Solvent extraction of europium and americium into phenyltrifluoromethyl sulfone by using synergistic mixture of hydrogen dicarbollylcobaltate and N,N,N′,N′-tetraethyl-2,6-dipicolinamide
Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H + B − ) in the presence of N,N,N′,N′ -tetraethyl-2,6-dipicolinamide (TEtDPA, L) has been investigated. The equilibrium data have been explained assuming that t...
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Published in | Journal of radioanalytical and nuclear chemistry Vol. 284; no. 3; pp. 629 - 633 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Dordrecht
Springer Netherlands
01.06.2010
Springer |
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Abstract | Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H
+
B
−
) in the presence of
N,N,N′,N′
-tetraethyl-2,6-dipicolinamide (TEtDPA, L) has been investigated. The equilibrium data have been explained assuming that the species HL
+
,
and
(M
3+
= Eu
3+
, Am
3+
) are extracted into the organic phase. The values of extraction and stability constants of the cationic complex species in FS 13 saturated with water have been determined. It was found that the stability constants of the corresponding complexes
and
, where
n
= 2, 3 and L is TEtDPA, in the mentioned FS 13 medium are comparable. |
---|---|
AbstractList | Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H
+
B
−
) in the presence of
N,N,N′,N′
-tetraethyl-2,6-dipicolinamide (TEtDPA, L) has been investigated. The equilibrium data have been explained assuming that the species HL
+
,
and
(M
3+
= Eu
3+
, Am
3+
) are extracted into the organic phase. The values of extraction and stability constants of the cationic complex species in FS 13 saturated with water have been determined. It was found that the stability constants of the corresponding complexes
and
, where
n
= 2, 3 and L is TEtDPA, in the mentioned FS 13 medium are comparable. Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate ([H.sup.+][B.sup.-]) in the presence of N,N,N',N'-tetraethyl-2,6-dipicolinamide (TEtDPA, L) has been investigated. The equilibrium data have been explained assuming that the species H[L.sup.+], H[L.sup.+.sub.2], M[L.sup.3+.sub.2] and M[L.sup.3+.sub.2] ([M.sup.3+] = [Eu.sup.3+], [Am.sup.3+]) are extracted into the organic phase. The values of extraction and stability constants of the cationic complex species in FS 13 saturated with water have been determined. It was found that the stability constants of the corresponding complexes Eu[L.sup.3+.sub.n] and Am[L.sub.3+.sub.n], where n = 2, 3 and L is TEtDPA, in the mentioned FS 13 medium are comparable. Keywords Europium * Americium * Extraction * Phenyltrifluoromethyl sulfone * Dicarbollylcobaltate * N,N,N',N'-tetraethyl-2,6-dipicolinamide * Complexes Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H+B-) in the presence of N,N,N',N'-tetraethyl-2,6-dipicolinamide (TEtDPA, L) has been investigated. The equilibrium data have been explained assuming that the species HL+, \textHL 2 + , HL2+\textML23 + ML23+and \textML 3 3+ ML33+(M3+ = Eu3+, Am3+) are extracted into the organic phase. The values of extraction and stability constants of the cationic complex species in FS 13 saturated with water have been determined. It was found that the stability constants of the corresponding complexes \textEuLn 3+ EuLn3+and \textAmLn 3+ AmLn3+, where n = 2, 3 and L is TEtDPA, in the mentioned FS 13 medium are comparable. |
Audience | Academic |
Author | Vaňura, P. Selucký, P. Smirnov, I. V. Babain, V. A. Makrlík, E. |
Author_xml | – sequence: 1 givenname: E. surname: Makrlík fullname: Makrlík, E. email: makrlik@centrum.cz organization: Faculty of Applied Sciences, University of West Bohemia – sequence: 2 givenname: P. surname: Vaňura fullname: Vaňura, P. organization: Department of Analytical Chemistry, Institute of Chemical Technology – sequence: 3 givenname: P. surname: Selucký fullname: Selucký, P. organization: Nuclear Research Institute – sequence: 4 givenname: V. A. surname: Babain fullname: Babain, V. A. organization: Khlopin Radium Institute, Research and Production Association – sequence: 5 givenname: I. V. surname: Smirnov fullname: Smirnov, I. V. organization: Khlopin Radium Institute, Research and Production Association |
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Cites_doi | 10.1081/SEI-100108822 10.1080/01496398808075625 10.1016/S0956-053X(98)00015-4 10.1080/01496390600744365 10.1081/SEI-100001371 10.1135/cccc19931324 10.1081/SEI-200066296 10.2298/JSC0907781M 10.1016/j.seppur.2003.09.005 10.1007/s10967-006-0071-3 10.2116/analsci.12.225 10.1007/s10967-007-7288-2 10.1081/SEI-100001370 10.1081/SEI-200049898 10.1080/07366299408918205 10.1007/s10967-008-7375-4 10.1135/cccc19920289 10.1007/s10967-006-0037-5 10.1021/ja01006a008 10.1081/SEI-100001376 10.1080/01496399108050526 10.1016/0039-9140(85)80110-7 10.1016/j.aca.2005.04.061 10.1524/ract.2007.95.4.217 10.1007/s10967-007-7203-2 10.1007/s10967-007-7058-6 |
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Keywords | Americium Extraction Dicarbollylcobaltate tetraethyl-2,6-dipicolinamide Europium Phenyltrifluoromethyl sulfone Complexes |
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Snippet | Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H
+
B
−
) in the... Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate ([H.sup.+][B.sup.-])... Extraction of microamounts of europium and americium by a phenyltrifluoromethyl sulfone (FS 13) solution of hydrogen dicarbollylcobaltate (H+B-) in the... |
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StartPage | 629 |
SubjectTerms | Americium Cationic Chemistry Chemistry and Materials Science Cytokinins Diagnostic Radiology Europium Hadrons Heavy Ions Hydrogen Inorganic Chemistry Nuclear Chemistry Nuclear Physics Physical Chemistry Rare earth metals Solvent extraction Stability constants Sulfones |
Title | Solvent extraction of europium and americium into phenyltrifluoromethyl sulfone by using synergistic mixture of hydrogen dicarbollylcobaltate and N,N,N′,N′-tetraethyl-2,6-dipicolinamide |
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