Study on Sorption Characteristics of Uranium onto Biochar Derived from Eucalyptus Wood
In this study, the sorption characteristics of U(VI) onto eucalyptus biochar as a function of various operating parameters such as solution pH, initial metal ion concentration, contact time and ionic strength of the medium are reported. Biochar was characterised using various techniques such as CHNS...
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Published in | Water, air, and soil pollution Vol. 228; no. 8; p. 1 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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01.08.2017
Springer Springer Nature B.V |
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Abstract | In this study, the sorption characteristics of U(VI) onto eucalyptus biochar as a function of various operating parameters such as solution pH, initial metal ion concentration, contact time and ionic strength of the medium are reported. Biochar was characterised using various techniques such as CHNS element analysis, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS). SEM analysis showed the presence of micro- and macropores in the sorbent, and FTIR spectra confirmed the presence of functional groups like carboxylic (−COOH), hydroxyls(−OH), carbonyls(–C=O), etc. Maximum sorption of about 95% is found to occur in the pH range of 5 to 6. U(VI) sorption onto biochar reached equilibrium within 20 min at pH 5.5. The kinetic data were analysed using both pseudo-first-order and pseudo-second-order kinetic models, and the latter is found to be more appropriate to explain the observed kinetics. The equilibrium data were correlated with Langmuir and Freundlich models, and the maximum monolayer adsorption capacity obtained from the Langmuir model was 27.2 mg/g at 293 K. From EDS, FTIR and XPS measurements, it is found that the sorption process involves chemical interaction between the U(VI) and the surface functional groups on the adsorbent. Efficient removal of low level of uranium from ammonium diuranate supernatant demonstrates its utility as sorbent for waste water treatment. |
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AbstractList | In this study, the sorption characteristics of U(VI) onto eucalyptus biochar as a function of various operating parameters such as solution pH, initial metal ion concentration, contact time and ionic strength of the medium are reported. Biochar was characterised using various techniques such as CHNS element analysis, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS). SEM analysis showed the presence of micro- and macropores in the sorbent, and FTIR spectra confirmed the presence of functional groups like carboxylic (-COOH), hydroxyls(-OH), carbonyls(-C=O), etc. Maximum sorption of about 95% is found to occur in the pH range of 5 to 6. U(VI) sorption onto biochar reached equilibrium within 20 min at pH 5.5. The kinetic data were analysed using both pseudo-first-order and pseudo-second-order kinetic models, and the latter is found to be more appropriate to explain the observed kinetics. The equilibrium data were correlated with Langmuir and Freundlich models, and the maximum monolayer adsorption capacity obtained from the Langmuir model was 27.2 mg/g at 293 K. From EDS, FTIR and XPS measurements, it is found that the sorption process involves chemical interaction between the U(VI) and the surface functional groups on the adsorbent. Efficient removal of low level of uranium from ammonium diuranate supernatant demonstrates its utility as sorbent for waste water treatment. In this study, the sorption characteristics of U(VI) onto eucalyptus biochar as a function of various operating parameters such as solution pH, initial metal ion concentration, contact time and ionic strength of the medium are reported. Biochar was characterised using various techniques such as CHNS element analysis, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS). SEM analysis showed the presence of micro- and macropores in the sorbent, and FTIR spectra confirmed the presence of functional groups like carboxylic (−COOH), hydroxyls(−OH), carbonyls(–C=O), etc. Maximum sorption of about 95% is found to occur in the pH range of 5 to 6. U(VI) sorption onto biochar reached equilibrium within 20 min at pH 5.5. The kinetic data were analysed using both pseudo-first-order and pseudo-second-order kinetic models, and the latter is found to be more appropriate to explain the observed kinetics. The equilibrium data were correlated with Langmuir and Freundlich models, and the maximum monolayer adsorption capacity obtained from the Langmuir model was 27.2 mg/g at 293 K. From EDS, FTIR and XPS measurements, it is found that the sorption process involves chemical interaction between the U(VI) and the surface functional groups on the adsorbent. Efficient removal of low level of uranium from ammonium diuranate supernatant demonstrates its utility as sorbent for waste water treatment. |
ArticleNumber | 309 |
Audience | Academic |
Author | Mishra, Vijayakriti Sureshkumar, M. K. Gupta, Nidhi Kaushik, C. P. |
Author_xml | – sequence: 1 givenname: Vijayakriti surname: Mishra fullname: Mishra, Vijayakriti email: vijayakm@barc.gov.in organization: Radiation Safety Systems Division, Bhabha Atomic Research Centre – sequence: 2 givenname: M. K. surname: Sureshkumar fullname: Sureshkumar, M. K. organization: Radiation Safety Systems Division, Bhabha Atomic Research Centre – sequence: 3 givenname: Nidhi surname: Gupta fullname: Gupta, Nidhi organization: Technical Physics Division, Bhabha Atomic Research Centre – sequence: 4 givenname: C. P. surname: Kaushik fullname: Kaushik, C. P. organization: Waste Management Division, Bhabha Atomic Research Centre |
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SubjectTerms | Adsorbents Adsorption Ammonium Ammonium compounds Analytical methods Atmospheric Protection/Air Quality Control/Air Pollution Capacity Carbonyl compounds Carbonyls Climate Change/Climate Change Impacts Data processing Earth and Environmental Science Electron microscopy Energy dispersive X ray spectroscopy Environment Environmental monitoring Eucalyptus Fourier transforms Functional groups Hydrogeology Infrared analysis Infrared spectroscopy Ion concentration Ionic strength Ions Kinetics Low level Metals Nuclear energy pH effects Photoelectron spectroscopy Reaction kinetics Removal Scanning electron microscopy Soil Science & Conservation Sorption Spectroscopic analysis Spectrum analysis Surface chemistry Thermogravimetric analysis Uranium Wastewater Wastewater treatment Water Quality/Water Pollution Water treatment Wood X ray photoelectron spectroscopy X-ray spectroscopy |
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Title | Study on Sorption Characteristics of Uranium onto Biochar Derived from Eucalyptus Wood |
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