Carbon fiber paper supported interlayer space enlarged Ni2Fe-LDHs improved OER electrocatalytic activity
Herein, a series of three-dimensional Ni2Fe-SDS-LDH/CFP non-precious metal electrocatalysts in a simple hydrothermal route using sodium dodecyl sulfonate (SDS) as an interlayer spacer agent, and carbon fiber paper (CFP) as a conductive substrate was tailored. The electrocatalytic performance towards...
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| Published in | Electrochimica acta Vol. 258; pp. 554 - 560 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
20.12.2017
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0013-4686 1873-3859 |
| DOI | 10.1016/j.electacta.2017.11.098 |
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| Abstract | Herein, a series of three-dimensional Ni2Fe-SDS-LDH/CFP non-precious metal electrocatalysts in a simple hydrothermal route using sodium dodecyl sulfonate (SDS) as an interlayer spacer agent, and carbon fiber paper (CFP) as a conductive substrate was tailored. The electrocatalytic performance towards oxygen evolution reaction (OER) in alkaline medium was investigated. The results demonstrate that the OER activity improvement is mainly related to the increased interlayer distance from 0.76 nm to 2.49 nm depending on the intercalated amount of SDS in Ni2Fe-LDH, and resulting in the enhanced superior surface characteristics (e.g., larger specific surface area, bigger pore size and pore volume). Among all the samples, the Ni2Fe-SDS-LDH/CFP (molar ratio SDS/Fe = 1.5) showed the best OER performance (η@10 mA cm−2 = 289 mV, Tafel slope = 39 mV dec−1) comparable with the commercial IrO2 catalyst, which corresponded to the largest interlayer space of 2.49 nm.
A series of three-dimensional Ni2Fe-SDS-LDH/CFP non-precious metal electrocatalysts in a simple hydrothermal route using sodium dodecyl sulfonate (SDS) as an interlayer spacer agent, and carbon fiber paper (CFP) as a conductive substrate was tailored. The electrocatalytic performance towards oxygen evolution reaction (OER) in alkaline medium was investigated. The results demonstrate that the OER activity improvement is mainly related to the increased interlayer distance from 0.76 nm to 2.49 nm, depending on the intercalation amount of SDS in the Ni2Fe-LDH. Among all samples, the Ni2Fe-SDS-LDH/CFP (molar ratio SDS/Fe = 1.5) showed the best OER performance (η@10 mA cm−2 = 289 mV, Tafel slope = 39 mV dec−1) comparable with the commercial IrO2 catalyst, which corresponded to the largest interlayer space of 2.49 nm. [Display omitted]
•SDS intercalated Ni2Fe-LDHs with different interlayer distances were prepared.•OER activity of Ni2Fe-SDS-LDH/CFP were related with the interlayer distance.•Electrocatalytic performance is higher than commercial IrO2 in alkaline medium. |
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| AbstractList | Herein, a series of three-dimensional Ni2Fe-SDS-LDH/CFP non-precious metal electrocatalysts in a simple hydrothermal route using sodium dodecyl sulfonate (SDS) as an interlayer spacer agent, and carbon fiber paper (CFP) as a conductive substrate was tailored. The electrocatalytic performance towards oxygen evolution reaction (OER) in alkaline medium was investigated. The results demonstrate that the OER activity improvement is mainly related to the increased interlayer distance from 0.76 nm to 2.49 nm depending on the intercalated amount of SDS in Ni2Fe-LDH, and resulting in the enhanced superior surface characteristics (e.g., larger specific surface area, bigger pore size and pore volume). Among all the samples, the Ni2Fe-SDS-LDH/CFP (molar ratio SDS/Fe = 1.5) showed the best OER performance (η@10 mA cm−2 = 289 mV, Tafel slope = 39 mV dec−1) comparable with the commercial IrO2 catalyst, which corresponded to the largest interlayer space of 2.49 nm.
A series of three-dimensional Ni2Fe-SDS-LDH/CFP non-precious metal electrocatalysts in a simple hydrothermal route using sodium dodecyl sulfonate (SDS) as an interlayer spacer agent, and carbon fiber paper (CFP) as a conductive substrate was tailored. The electrocatalytic performance towards oxygen evolution reaction (OER) in alkaline medium was investigated. The results demonstrate that the OER activity improvement is mainly related to the increased interlayer distance from 0.76 nm to 2.49 nm, depending on the intercalation amount of SDS in the Ni2Fe-LDH. Among all samples, the Ni2Fe-SDS-LDH/CFP (molar ratio SDS/Fe = 1.5) showed the best OER performance (η@10 mA cm−2 = 289 mV, Tafel slope = 39 mV dec−1) comparable with the commercial IrO2 catalyst, which corresponded to the largest interlayer space of 2.49 nm. [Display omitted]
•SDS intercalated Ni2Fe-LDHs with different interlayer distances were prepared.•OER activity of Ni2Fe-SDS-LDH/CFP were related with the interlayer distance.•Electrocatalytic performance is higher than commercial IrO2 in alkaline medium. |
| Author | Zhong, Haihong Li, Lin Cheng, Xiaokang Alonso-Vante, Nicolas Xu, Hantao Tang, Pinggui Li, Dianqing Feng, Yongjun |
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