The comparative analyses of reduced graphene oxide (RGO) prepared via green, mild and chemical approaches
In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of Amaranthus hybridus (green) were investigated. Graphene oxide (GO) was synthesized by modified Hummer’s method and was reduced by hydrazine (RGO-HZ), ascorbic acid (RGO-AA) and the ext...
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| Published in | SN applied sciences Vol. 1; no. 10; p. 1181 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
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Springer International Publishing
01.10.2019
Springer Nature B.V |
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| Abstract | In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of
Amaranthus hybridus
(green) were investigated. Graphene oxide (GO) was synthesized by modified Hummer’s method and was reduced by hydrazine (RGO-HZ), ascorbic acid (RGO-AA) and the extract of
Amaranthus hybridus
(RGO-
AH
). GO, RGO-HZ, RGO-AA and RGO-
AH
were characterized using Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy and ultraviolet visible spectrometry. The FTIR spectra showed the presence of oxygen functionality groups in GO which were reduced in all RGOs. The morphological properties showed that RGOs sheets were exfoliated forming clusters with roughened surfaces while the optical energy band gaps of 2.19, 3.90, 3.60, and 3.20 eV were estimated for GO, RGO-HZ, RGO-AA and RGO-
AH
respectively. It can be concluded that the three reductants demonstrated good reducing capacities. The ascorbic acid and the extract of
Amaranthus hybridus
, apart from being environmentally friendly, can also be good substitutes for the dangerous chemical hydrazine. |
|---|---|
| AbstractList | In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of Amaranthus hybridus (green) were investigated. Graphene oxide (GO) was synthesized by modified Hummer’s method and was reduced by hydrazine (RGO-HZ), ascorbic acid (RGO-AA) and the extract of Amaranthus hybridus (RGO-AH). GO, RGO-HZ, RGO-AA and RGO-AH were characterized using Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy and ultraviolet visible spectrometry. The FTIR spectra showed the presence of oxygen functionality groups in GO which were reduced in all RGOs. The morphological properties showed that RGOs sheets were exfoliated forming clusters with roughened surfaces while the optical energy band gaps of 2.19, 3.90, 3.60, and 3.20 eV were estimated for GO, RGO-HZ, RGO-AA and RGO-AH respectively. It can be concluded that the three reductants demonstrated good reducing capacities. The ascorbic acid and the extract of Amaranthus hybridus, apart from being environmentally friendly, can also be good substitutes for the dangerous chemical hydrazine. In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of Amaranthus hybridus (green) were investigated. Graphene oxide (GO) was synthesized by modified Hummer’s method and was reduced by hydrazine (RGO-HZ), ascorbic acid (RGO-AA) and the extract of Amaranthus hybridus (RGO- AH ). GO, RGO-HZ, RGO-AA and RGO- AH were characterized using Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy and ultraviolet visible spectrometry. The FTIR spectra showed the presence of oxygen functionality groups in GO which were reduced in all RGOs. The morphological properties showed that RGOs sheets were exfoliated forming clusters with roughened surfaces while the optical energy band gaps of 2.19, 3.90, 3.60, and 3.20 eV were estimated for GO, RGO-HZ, RGO-AA and RGO- AH respectively. It can be concluded that the three reductants demonstrated good reducing capacities. The ascorbic acid and the extract of Amaranthus hybridus , apart from being environmentally friendly, can also be good substitutes for the dangerous chemical hydrazine. |
| ArticleNumber | 1181 |
| Author | Oluwasusi, T. V. Faniyi, I. O. Eleruja, M. A. Adekunle, A. S. Fasakin, O. Olofinjana, B. Ajayi, E. O. B. |
| Author_xml | – sequence: 1 givenname: I. O. surname: Faniyi fullname: Faniyi, I. O. organization: Department of Physics and Engineering Physics, Obafemi Awolowo University – sequence: 2 givenname: O. surname: Fasakin fullname: Fasakin, O. email: fasakinoladepo@gmail.com organization: Department of Physics and Engineering Physics, Obafemi Awolowo University – sequence: 3 givenname: B. surname: Olofinjana fullname: Olofinjana, B. organization: Department of Physics and Engineering Physics, Obafemi Awolowo University – sequence: 4 givenname: A. S. surname: Adekunle fullname: Adekunle, A. S. organization: Department of Chemistry, Obafemi Awolowo University – sequence: 5 givenname: T. V. surname: Oluwasusi fullname: Oluwasusi, T. V. organization: Department of Physics, Bingham University – sequence: 6 givenname: M. A. surname: Eleruja fullname: Eleruja, M. A. organization: Department of Physics and Engineering Physics, Obafemi Awolowo University – sequence: 7 givenname: E. O. B. surname: Ajayi fullname: Ajayi, E. O. B. organization: Department of Physics and Engineering Physics, Obafemi Awolowo University |
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| Keywords | Graphene oxide Ascorbic acid Reduced graphene oxide Hydrazine |
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| Snippet | In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of
Amaranthus hybridus
(green) were... In this work, the reducing power of three reductants: hydrazine (chemical), ascorbic acid (mild) and the extract of Amaranthus hybridus (green) were... |
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| SubjectTerms | Acids Amaranthus hybridus Antioxidants Applied and Technical Physics Ascorbic acid Chemistry/Food Science Chemistry: Green Chemistry: Multidisciplinary Research Approach Comparative analysis Earth Sciences Energy bands Energy consumption Energy gap Engineering Environment Fourier transforms Graphene Graphite Hydrazine Hydrazines Infrared spectroscopy Materials Science Reducing agents Research Article Scanning electron microscopy Spectrometry Vitamin C |
| Title | The comparative analyses of reduced graphene oxide (RGO) prepared via green, mild and chemical approaches |
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