Sandwich-type ferrocene-functionalized magnetic nanoparticles: synthesis, characterization, and the adsorption of Cr(VI)

In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe 3 O 4 @SiO 2 –FC/COOH) are synthesized using the Fe 3 O 4 as the core and the ferrocene and 5-Aminoisophthalic acid as the functional dendrimers. Taking advantage of high redox activity benef...

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Published in	Journal of materials science. Materials in electronics Vol. 30; no. 15; pp. 13924 - 13932
Main Authors	Danyang, Liu, Yimin, Dai, Jiaqi, Zou, Shengyun, Wang, Qi, Lu, Ling, Chen
Format	Journal Article
Language	English
Published	New York Springer US 01.08.2019 Springer Nature B.V
Subjects	Adsorbents Adsorption Aqueous solutions Characterization and Evaluation of Materials Chemistry and Materials Science Core-shell structure Dendrimers Desorption Iron oxides Materials Science Morphology Nanocomposites Nanoparticles Optical and Electronic Materials Silicon dioxide Trivalent chromium X ray photoelectron spectroscopy
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Abstract	In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe 3 O 4 @SiO 2 –FC/COOH) are synthesized using the Fe 3 O 4 as the core and the ferrocene and 5-Aminoisophthalic acid as the functional dendrimers. Taking advantage of high redox activity benefit of ferrocene, Fe 3 O 4 @SiO 2 –FC/COOH is fabricated to adsorb Cr(VI) and reduce it to nontoxic Cr(III) in aqueous solution. The structure and morphology of prepared magnetic adsorbent are characterized by FTIR, XRD, SEM, XPS, TEM, EDS, and TGA. Moreover, the effects of different factors (such as solution pH, adsorption time, adsorption temperature, adsorbent dosage etc.) on adsorption are evaluated. XPS analysis indicates that Cr(VI) is successfully reduced to nontoxic Cr(III) after adsorption by Fe 3 O 4 @SiO 2 –FC/COOH. The Fe 3 O 4 @SiO 2 –FC/COOH exhibits excellent removal efficiency with a maximum Cr(VI) adsorption of 228.395 mg g −1 at pH 2.0. In addition, the adsorption experimental results fit well with the Freundlich isotherm model and the pseudo-second-order kinetic model. Desorption experiment results demonstrate that the regenerated adsorption capacity can exceed more than 95% after five times adsorption–desorption cycles. Therefore, this work provides a promising approach for Cr(VI) removal from water solution.
AbstractList	In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe 3 O 4 @SiO 2 –FC/COOH) are synthesized using the Fe 3 O 4 as the core and the ferrocene and 5-Aminoisophthalic acid as the functional dendrimers. Taking advantage of high redox activity benefit of ferrocene, Fe 3 O 4 @SiO 2 –FC/COOH is fabricated to adsorb Cr(VI) and reduce it to nontoxic Cr(III) in aqueous solution. The structure and morphology of prepared magnetic adsorbent are characterized by FTIR, XRD, SEM, XPS, TEM, EDS, and TGA. Moreover, the effects of different factors (such as solution pH, adsorption time, adsorption temperature, adsorbent dosage etc.) on adsorption are evaluated. XPS analysis indicates that Cr(VI) is successfully reduced to nontoxic Cr(III) after adsorption by Fe 3 O 4 @SiO 2 –FC/COOH. The Fe 3 O 4 @SiO 2 –FC/COOH exhibits excellent removal efficiency with a maximum Cr(VI) adsorption of 228.395 mg g −1 at pH 2.0. In addition, the adsorption experimental results fit well with the Freundlich isotherm model and the pseudo-second-order kinetic model. Desorption experiment results demonstrate that the regenerated adsorption capacity can exceed more than 95% after five times adsorption–desorption cycles. Therefore, this work provides a promising approach for Cr(VI) removal from water solution. In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe3O4@SiO2–FC/COOH) are synthesized using the Fe3O4 as the core and the ferrocene and 5-Aminoisophthalic acid as the functional dendrimers. Taking advantage of high redox activity benefit of ferrocene, Fe3O4@SiO2–FC/COOH is fabricated to adsorb Cr(VI) and reduce it to nontoxic Cr(III) in aqueous solution. The structure and morphology of prepared magnetic adsorbent are characterized by FTIR, XRD, SEM, XPS, TEM, EDS, and TGA. Moreover, the effects of different factors (such as solution pH, adsorption time, adsorption temperature, adsorbent dosage etc.) on adsorption are evaluated. XPS analysis indicates that Cr(VI) is successfully reduced to nontoxic Cr(III) after adsorption by Fe3O4@SiO2–FC/COOH. The Fe3O4@SiO2–FC/COOH exhibits excellent removal efficiency with a maximum Cr(VI) adsorption of 228.395 mg g−1 at pH 2.0. In addition, the adsorption experimental results fit well with the Freundlich isotherm model and the pseudo-second-order kinetic model. Desorption experiment results demonstrate that the regenerated adsorption capacity can exceed more than 95% after five times adsorption–desorption cycles. Therefore, this work provides a promising approach for Cr(VI) removal from water solution.
Author	Qi, Lu Ling, Chen Shengyun, Wang Jiaqi, Zou Yimin, Dai Danyang, Liu
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Snippet	In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe 3 O 4 @SiO 2 –FC/COOH) are synthesized using the... In this paper, novel ferrocene functionalized sandwich-type core–shell structure magnetic nanocomposites (Fe3O4@SiO2–FC/COOH) are synthesized using the Fe3O4...
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SubjectTerms	Adsorbents Adsorption Aqueous solutions Characterization and Evaluation of Materials Chemistry and Materials Science Core-shell structure Dendrimers Desorption Iron oxides Materials Science Morphology Nanocomposites Nanoparticles Optical and Electronic Materials Silicon dioxide Trivalent chromium X ray photoelectron spectroscopy
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Title	Sandwich-type ferrocene-functionalized magnetic nanoparticles: synthesis, characterization, and the adsorption of Cr(VI)
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