Spectroscopic, Structural, Thermal, and Mechanical Properties of B2O3-CeO2-PbO2 Glasses
The melt-quenching method has been used to fabricate a PbO 2 –B 2 O 3 –CeO 2 glass system. The XRD diffractometer procedure was used to check the status of these samples. It can be concluded, from the X-ray diffraction curves, that the tested samples have high levels of glassiness. As the CeO 2 conc...
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| Published in | Journal of inorganic and organometallic polymers and materials Vol. 31; no. 4; pp. 1774 - 1786 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.04.2021
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1574-1443 1574-1451 |
| DOI | 10.1007/s10904-020-01799-w |
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| Abstract | The melt-quenching method has been used to fabricate a PbO
2
–B
2
O
3
–CeO
2
glass system. The XRD diffractometer procedure was used to check the status of these samples. It can be concluded, from the X-ray diffraction curves, that the tested samples have high levels of glassiness. As the CeO
2
concentration increased most of the [BO
4
] are converted into [BO
3
] structural units with the formation of non-bridging oxygen ions in the borate matrix. It can be cross verified with the decrease of the
N
4
fraction from 0.654 to 0.239. This decrease may be attributed to the formation of [CeO
7
] structural units that needs more oxygen atoms. The ultrasonic velocities of the prepared glasses are decreased with the increase of CeO
2
content. Different types of elastic modules were evaluated (experimental and theoretical) for the prepared glasses are increases with the increase of CeO
2
content. Glass transition temperature (T
g
), crystallization temperature (T
c
), the peak of crystallization temperature (T
p
) and thermal stability values decreases with the increase of CeO
2
content. The refractive index of these samples is increasing with the increase in the reflection and the density. |
|---|---|
| AbstractList | The melt-quenching method has been used to fabricate a PbO
2
–B
2
O
3
–CeO
2
glass system. The XRD diffractometer procedure was used to check the status of these samples. It can be concluded, from the X-ray diffraction curves, that the tested samples have high levels of glassiness. As the CeO
2
concentration increased most of the [BO
4
] are converted into [BO
3
] structural units with the formation of non-bridging oxygen ions in the borate matrix. It can be cross verified with the decrease of the
N
4
fraction from 0.654 to 0.239. This decrease may be attributed to the formation of [CeO
7
] structural units that needs more oxygen atoms. The ultrasonic velocities of the prepared glasses are decreased with the increase of CeO
2
content. Different types of elastic modules were evaluated (experimental and theoretical) for the prepared glasses are increases with the increase of CeO
2
content. Glass transition temperature (T
g
), crystallization temperature (T
c
), the peak of crystallization temperature (T
p
) and thermal stability values decreases with the increase of CeO
2
content. The refractive index of these samples is increasing with the increase in the reflection and the density. The melt-quenching method has been used to fabricate a PbO2–B2O3–CeO2 glass system. The XRD diffractometer procedure was used to check the status of these samples. It can be concluded, from the X-ray diffraction curves, that the tested samples have high levels of glassiness. As the CeO2 concentration increased most of the [BO4] are converted into [BO3] structural units with the formation of non-bridging oxygen ions in the borate matrix. It can be cross verified with the decrease of the N4 fraction from 0.654 to 0.239. This decrease may be attributed to the formation of [CeO7] structural units that needs more oxygen atoms. The ultrasonic velocities of the prepared glasses are decreased with the increase of CeO2 content. Different types of elastic modules were evaluated (experimental and theoretical) for the prepared glasses are increases with the increase of CeO2 content. Glass transition temperature (Tg), crystallization temperature (Tc), the peak of crystallization temperature (Tp) and thermal stability values decreases with the increase of CeO2 content. The refractive index of these samples is increasing with the increase in the reflection and the density. |
| Author | Zahran, H. Y. Shaaban, Kh. S. Yahia, I. S. El-Rehim, A. F. Abd Ali, Atif Mossad |
| Author_xml | – sequence: 1 givenname: A. F. Abd surname: El-Rehim fullname: El-Rehim, A. F. Abd organization: Physics Department, Faculty of Science, King Khalid University, Physics Department, Faculty of Education, Ain Shams University – sequence: 2 givenname: Atif Mossad surname: Ali fullname: Ali, Atif Mossad email: atifalimossad@gmail.com organization: Physics Department, Faculty of Science, King Khalid University, Physics Department, Faculty of Science, Assiut University – sequence: 3 givenname: H. Y. surname: Zahran fullname: Zahran, H. Y. organization: Physics Department, Faculty of Science, King Khalid University, Physics Department, Faculty of Education, Ain Shams University – sequence: 4 givenname: I. S. surname: Yahia fullname: Yahia, I. S. organization: Physics Department, Faculty of Science, King Khalid University, Physics Department, Faculty of Education, Ain Shams University – sequence: 5 givenname: Kh. S. surname: Shaaban fullname: Shaaban, Kh. S. email: khamies1078@yahoo.com organization: Chemistry Department, Faculty of Science, Al-Azhar University |
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| Snippet | The melt-quenching method has been used to fabricate a PbO
2
–B
2
O
3
–CeO
2
glass system. The XRD diffractometer procedure was used to check the status of... The melt-quenching method has been used to fabricate a PbO2–B2O3–CeO2 glass system. The XRD diffractometer procedure was used to check the status of these... |
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| SubjectTerms | Boron oxides Cerium oxides Chemistry Chemistry and Materials Science Crystallization Glass transition temperature Inorganic Chemistry Lead oxides Mechanical properties Organic Chemistry Oxygen atoms Oxygen ions Polymer Sciences Refractivity Thermal stability |
| Title | Spectroscopic, Structural, Thermal, and Mechanical Properties of B2O3-CeO2-PbO2 Glasses |
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