Acetylene Black/Sulfur Composites Synthesized by a Solution Evaporation Concentration Crystallization Method and Their Electrochemical Properties for Li/S Batteries
A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the ‘solution evaporation concentration crystallization’ method. Three composites with different S loadings were prepared, subject to two different solvent evaporation rates from...
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| Published in | Energies (Basel) Vol. 6; no. 7; pp. 3466 - 3480 |
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| Main Authors | , , , |
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| Language | English |
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01.07.2013
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| Abstract | A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the ‘solution evaporation concentration crystallization’ method. Three composites with different S loadings were prepared, subject to two different solvent evaporation rates from acetylene black (AB)/sulfur in carbon disulfide solutions. X-ray diffraction, environmental scanning electron microscopy, transmission electron microscopy, and Brunauer-Emmett-Teller measurements all show that the porous AB structure is well-filled with S. Composites prepared at a lower solvent evaporation rate with 50 wt % S content, had good electrochemical properties, with 1609.67 mAh g−1 after 100 cycles. Composites with better dispersibility at a low solvent evaporation rate can effectively prevent polysulfide from dissolving in the electrolyte, and serve to stabilize the structure of the S cathode during the charge-discharge process. |
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| AbstractList | A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the ‘solution evaporation concentration crystallization’ method. Three composites with different S loadings were prepared, subject to two different solvent evaporation rates from acetylene black (AB)/sulfur in carbon disulfide solutions. X-ray diffraction, environmental scanning electron microscopy, transmission electron microscopy, and Brunauer-Emmett-Teller measurements all show that the porous AB structure is well-filled with S. Composites prepared at a lower solvent evaporation rate with 50 wt % S content, had good electrochemical properties, with 1609.67 mAh g−1 after 100 cycles. Composites with better dispersibility at a low solvent evaporation rate can effectively prevent polysulfide from dissolving in the electrolyte, and serve to stabilize the structure of the S cathode during the charge-discharge process. A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the 'solution evaporation concentration crystallization' method. Three composites with different S loadings were prepared, subject to two different solvent evaporation rates from acetylene black (AB)/sulfur in carbon disulfide solutions. X-ray diffraction, environmental scanning electron microscopy, transmission electron microscopy, and Brunauer-Emmett-Teller measurements all show that the porous AB structure is well-filled with S. Composites prepared at a lower solvent evaporation rate with 50 wt % S content, had good electrochemical properties, with 1609.67 mAh g-1 after 100 cycles. Composites with better dispersibility at a low solvent evaporation rate can effectively prevent polysulfide from dissolving in the electrolyte, and serve to stabilize the structure of the S cathode during the charge-discharge process. |
| Author | Tan, Haibo Yang, Zhigao Tao, Du Wang, Shengping |
| Author_xml | – sequence: 1 givenname: Haibo surname: Tan fullname: Tan, Haibo – sequence: 2 givenname: Shengping surname: Wang fullname: Wang, Shengping – sequence: 3 givenname: Du surname: Tao fullname: Tao, Du – sequence: 4 givenname: Zhigao surname: Yang fullname: Yang, Zhigao |
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| CitedBy_id | crossref_primary_10_1016_j_apsusc_2017_04_046 crossref_primary_10_1002_aenm_201500118 crossref_primary_10_1016_j_apsusc_2019_02_109 crossref_primary_10_1016_j_jelechem_2021_115564 crossref_primary_10_3390_en14092649 crossref_primary_10_1016_j_electacta_2015_11_116 crossref_primary_10_1016_j_jpowsour_2020_228424 crossref_primary_10_1016_j_jpowsour_2015_01_180 crossref_primary_10_1039_C4TA02821J crossref_primary_10_1002_cssc_201902305 crossref_primary_10_1021_acs_energyfuels_2c00413 |
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| Snippet | A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the ‘solution evaporation... A novel technique to prepare carbon/sulfur composites as cathode materials for Li/S batteries is proposed, which we call the 'solution evaporation... |
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| SubjectTerms | Batteries Carbon Composite materials Crystallization Electrodes Electrolytes Electrons Engineers Lithium lithium sulfur batteries Methods Microscopy solution evaporation concentration crystallization method Solvents Sulfur sulfur/carbon composites |
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| Title | Acetylene Black/Sulfur Composites Synthesized by a Solution Evaporation Concentration Crystallization Method and Their Electrochemical Properties for Li/S Batteries |
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