Electrochemical performance of three shaped ZnO nanoparticles prepared in LiOH, NaOH and KOH alkaline solutions as anodic materials for Ni/Zn redox batteries
ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 °C for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH. We analyzed them by X-ray diffraction (XRD), scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS), cyclic voltammetry (CV),...
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| Published in | The Korean journal of chemical engineering Vol. 33; no. 4; pp. 1447 - 1455 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.04.2016
한국화학공학회 |
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| Online Access | Get full text |
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| Abstract | ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 °C for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH. We analyzed them by X-ray diffraction (XRD), scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS), cyclic voltammetry (CV), Zeta potential measurement, and impedance. XRD and SEM showed that the obtained ZnO nanoparticles had high purity and perfect crystallinity, and the morphologies of the particles prepared in the LiOH, NaOH, and KOH solutions showed nanoplate, nanobead, and nanorod shapes, respectively. CV showed that the nanoplate ZnO-LiOH and nanorod ZnO-KOH have superior electrochemical activity to that of the other ZnO nanostructures. As electrode materials of Ni/Zn redox batteries, the nanoplate ZnO-LiOH showed a significantly improved cycle stability after the 30
th
cycle compared to that of ZnO-NaOH and conventional ZnO with a mean discharge capacity of 153 mA h g
−1
, a cell efficiency of 93%, and higher discharge voltages of 1.9. In addition, during the charging/discharging cycles, the growth of zinc dendrite clusters could be suppressed, which resulted in an improvement in the cycle stability of the Ni/nanoplate ZnO-LiOH redox cell. |
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| AbstractList | ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 oC for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH. We analyzed them by X-ray diffraction (XRD), scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS), cyclic voltammetry (CV), Zeta potential measurement, and impedance. XRD and SEM showed that the obtained ZnO nanoparticles had high purity and perfect crystallinity, and the morphologies of the particles prepared in the LiOH, NaOH, and KOH solutions showed nanoplate, nanobead, and nanorod shapes, respectively. CV showed that the nanoplate ZnO-LiOH and nanorod ZnO-KOH have superior electrochemical activity to that of the other ZnO nanostructures. As electrode materials of Ni/Zn redox batteries, the nanoplate ZnO-LiOH showed a significantly improved cycle stability after the 30th cycle compared to that of ZnO-NaOH and conventional ZnO with a mean discharge capacity of 153 mA h g−1, a cell efficiency of 93%, and higher discharge voltages of 1.9. In addition, during the charging/discharging cycles, the growth of zinc dendrite clusters could be suppressed, which resulted in an improvement in the cycle stability of the Ni/nanoplate ZnO-LiOH redox cell. KCI Citation Count: 17 ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 °C for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH. We analyzed them by X-ray diffraction (XRD), scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS), cyclic voltammetry (CV), Zeta potential measurement, and impedance. XRD and SEM showed that the obtained ZnO nanoparticles had high purity and perfect crystallinity, and the morphologies of the particles prepared in the LiOH, NaOH, and KOH solutions showed nanoplate, nanobead, and nanorod shapes, respectively. CV showed that the nanoplate ZnO-LiOH and nanorod ZnO-KOH have superior electrochemical activity to that of the other ZnO nanostructures. As electrode materials of Ni/Zn redox batteries, the nanoplate ZnO-LiOH showed a significantly improved cycle stability after the 30 th cycle compared to that of ZnO-NaOH and conventional ZnO with a mean discharge capacity of 153 mA h g −1 , a cell efficiency of 93%, and higher discharge voltages of 1.9. In addition, during the charging/discharging cycles, the growth of zinc dendrite clusters could be suppressed, which resulted in an improvement in the cycle stability of the Ni/nanoplate ZnO-LiOH redox cell. |
| Author | Lee, Jin-Sik Im, Younghwan Park, Kyoung Soo Cho, Tae Woo Kang, Sora Kwak, Byeong Sub Kang, Misook |
| Author_xml | – sequence: 1 givenname: Younghwan surname: Im fullname: Im, Younghwan organization: Department of Chemistry, College of Science, Yeungnam University – sequence: 2 givenname: Sora surname: Kang fullname: Kang, Sora organization: Department of Chemistry, College of Science, Yeungnam University – sequence: 3 givenname: Byeong Sub surname: Kwak fullname: Kwak, Byeong Sub organization: Department of Chemistry, College of Science, Yeungnam University – sequence: 4 givenname: Kyoung Soo surname: Park fullname: Park, Kyoung Soo organization: Research & Development Center, Vitzrocell Co – sequence: 5 givenname: Tae Woo surname: Cho fullname: Cho, Tae Woo organization: Research & Development Center, Vitzrocell Co – sequence: 6 givenname: Jin-Sik surname: Lee fullname: Lee, Jin-Sik organization: Research & Development Center, Vitzrocell Co – sequence: 7 givenname: Misook surname: Kang fullname: Kang, Misook email: mskang@ynu.ac.kr organization: Department of Chemistry, College of Science, Yeungnam University |
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| Keywords | Charge/Discharge ZnO Nanoparticles Zinc Dendrite Clusters Ni/Zn Redox Battery |
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| Snippet | ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 °C for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH.... ZnO nanoparticles with three morphologies were synthesized by a hydrothermal route at 120 oC for 3 h in high alkaline aqueous solutions of LiOH, NaOH, and KOH.... |
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| SubjectTerms | Biotechnology Catalysis Chemistry Chemistry and Materials Science Electronic Industrial Chemistry/Chemical Engineering Inorganic Materials (Organic Materials Science Thin Films 화학공학 |
| Title | Electrochemical performance of three shaped ZnO nanoparticles prepared in LiOH, NaOH and KOH alkaline solutions as anodic materials for Ni/Zn redox batteries |
| URI | https://link.springer.com/article/10.1007/s11814-015-0280-y https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART002092879 |
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