main Authors Tian, Xiuzhi, Ren, Erhui, Wang, Junhua, Zou, Jinlei, Tao, Yong, Wang, Shugen, Jiang, Xue
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier Ltd 14.02.2012
Elsevier
Subjects
acrylic acid
adsorption
Applied sciences
aqueous solutions
Cationic
composite polymers
Decolorization
esterification
Exact sciences and technology
Flocculant
flocculation
Fourier transform infrared spectroscopy
Natural polymers
nuclear magnetic resonance spectroscopy
Physicochemistry of polymers
poly (β-CD–AA–DMC)
reactive dyes
scanning electron microscopy
Starch and polysaccharides
thermal stability
Decolorization
Cationic
Flocculant
poly (β-CD–AA–DMC)
Acrylic acid copolymer
Organic dye
Molecular structure
Quaternary ammonium copolymer
Crosslinking
Experimental study
Thermal stability
Crosslinked copolymer
Cyclodextrin
Flocculation reagent
Ionic strength
Flocculation
Morphology
Preparation
poly (β-CD-AA-DMC)
pH
Oside polymer
Acrylate copolymer
Aqueous solution
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Abstract In aqueous solution a cationic copolymer, poly (β-CD–AA–DMC) was synthesized via free radical copolymerization of acrylic acid (AA) esterified β-CD (β-CD–AA), and a cationic monomer [2-(Acryloyloxy)ethyl] trimethyl ammonium chloride (DMC). The copolymer's structure, morphology and thermal stability were demonstrated by FT-IR, 1H NMR, SEM and TGA analysis. The flocculation properties of the copolymer were evaluated by the decolorization solutions of two reactive dyes using a jar test method. The decolorization efficiency is influenced by both the nature of the anionic dyes and the pH of the initial dye solution. Electrostatic adsorption played a more important role in flocculation of dyes than bridging of the polymer. Moreover, the inorganic salt decreased the efficiency of color removal.
AbstractList In aqueous solution a cationic copolymer, poly (β-CD–AA–DMC) was synthesized via free radical copolymerization of acrylic acid (AA) esterified β-CD (β-CD–AA), and a cationic monomer [2-(Acryloyloxy)ethyl] trimethyl ammonium chloride (DMC). The copolymer's structure, morphology and thermal stability were demonstrated by FT-IR, 1H NMR, SEM and TGA analysis. The flocculation properties of the copolymer were evaluated by the decolorization solutions of two reactive dyes using a jar test method. The decolorization efficiency is influenced by both the nature of the anionic dyes and the pH of the initial dye solution. Electrostatic adsorption played a more important role in flocculation of dyes than bridging of the polymer. Moreover, the inorganic salt decreased the efficiency of color removal.
In aqueous solution a cationic copolymer, poly (β-CD–AA–DMC) was synthesized via free radical copolymerization of acrylic acid (AA) esterified β-CD (β-CD–AA), and a cationic monomer [2-(Acryloyloxy)ethyl] trimethyl ammonium chloride (DMC). The copolymer's structure, morphology and thermal stability were demonstrated by FT-IR, ¹H NMR, SEM and TGA analysis. The flocculation properties of the copolymer were evaluated by the decolorization solutions of two reactive dyes using a jar test method. The decolorization efficiency is influenced by both the nature of the anionic dyes and the pH of the initial dye solution. Electrostatic adsorption played a more important role in flocculation of dyes than bridging of the polymer. Moreover, the inorganic salt decreased the efficiency of color removal.
Author Jiang, Xue
Ren, Erhui
Zou, Jinlei
Tao, Yong
Tian, Xiuzhi
Wang, Junhua
Wang, Shugen
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Issue 3
Keywords Decolorization
Cationic
Flocculant
poly (β-CD–AA–DMC)
Acrylic acid copolymer
Organic dye
Molecular structure
Quaternary ammonium copolymer
Crosslinking
Experimental study
Thermal stability
Crosslinked copolymer
Cyclodextrin
Flocculation reagent
Ionic strength
Flocculation
Morphology
Preparation
poly (β-CD-AA-DMC)
pH
Oside polymer
Acrylate copolymer
Aqueous solution
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Snippet In aqueous solution a cationic copolymer, poly (β-CD–AA–DMC) was synthesized via free radical copolymerization of acrylic acid (AA) esterified β-CD (β-CD–AA),...
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SubjectTerms acrylic acid
adsorption
Applied sciences
aqueous solutions
Cationic
composite polymers
Decolorization
esterification
Exact sciences and technology
Flocculant
flocculation
Fourier transform infrared spectroscopy
Natural polymers
nuclear magnetic resonance spectroscopy
Physicochemistry of polymers
poly (β-CD–AA–DMC)
reactive dyes
scanning electron microscopy
Starch and polysaccharides
thermal stability
Title Synthesis and flocculation property in dye solutions of β-cyclodextrin–acrylic acid–[2-(Acryloyloxy)ethyl] trimethyl ammonium chloride copolymer
URI https://dx.doi.org/10.1016/j.carbpol.2011.10.003
Volume 87
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