MoS2 microspheres/MOF-derived In2S3 heterostructures with enhanced visible-light photocatalytic activity

MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS 2 microspheres further in situ grew on the surf...

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Published in	Journal of sol-gel science and technology Vol. 94; no. 2; pp. 251 - 256
Main Authors	Wu, Deyong, Wu, Chengyi
Format	Journal Article
Language	English
Published	New York Springer US 01.05.2020 Springer Nature B.V
Subjects	Brief Communication: Sol-gel and hybrid materials for energy Catalytic activity Ceramics Chemistry and Materials Science Composites Dyes Electromagnetic absorption environment and building applications Glass Heterostructures Inorganic Chemistry Light irradiation Materials Science Microspheres Molybdenum disulfide Nanotechnology Natural Materials Optical and Electronic Materials Photocatalysis Photodegradation Precursors Separation Sulfidation X ray photoelectron spectroscopy Visible light Semiconductors Microstructure Metal-organic frameworks Photocatalysis
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Abstract	MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS 2 microspheres further in situ grew on the surface of In 2 S 3 porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In 2 S 3 , MoS 2 /In 2 S 3 heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes. Highlights MIL-68(In) is used as the morphological template and the indium precursor. One-pot synthesis involving a two-step temperature-raising hydrothermal process. Strong visible light absorption and effective separation of photo-generated carries. MoS 2 /In 2 S 3 heterostructures exhibit excellent visible-light photocatalytic activity.
AbstractList	MoS2 microspheres/MOF-derived In2S3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In2S3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS2 microspheres further in situ grew on the surface of In2S3 porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In2S3, MoS2/In2S3 heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes.HighlightsMIL-68(In) is used as the morphological template and the indium precursor.One-pot synthesis involving a two-step temperature-raising hydrothermal process.Strong visible light absorption and effective separation of photo-generated carries.MoS2/In2S3 heterostructures exhibit excellent visible-light photocatalytic activity. MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS 2 microspheres further in situ grew on the surface of In 2 S 3 porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In 2 S 3 , MoS 2 /In 2 S 3 heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes. Highlights MIL-68(In) is used as the morphological template and the indium precursor. One-pot synthesis involving a two-step temperature-raising hydrothermal process. Strong visible light absorption and effective separation of photo-generated carries. MoS 2 /In 2 S 3 heterostructures exhibit excellent visible-light photocatalytic activity.
Author	Wu, Chengyi Wu, Deyong
Author_xml	– sequence: 1 givenname: Deyong surname: Wu fullname: Wu, Deyong email: wdy001815@126.com organization: School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 2 givenname: Chengyi surname: Wu fullname: Wu, Chengyi organization: School of Chemical and Environmental Engineering, Hubei Minzu University
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Selvaraj
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Snippet	MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3... MoS2 microspheres/MOF-derived In2S3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In2S3 porous...
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SubjectTerms	Brief Communication: Sol-gel and hybrid materials for energy Catalytic activity Ceramics Chemistry and Materials Science Composites Dyes Electromagnetic absorption environment and building applications Glass Heterostructures Inorganic Chemistry Light irradiation Materials Science Microspheres Molybdenum disulfide Nanotechnology Natural Materials Optical and Electronic Materials Photocatalysis Photodegradation Precursors Separation Sulfidation X ray photoelectron spectroscopy
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Title	MoS2 microspheres/MOF-derived In2S3 heterostructures with enhanced visible-light photocatalytic activity
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