Telechelic oligo(2,3-dihydroxypropylmethacrylate acetonide)s with aldehyde end functionality prepared by ozonolytic cleavage of poly(2,3-dihydroxypropan-1-methacrylate acetonide- stat-butadiene), prepared by monomer starve-fed emulsion polymerization
Telechelic oligomers with dialdehyde end groups and 2,3-dihydroxypropan-1-methacrylate acetonide repeat units were prepared by the ozonolytic cleavage of poly(2,3-dihydroxypropan-1-methacrylate acetonide- stat-butadiene) copolymers. The latter were prepared by monomer starve-fed emulsion polymerizat...
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| Published in | Reactive & functional polymers Vol. 58; no. 3; pp. 213 - 224 |
|---|---|
| Main Authors | , , |
| Format | Journal Article Conference Proceeding |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.03.2004
Elsevier Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Telechelic oligomers with dialdehyde end groups and 2,3-dihydroxypropan-1-methacrylate acetonide repeat units were prepared by the ozonolytic cleavage of poly(2,3-dihydroxypropan-1-methacrylate acetonide-
stat-butadiene) copolymers. The latter were prepared by monomer starve-fed emulsion polymerization at elevated temperatures and at atmospheric pressure. In contrast to similar copolymerizations of methyl and butyl methacrylate these polymerizations generated a gel fraction as well as the usual soluble copolymer. However, following ozonolysis and work up with dimethyl sulphide the whole reaction mixture became soluble. Impurities derived from oligomers with carboxylic acid end groups were removed by preparative ion exchange with a strong base ion exchange resin. The oligomers have potential applications as components of amphiphilic networks. |
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| AbstractList | Telechelic oligomers with dialdehyde end groups and 2,3-dihydroxypropan-1-methacrylate acetonide repeat units were prepared by the ozonolytic cleavage of poly(2,3-dihydroxypropan-1-methacrylate acetonide-
stat-butadiene) copolymers. The latter were prepared by monomer starve-fed emulsion polymerization at elevated temperatures and at atmospheric pressure. In contrast to similar copolymerizations of methyl and butyl methacrylate these polymerizations generated a gel fraction as well as the usual soluble copolymer. However, following ozonolysis and work up with dimethyl sulphide the whole reaction mixture became soluble. Impurities derived from oligomers with carboxylic acid end groups were removed by preparative ion exchange with a strong base ion exchange resin. The oligomers have potential applications as components of amphiphilic networks. |
| Author | Liu, Zuifang Ebdon, John Rimmer, Stephen |
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| CitedBy_id | crossref_primary_10_1016_j_reactfunctpolym_2005_07_014 crossref_primary_10_1002_macp_201100212 crossref_primary_10_1021_ie050144s |
| Cites_doi | 10.1002/marc.1997.030180814 10.1016/1381-5148(95)00014-7 10.1016/0168-3659(93)90100-J 10.1080/10601329408545881 10.1002/masy.19961020112 10.1002/(SICI)1099-0518(199612)34:17<3591::AID-POLA14>3.0.CO;2-9 10.1039/a703859c 10.1021/ma025646l 10.1007/BF00294894 10.1002/pola.1252 10.1002/pola.1994.080321616 10.1021/ma011376f 10.1016/S0032-3861(03)00178-2 10.1002/macp.1993.021940413 10.1080/10601329508018949 10.1002/(SICI)1099-0518(19990715)37:14<2401::AID-POLA14>3.0.CO;2-9 10.1002/(SICI)1099-0518(199612)34:17<3573::AID-POLA12>3.0.CO;2-B 10.1021/ma020362m 10.1002/jbm.820231109 10.1016/S1359-0294(03)00005-0 10.1002/1521-3900(200010)161:1<63::AID-MASY63>3.0.CO;2-1 10.1016/S1381-5148(99)00035-8 10.1002/1521-3900(200107)172:1<56::AID-MASY56>3.0.CO;2-D 10.1002/(SICI)1099-0518(19971115)35:15<3255::AID-POLA19>3.0.CO;2-A 10.1016/S0142-9612(99)00245-8 10.1016/S0142-9612(02)00081-9 |
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| Keywords | Ozonolysis Telechelic oligomer Aldehyde Emulsion Polymerization Methacrylate polymer Butadiene copolymer Emulsion copolymerization Telechelic polymer Chemical degradation Experimental study Dioxolane derivative polymer Random copolymer Dioxolane derivative copolymer Preparation Unsaturated copolymer Methacrylate copolymer Radical copolymerization |
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| Snippet | Telechelic oligomers with dialdehyde end groups and 2,3-dihydroxypropan-1-methacrylate acetonide repeat units were prepared by the ozonolytic cleavage of... |
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| SubjectTerms | Aldehyde Applied sciences Copolymerization Emulsion Polymerization Exact sciences and technology Organic polymers Ozonolysis Physicochemistry of polymers Preparation, kinetics, thermodynamics, mechanism and catalysts Telechelic oligomer |
| Title | Telechelic oligo(2,3-dihydroxypropylmethacrylate acetonide)s with aldehyde end functionality prepared by ozonolytic cleavage of poly(2,3-dihydroxypropan-1-methacrylate acetonide- stat-butadiene), prepared by monomer starve-fed emulsion polymerization |
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