Synergistic role of electron-trapped oxygen vacancy and exposed TiO2 [001] facets toward electrochemical p-nitrophenol reduction: Characterization, performance and mechanism
[Display omitted] •Electron-trapped oxygen vacancy was introduced in Ti/TiO2-001 by H2 reduction.•Increasing electron-trapped oxygen vacancy in Ti/TiO2-001 enhanced its reduction activity.•The synergistic role between electron-trapped oxygen vacancy and [001] facets was proposed.•Electron-trapped ox...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 411; p. 128485 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.05.2021
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| Subjects | |
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| Abstract | [Display omitted]
•Electron-trapped oxygen vacancy was introduced in Ti/TiO2-001 by H2 reduction.•Increasing electron-trapped oxygen vacancy in Ti/TiO2-001 enhanced its reduction activity.•The synergistic role between electron-trapped oxygen vacancy and [001] facets was proposed.•Electron-trapped oxygen vacancy on TiO2 acted as adsorption site and reactivity sites.
Despite the fact that electron-trapped oxygen vacancy and [001] facets fundamentally affect the reactivity of TiO2, their synergistic role in the electrochemical activity of TiO2 toward p-nitrophenol (p-NP) reduction is still unknown. In this study, defective and [001] facets engineered TiO2 cathode, i.e. Ti/TiO2−x-001, was prepared for p-NP reduction. In comparison to defective Ti/TiO2 cathode with [101] facets (Ti/TiO2−x-101), the combination of the electron-trapped oxygen vacancy and [001] facets exhibited a synergistic effect to improve the electrochemical reduction efficiency of TiO2. Density functional theory calculations verified that the introduction of [001] facets and electron-trapped oxygen vacancy on TiO2 was beneficial to facilitate electron transfer and improve the indirect reduction efficiency for p-NP electrochemical reduction. Moreover, the electron-trapped oxygen vacancy extent of Ti/TiO2−x-001 was modulated by adjusting reduction temperature (250–650 °C). The maximum electron-trapped oxygen vacancy amount of Ti/TiO2−x-001 was attained at the reduction temperature of 350 °C, which resulted in the highest p-NP reduction efficiency of 99.3%, accompanying the p-AP selectivity of 89.5%. In this case, the abundant active and adsorption sites were provided on the surface of Ti/TiO2−x-001 prepared at 350 °C, in which p-NP adsorption coefficient and electrochemical surface area increased to 1.01 L mg−1 and 25 cm2, respectively. Generally, this work provides a paradigm for the design of efficient non-metallic catalyst for nitroaromatic chemicals reduction. |
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| AbstractList | [Display omitted]
•Electron-trapped oxygen vacancy was introduced in Ti/TiO2-001 by H2 reduction.•Increasing electron-trapped oxygen vacancy in Ti/TiO2-001 enhanced its reduction activity.•The synergistic role between electron-trapped oxygen vacancy and [001] facets was proposed.•Electron-trapped oxygen vacancy on TiO2 acted as adsorption site and reactivity sites.
Despite the fact that electron-trapped oxygen vacancy and [001] facets fundamentally affect the reactivity of TiO2, their synergistic role in the electrochemical activity of TiO2 toward p-nitrophenol (p-NP) reduction is still unknown. In this study, defective and [001] facets engineered TiO2 cathode, i.e. Ti/TiO2−x-001, was prepared for p-NP reduction. In comparison to defective Ti/TiO2 cathode with [101] facets (Ti/TiO2−x-101), the combination of the electron-trapped oxygen vacancy and [001] facets exhibited a synergistic effect to improve the electrochemical reduction efficiency of TiO2. Density functional theory calculations verified that the introduction of [001] facets and electron-trapped oxygen vacancy on TiO2 was beneficial to facilitate electron transfer and improve the indirect reduction efficiency for p-NP electrochemical reduction. Moreover, the electron-trapped oxygen vacancy extent of Ti/TiO2−x-001 was modulated by adjusting reduction temperature (250–650 °C). The maximum electron-trapped oxygen vacancy amount of Ti/TiO2−x-001 was attained at the reduction temperature of 350 °C, which resulted in the highest p-NP reduction efficiency of 99.3%, accompanying the p-AP selectivity of 89.5%. In this case, the abundant active and adsorption sites were provided on the surface of Ti/TiO2−x-001 prepared at 350 °C, in which p-NP adsorption coefficient and electrochemical surface area increased to 1.01 L mg−1 and 25 cm2, respectively. Generally, this work provides a paradigm for the design of efficient non-metallic catalyst for nitroaromatic chemicals reduction. |
| ArticleNumber | 128485 |
| Author | Liu, Shuliang Meng, Xianzhe Li, Yifan Ni, Congcong Guan, Jing Jiang, Bo Luo, Siyi |
| Author_xml | – sequence: 1 givenname: Congcong surname: Ni fullname: Ni, Congcong – sequence: 2 givenname: Yifan surname: Li fullname: Li, Yifan – sequence: 3 givenname: Xianzhe surname: Meng fullname: Meng, Xianzhe – sequence: 4 givenname: Shuliang surname: Liu fullname: Liu, Shuliang – sequence: 5 givenname: Siyi surname: Luo fullname: Luo, Siyi – sequence: 6 givenname: Jing surname: Guan fullname: Guan, Jing – sequence: 7 givenname: Bo surname: Jiang fullname: Jiang, Bo email: bjiang86upc@163.com |
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| Title | Synergistic role of electron-trapped oxygen vacancy and exposed TiO2 [001] facets toward electrochemical p-nitrophenol reduction: Characterization, performance and mechanism |
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