Investigating nano-precipitation in a V-containing HSLA steel using small angle neutron scattering

Interphase precipitation (IPP) of nanoscale carbides in a vanadium-containing high-strength low-alloy steel has been investigated. Small angle neutron scattering (SANS) and transmission electron microscopy (TEM) were employed to characterize the precipitates and their size distributions in Fe-0.047C...

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Published inActa materialia Vol. 145; pp. 84 - 96
Main Authors Wang, Y.Q., Clark, S.J., Janik, V., Heenan, R.K., Venero, D. Alba, Yan, K., McCartney, D.G., Sridhar, S., Lee, P.D.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 15.02.2018
Subjects
Microalloyed steel
Precipitation
Small angle scattering
Transmission electron microscopy
Small angle scattering
Precipitation
Transmission electron microscopy
Microalloyed steel
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Abstract Interphase precipitation (IPP) of nanoscale carbides in a vanadium-containing high-strength low-alloy steel has been investigated. Small angle neutron scattering (SANS) and transmission electron microscopy (TEM) were employed to characterize the precipitates and their size distributions in Fe-0.047C-0.2V-1.6Mn (in wt.%) alloy samples which had been austenitized, isothermally transformed at 700 °C for between 3 and 600 min and water quenched. TEM confirms that, following heat treatment, rows of vanadium-containing nanoscale interphase precipitates were present. Model-independent analysis of the nuclear SANS signal and model fitting calculations, using oblate spheroid and disc-shapes, were performed. The major axis diameter increased from 18 nm after 3 min to 35 nm after 600 min. Precipitate volume percent increased from 0.09 to 0.22 vol% over the same period and number density fell from 2 × 1021 to 5 × 1020 m−3. A limited number of measurements of precipitate maximum diameters from TEM images showed the mean value increased from 8 nm after 5 min to 28 nm after 600 min which is in reasonable agreement with the SANS data. [Display omitted]
AbstractList Interphase precipitation (IPP) of nanoscale carbides in a vanadium-containing high-strength low-alloy steel has been investigated. Small angle neutron scattering (SANS) and transmission electron microscopy (TEM) were employed to characterize the precipitates and their size distributions in Fe-0.047C-0.2V-1.6Mn (in wt.%) alloy samples which had been austenitized, isothermally transformed at 700 °C for between 3 and 600 min and water quenched. TEM confirms that, following heat treatment, rows of vanadium-containing nanoscale interphase precipitates were present. Model-independent analysis of the nuclear SANS signal and model fitting calculations, using oblate spheroid and disc-shapes, were performed. The major axis diameter increased from 18 nm after 3 min to 35 nm after 600 min. Precipitate volume percent increased from 0.09 to 0.22 vol% over the same period and number density fell from 2 × 1021 to 5 × 1020 m−3. A limited number of measurements of precipitate maximum diameters from TEM images showed the mean value increased from 8 nm after 5 min to 28 nm after 600 min which is in reasonable agreement with the SANS data. [Display omitted]
Author Lee, P.D.
Venero, D. Alba
McCartney, D.G.
Sridhar, S.
Clark, S.J.
Janik, V.
Heenan, R.K.
Wang, Y.Q.
Yan, K.
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Snippet Interphase precipitation (IPP) of nanoscale carbides in a vanadium-containing high-strength low-alloy steel has been investigated. Small angle neutron...
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SubjectTerms Microalloyed steel
Precipitation
Small angle scattering
Transmission electron microscopy
Title Investigating nano-precipitation in a V-containing HSLA steel using small angle neutron scattering
URI https://dx.doi.org/10.1016/j.actamat.2017.11.032
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