pH-Dependent Self-Assembly of Complexes with Tripodal Amino Acid Ligand
Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH values. Their structures were characterized by X‐ray crystallography. Interestingly, under acidic conditions, the dinuclear structure {Cu2[H(L)]2Cl2}(ClO4)...
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| Published in | Zeitschrift für anorganische und allgemeine Chemie (1950) Vol. 639; no. 5; pp. 733 - 738 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English German |
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Weinheim
WILEY-VCH Verlag
01.04.2013
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| Abstract | Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH values. Their structures were characterized by X‐ray crystallography. Interestingly, under acidic conditions, the dinuclear structure {Cu2[H(L)]2Cl2}(ClO4)2 (1) was obtained, whereas under alkaline conditions, the complexes {[Cu(L)](ClO4)}n (2) and [Cd(L)Cl]n (3), which exhibit distinct one‐dimensional (1D) structures, were obtained. The results indicate that the pH value, metal ions, and anions have remarkable influence on the formation and structure of the complexes. |
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| AbstractList | Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH values. Their structures were characterized by X‐ray crystallography. Interestingly, under acidic conditions, the dinuclear structure {Cu2[H(L)]2Cl2}(ClO4)2 (1) was obtained, whereas under alkaline conditions, the complexes {[Cu(L)](ClO4)}n (2) and [Cd(L)Cl]n (3), which exhibit distinct one‐dimensional (1D) structures, were obtained. The results indicate that the pH value, metal ions, and anions have remarkable influence on the formation and structure of the complexes. Three new metal complexes were synthesized by reactions of [bis(2-amino-ethyl)-amino]-acetic acid (HL) and different metal salts at different pH values. Their structures were characterized by X-ray crystallography. Interestingly, under acidic conditions, the dinuclear structure {Cu2[H(L)]2Cl2}(ClO4)2 (1) was obtained, whereas under alkaline conditions, the complexes {[Cu(L)](ClO4)}n (2) and [Cd(L)Cl]n (3), which exhibit distinct one-dimensional (1D) structures, were obtained. The results indicate that the pH value, metal ions, and anions have remarkable influence on the formation and structure of the complexes. [PUBLICATION ABSTRACT] Abstract Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH values. Their structures were characterized by X‐ray crystallography. Interestingly, under acidic conditions, the dinuclear structure {Cu 2 [H(L)] 2 Cl 2 }(ClO 4 ) 2 ( 1 ) was obtained, whereas under alkaline conditions, the complexes {[Cu(L)](ClO 4 )} n ( 2 ) and [Cd(L)Cl] n ( 3 ), which exhibit distinct one‐dimensional (1D) structures, were obtained. The results indicate that the pH value, metal ions, and anions have remarkable influence on the formation and structure of the complexes. |
| Author | Zhang, Hui Cheng, Xing Li, Pei-Yu Qi, Zhao-Peng Zhou, Hong-Fei Zhou, Lei |
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| CitedBy_id | crossref_primary_10_1016_j_poly_2014_11_037 crossref_primary_10_1002_hc_21454 crossref_primary_10_1016_j_poly_2013_11_006 crossref_primary_10_1016_j_ica_2021_120436 crossref_primary_10_1016_j_poly_2016_10_016 |
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| Snippet | Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH values. Their... Abstract Three new metal complexes were synthesized by reactions of [bis(2‐amino‐ethyl)‐amino]‐acetic acid (HL) and different metal salts at different pH... Three new metal complexes were synthesized by reactions of [bis(2-amino-ethyl)-amino]-acetic acid (HL) and different metal salts at different pH values. Their... |
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| StartPage | 733 |
| SubjectTerms | Cadmium Copper Crystal growth Self-assembly |
| Title | pH-Dependent Self-Assembly of Complexes with Tripodal Amino Acid Ligand |
| URI | https://api.istex.fr/ark:/67375/WNG-GT75V64S-H/fulltext.pdf https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fzaac.201200527 https://www.proquest.com/docview/1346192476 |
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