MoS2 microspheres/MOF-derived In2S3 heterostructures with enhanced visible-light photocatalytic activity
MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS 2 microspheres further in situ grew on the surf...
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Published in | Journal of sol-gel science and technology Vol. 94; no. 2; pp. 251 - 256 |
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Main Authors | , |
Format | Journal Article |
Language | English |
Published |
New York
Springer US
01.05.2020
Springer Nature B.V |
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Abstract | MoS
2
microspheres/MOF-derived In
2
S
3
heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In
2
S
3
porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS
2
microspheres further in situ grew on the surface of In
2
S
3
porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In
2
S
3
, MoS
2
/In
2
S
3
heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes.
Highlights
MIL-68(In) is used as the morphological template and the indium precursor.
One-pot synthesis involving a two-step temperature-raising hydrothermal process.
Strong visible light absorption and effective separation of photo-generated carries.
MoS
2
/In
2
S
3
heterostructures exhibit excellent visible-light photocatalytic activity. |
---|---|
AbstractList | MoS2 microspheres/MOF-derived In2S3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In2S3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS2 microspheres further in situ grew on the surface of In2S3 porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In2S3, MoS2/In2S3 heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes.HighlightsMIL-68(In) is used as the morphological template and the indium precursor.One-pot synthesis involving a two-step temperature-raising hydrothermal process.Strong visible light absorption and effective separation of photo-generated carries.MoS2/In2S3 heterostructures exhibit excellent visible-light photocatalytic activity. MoS 2 microspheres/MOF-derived In 2 S 3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In 2 S 3 porous structures were synthesized via a sulfidation process of MIL-68(In) precursor, and then MoS 2 microspheres further in situ grew on the surface of In 2 S 3 porous structures at the increased temperature. The as-obtained samples were characterized by XRD, SEM, XPS, UV-Vis DRS, and PL. Compared with pure In 2 S 3 , MoS 2 /In 2 S 3 heterostructures exhibited a higher photocatalytic activity towards methyl orange degradation under visible light irradiation, which should be attributed to the stronger visible light absorption as well as the effective separation of photo-generated electrons and holes. Highlights MIL-68(In) is used as the morphological template and the indium precursor. One-pot synthesis involving a two-step temperature-raising hydrothermal process. Strong visible light absorption and effective separation of photo-generated carries. MoS 2 /In 2 S 3 heterostructures exhibit excellent visible-light photocatalytic activity. |
Author | Wu, Chengyi Wu, Deyong |
Author_xml | – sequence: 1 givenname: Deyong surname: Wu fullname: Wu, Deyong email: wdy001815@126.com organization: School of Chemical and Environmental Engineering, Hubei Minzu University – sequence: 2 givenname: Chengyi surname: Wu fullname: Wu, Chengyi organization: School of Chemical and Environmental Engineering, Hubei Minzu University |
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CitedBy_id | crossref_primary_10_1002_asia_202400161 crossref_primary_10_1016_j_jssc_2021_122287 crossref_primary_10_1002_smll_202102307 crossref_primary_10_1515_revce_2022_0026 crossref_primary_10_1016_j_physb_2024_416053 crossref_primary_10_1016_S1872_2067_21_63934_7 crossref_primary_10_1039_D2CE01055K crossref_primary_10_1016_j_jcis_2023_01_116 crossref_primary_10_1016_j_seppur_2024_128063 crossref_primary_10_1016_j_synthmet_2021_116815 crossref_primary_10_1002_slct_202004839 |
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Selvaraj |
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microspheres/MOF-derived In
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heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In
2
S
3... MoS2 microspheres/MOF-derived In2S3 heterostructures were fabricated through a two-step temperature-raising hydrothermal method. MOF-derived In2S3 porous... |
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SubjectTerms | Brief Communication: Sol-gel and hybrid materials for energy Catalytic activity Ceramics Chemistry and Materials Science Composites Dyes Electromagnetic absorption environment and building applications Glass Heterostructures Inorganic Chemistry Light irradiation Materials Science Microspheres Molybdenum disulfide Nanotechnology Natural Materials Optical and Electronic Materials Photocatalysis Photodegradation Precursors Separation Sulfidation X ray photoelectron spectroscopy |
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Title | MoS2 microspheres/MOF-derived In2S3 heterostructures with enhanced visible-light photocatalytic activity |
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